Hidroksida Berlapis Ganda ZnCrCI: Kesan Haba Terhadap Luas Perm.ukaan dan Keliangan

ZnCrCI layered double hydroxides, with Zn/Cr ratios (R) 3 and 4 were prepared by a coprecipitation method and heat treated samples were subsequently prepared. Their bulk structure was investigated by X-ray diffraction and surface area techniques. X-ray diffraction analysis showed that the layered d...

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Main Authors: Hussien, Mohd Zobir, Zainal, Zulkarnain, Ibrahim, Ramli, Hii, Hiong Swee
Format: Article
Language:English
English
Published: Universiti Putra Malaysia Press 1996
Online Access:http://psasir.upm.edu.my/id/eprint/3225/
http://psasir.upm.edu.my/id/eprint/3225/1/Hidroksida_Berlapis_Ganda_ZnCrCI_Kesan_Haba.pdf
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author Hussien, Mohd Zobir
Zainal, Zulkarnain
Ibrahim, Ramli
Hii, Hiong Swee
author_facet Hussien, Mohd Zobir
Zainal, Zulkarnain
Ibrahim, Ramli
Hii, Hiong Swee
author_sort Hussien, Mohd Zobir
building UPM Institutional Repository
collection Online Access
description ZnCrCI layered double hydroxides, with Zn/Cr ratios (R) 3 and 4 were prepared by a coprecipitation method and heat treated samples were subsequently prepared. Their bulk structure was investigated by X-ray diffraction and surface area techniques. X-ray diffraction analysis showed that the layered double hydroxide phase remained unchanged upon heating up to 250°C for 5 h in an oven at atmospheric pressure. However, new phases, namely spinel-like and ZnO phases appeared when the samples were heated at 350°C and above for the same duration. The specific surface areas decreased with increasing temperature (between 450850° C) for both R values but no trend was observed for temperatures between 250-350°C. Average pore diameter was found to be optimum at 550°C and 450°C for R = 3 and 4, respectively.
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language English
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publishDate 1996
publisher Universiti Putra Malaysia Press
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spelling upm-32252013-05-27T07:06:34Z http://psasir.upm.edu.my/id/eprint/3225/ Hidroksida Berlapis Ganda ZnCrCI: Kesan Haba Terhadap Luas Perm.ukaan dan Keliangan Hussien, Mohd Zobir Zainal, Zulkarnain Ibrahim, Ramli Hii, Hiong Swee ZnCrCI layered double hydroxides, with Zn/Cr ratios (R) 3 and 4 were prepared by a coprecipitation method and heat treated samples were subsequently prepared. Their bulk structure was investigated by X-ray diffraction and surface area techniques. X-ray diffraction analysis showed that the layered double hydroxide phase remained unchanged upon heating up to 250°C for 5 h in an oven at atmospheric pressure. However, new phases, namely spinel-like and ZnO phases appeared when the samples were heated at 350°C and above for the same duration. The specific surface areas decreased with increasing temperature (between 450850° C) for both R values but no trend was observed for temperatures between 250-350°C. Average pore diameter was found to be optimum at 550°C and 450°C for R = 3 and 4, respectively. Universiti Putra Malaysia Press 1996 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/3225/1/Hidroksida_Berlapis_Ganda_ZnCrCI_Kesan_Haba.pdf Hussien, Mohd Zobir and Zainal, Zulkarnain and Ibrahim, Ramli and Hii, Hiong Swee (1996) Hidroksida Berlapis Ganda ZnCrCI: Kesan Haba Terhadap Luas Perm.ukaan dan Keliangan. Pertanika Journal of Science & Technology, 4 (1). pp. 31-39. ISSN 0128-7680 English
spellingShingle Hussien, Mohd Zobir
Zainal, Zulkarnain
Ibrahim, Ramli
Hii, Hiong Swee
Hidroksida Berlapis Ganda ZnCrCI: Kesan Haba Terhadap Luas Perm.ukaan dan Keliangan
title Hidroksida Berlapis Ganda ZnCrCI: Kesan Haba Terhadap Luas Perm.ukaan dan Keliangan
title_full Hidroksida Berlapis Ganda ZnCrCI: Kesan Haba Terhadap Luas Perm.ukaan dan Keliangan
title_fullStr Hidroksida Berlapis Ganda ZnCrCI: Kesan Haba Terhadap Luas Perm.ukaan dan Keliangan
title_full_unstemmed Hidroksida Berlapis Ganda ZnCrCI: Kesan Haba Terhadap Luas Perm.ukaan dan Keliangan
title_short Hidroksida Berlapis Ganda ZnCrCI: Kesan Haba Terhadap Luas Perm.ukaan dan Keliangan
title_sort hidroksida berlapis ganda zncrci: kesan haba terhadap luas perm.ukaan dan keliangan
url http://psasir.upm.edu.my/id/eprint/3225/
http://psasir.upm.edu.my/id/eprint/3225/1/Hidroksida_Berlapis_Ganda_ZnCrCI_Kesan_Haba.pdf