Structural and electrical properties of Nb-substituted LiTa1-xNbxO3

Single phase LiTa1-xNbxO3 solid solution with 0.00 ≤ x ≤ 1.00 was successfully synthesised via conventional solid-state method at 950°C for 24 h. These materials were refined and fully indexed with hexagonal crystal system, space group of R3c; lattice parameters, a ranging from 5.1410(6) Ǻ to 5.1471...

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Main Authors: Bak, K. Y., Tan, Kar Ban, Khaw, Chwin Chieh, Zainal, Zulkarnain, Tan, P. Y., Chon, Mun Ping
Format: Article
Language:English
Published: Penerbit Universiti Kebangsaan Malaysia 2014
Online Access:http://psasir.upm.edu.my/id/eprint/35490/
http://psasir.upm.edu.my/id/eprint/35490/1/Structural%20and%20electrical%20properties%20of%20Nb-substituted%20LiTa1-xNbxO3.pdf
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author Bak, K. Y.
Tan, Kar Ban
Khaw, Chwin Chieh
Zainal, Zulkarnain
Tan, P. Y.
Chon, Mun Ping
author_facet Bak, K. Y.
Tan, Kar Ban
Khaw, Chwin Chieh
Zainal, Zulkarnain
Tan, P. Y.
Chon, Mun Ping
author_sort Bak, K. Y.
building UPM Institutional Repository
collection Online Access
description Single phase LiTa1-xNbxO3 solid solution with 0.00 ≤ x ≤ 1.00 was successfully synthesised via conventional solid-state method at 950°C for 24 h. These materials were refined and fully indexed with hexagonal crystal system, space group of R3c; lattice parameters, a ranging from 5.1410(6) Ǻ to 5.1471(3) Ǻ and c ranging from 13.7467(1) Ǻ to 13.8341(1) Ǻ; with α = β = 90° and γ = 120°. Variation of the lattice parameters in these materials was found to be negligibly small throughout the subsolidus solution. No thermal event was detected within the studied temperature range of 50 to 1000°C. The electrical properties of samples were characterised by AC impedance analyser, HP4192A at temperature ranging from room temperature to 850°C over a frequency range of 5 Hz to 13 MHz. LiTa1-xNbxO3 materials exhibited bulk response with associated capacitances in the order of 10-12 F cm-1 and the temperature-dependent conductivities were found to increase with increasing temperatures. The results showed that LiTa1-xNbxO3 samples were of typical ferroelectrics.
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spelling upm-354902018-10-17T00:45:33Z http://psasir.upm.edu.my/id/eprint/35490/ Structural and electrical properties of Nb-substituted LiTa1-xNbxO3 Bak, K. Y. Tan, Kar Ban Khaw, Chwin Chieh Zainal, Zulkarnain Tan, P. Y. Chon, Mun Ping Single phase LiTa1-xNbxO3 solid solution with 0.00 ≤ x ≤ 1.00 was successfully synthesised via conventional solid-state method at 950°C for 24 h. These materials were refined and fully indexed with hexagonal crystal system, space group of R3c; lattice parameters, a ranging from 5.1410(6) Ǻ to 5.1471(3) Ǻ and c ranging from 13.7467(1) Ǻ to 13.8341(1) Ǻ; with α = β = 90° and γ = 120°. Variation of the lattice parameters in these materials was found to be negligibly small throughout the subsolidus solution. No thermal event was detected within the studied temperature range of 50 to 1000°C. The electrical properties of samples were characterised by AC impedance analyser, HP4192A at temperature ranging from room temperature to 850°C over a frequency range of 5 Hz to 13 MHz. LiTa1-xNbxO3 materials exhibited bulk response with associated capacitances in the order of 10-12 F cm-1 and the temperature-dependent conductivities were found to increase with increasing temperatures. The results showed that LiTa1-xNbxO3 samples were of typical ferroelectrics. Penerbit Universiti Kebangsaan Malaysia 2014-10 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/35490/1/Structural%20and%20electrical%20properties%20of%20Nb-substituted%20LiTa1-xNbxO3.pdf Bak, K. Y. and Tan, Kar Ban and Khaw, Chwin Chieh and Zainal, Zulkarnain and Tan, P. Y. and Chon, Mun Ping (2014) Structural and electrical properties of Nb-substituted LiTa1-xNbxO3. Sains Malaysiana, 43 (10). pp. 1573-1582. ISSN 0026-6039 http://www.ukm.my/jsm/english_journals/vol43num10_2014/contentsVol43num10_2014.html
spellingShingle Bak, K. Y.
Tan, Kar Ban
Khaw, Chwin Chieh
Zainal, Zulkarnain
Tan, P. Y.
Chon, Mun Ping
Structural and electrical properties of Nb-substituted LiTa1-xNbxO3
title Structural and electrical properties of Nb-substituted LiTa1-xNbxO3
title_full Structural and electrical properties of Nb-substituted LiTa1-xNbxO3
title_fullStr Structural and electrical properties of Nb-substituted LiTa1-xNbxO3
title_full_unstemmed Structural and electrical properties of Nb-substituted LiTa1-xNbxO3
title_short Structural and electrical properties of Nb-substituted LiTa1-xNbxO3
title_sort structural and electrical properties of nb-substituted lita1-xnbxo3
url http://psasir.upm.edu.my/id/eprint/35490/
http://psasir.upm.edu.my/id/eprint/35490/
http://psasir.upm.edu.my/id/eprint/35490/1/Structural%20and%20electrical%20properties%20of%20Nb-substituted%20LiTa1-xNbxO3.pdf