Microstructural and Dielectric Properties of Ni-Zn and Li-Ni-Zn Ferrites by Impedance Spectroscopy.

The real and imaginary parts of the complex impedances and the loss angle (8) of iO.5Zn05Fe20, and (Lioleo.5)O.5Nio.2ZnO.3 Fe20, ferrites were measured at 300 K in the frequency range of 1 - 10 MHz using a frequency response analyser. The complex - plane impedance spectra of the samples are associa...

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Main Authors: Abdullah, Mustaffa, Yusoff, Ahmad Nazlim
Format: Article
Language:English
English
Published: Universiti Putra Malaysia Press 1998
Online Access:http://psasir.upm.edu.my/id/eprint/3425/
http://psasir.upm.edu.my/id/eprint/3425/1/Microstructural_and_Dielectric_Properties_of_Ni-Zn_and_Li-Ni-Zn.pdf
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author Abdullah, Mustaffa
Yusoff, Ahmad Nazlim
author_facet Abdullah, Mustaffa
Yusoff, Ahmad Nazlim
author_sort Abdullah, Mustaffa
building UPM Institutional Repository
collection Online Access
description The real and imaginary parts of the complex impedances and the loss angle (8) of iO.5Zn05Fe20, and (Lioleo.5)O.5Nio.2ZnO.3 Fe20, ferrites were measured at 300 K in the frequency range of 1 - 10 MHz using a frequency response analyser. The complex - plane impedance spectra of the samples are associated with equivalent circuits composed of resistive and capacitive elements due to the bulk (grain) and the grain boundary components. The measured and simulated impedances were analysed using the complex nonlinear least square (CNLS) fitting method. The simulated components of the circuit are interpreted as the characteristic parameters of the microstructural properties of the materials. Microstructural properties are complemented by a morphological study using a scanning electron microscope. The dielectric properties at low and high frequency regimes are interpreted as mainly due to the interfacial and orientational polarizations respectively. A region of negative capacitances at low frequencies is observed for both samples. Frequency dependence of the characteristic parameters of the microstructural components and the dielectric behaviour of the materials are discussed.
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spelling upm-34252014-09-17T08:54:58Z http://psasir.upm.edu.my/id/eprint/3425/ Microstructural and Dielectric Properties of Ni-Zn and Li-Ni-Zn Ferrites by Impedance Spectroscopy. Abdullah, Mustaffa Yusoff, Ahmad Nazlim The real and imaginary parts of the complex impedances and the loss angle (8) of iO.5Zn05Fe20, and (Lioleo.5)O.5Nio.2ZnO.3 Fe20, ferrites were measured at 300 K in the frequency range of 1 - 10 MHz using a frequency response analyser. The complex - plane impedance spectra of the samples are associated with equivalent circuits composed of resistive and capacitive elements due to the bulk (grain) and the grain boundary components. The measured and simulated impedances were analysed using the complex nonlinear least square (CNLS) fitting method. The simulated components of the circuit are interpreted as the characteristic parameters of the microstructural properties of the materials. Microstructural properties are complemented by a morphological study using a scanning electron microscope. The dielectric properties at low and high frequency regimes are interpreted as mainly due to the interfacial and orientational polarizations respectively. A region of negative capacitances at low frequencies is observed for both samples. Frequency dependence of the characteristic parameters of the microstructural components and the dielectric behaviour of the materials are discussed. Universiti Putra Malaysia Press 1998 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/3425/1/Microstructural_and_Dielectric_Properties_of_Ni-Zn_and_Li-Ni-Zn.pdf Abdullah, Mustaffa and Yusoff, Ahmad Nazlim (1998) Microstructural and Dielectric Properties of Ni-Zn and Li-Ni-Zn Ferrites by Impedance Spectroscopy. Pertanika Journal of Science & Technology, 6 (2). pp. 95-105. ISSN 0128-7680 English
spellingShingle Abdullah, Mustaffa
Yusoff, Ahmad Nazlim
Microstructural and Dielectric Properties of Ni-Zn and Li-Ni-Zn Ferrites by Impedance Spectroscopy.
title Microstructural and Dielectric Properties of Ni-Zn and Li-Ni-Zn Ferrites by Impedance Spectroscopy.
title_full Microstructural and Dielectric Properties of Ni-Zn and Li-Ni-Zn Ferrites by Impedance Spectroscopy.
title_fullStr Microstructural and Dielectric Properties of Ni-Zn and Li-Ni-Zn Ferrites by Impedance Spectroscopy.
title_full_unstemmed Microstructural and Dielectric Properties of Ni-Zn and Li-Ni-Zn Ferrites by Impedance Spectroscopy.
title_short Microstructural and Dielectric Properties of Ni-Zn and Li-Ni-Zn Ferrites by Impedance Spectroscopy.
title_sort microstructural and dielectric properties of ni-zn and li-ni-zn ferrites by impedance spectroscopy.
url http://psasir.upm.edu.my/id/eprint/3425/
http://psasir.upm.edu.my/id/eprint/3425/1/Microstructural_and_Dielectric_Properties_of_Ni-Zn_and_Li-Ni-Zn.pdf