Analysis of chicken fat as adulterant in butter using Fourier transform infrared spectroscopy and chemometrics

Butter may be adulterated with cheaper animal fats, such as chicken fat (CF). Thus, the detection and quantification of butter adulteration with CF was monitored using Fourier transform infrared (FTIR) spectroscopy, combined with chemometric of partial least square (PLS) at the frequency regions of...

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Main Authors: Ahmad Fadzlillah, Nurrulhidayah, Abdul Rohman, Ismail, Amin, Mustafa, Shuhaimi, Khatib, Alfi
Format: Article
Language:English
Published: Consejo Superior de Investigaciones Cientificas 2013
Online Access:http://psasir.upm.edu.my/id/eprint/30472/
http://psasir.upm.edu.my/id/eprint/30472/1/Analysis%20of%20chicken%20fat%20as%20adulterant%20in%20butter%20using%20Fourier%20transform%20infrared%20spectroscopy%20and%20chemometrics.pdf
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author Ahmad Fadzlillah, Nurrulhidayah
Abdul Rohman,
Ismail, Amin
Mustafa, Shuhaimi
Khatib, Alfi
author_facet Ahmad Fadzlillah, Nurrulhidayah
Abdul Rohman,
Ismail, Amin
Mustafa, Shuhaimi
Khatib, Alfi
author_sort Ahmad Fadzlillah, Nurrulhidayah
building UPM Institutional Repository
collection Online Access
description Butter may be adulterated with cheaper animal fats, such as chicken fat (CF). Thus, the detection and quantification of butter adulteration with CF was monitored using Fourier transform infrared (FTIR) spectroscopy, combined with chemometric of partial least square (PLS) at the frequency regions of 1200-1000cm–1. FTIR measurements were made on pure butter and that adulterated with varying concentrations of CF (0-100% w/w in butter). PLS calibration exhibits a good relationship between actual and FTIR predicted values of CF with a coefficient of determination (R2) of 0.981. The root means standard error of calibration (RMSEC) and during cross validation (RMSECV) obtained using six principal components (PCs) are 2.08 and 4.33% v/v, respectively.
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language English
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publishDate 2013
publisher Consejo Superior de Investigaciones Cientificas
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spelling upm-304722016-02-15T05:17:21Z http://psasir.upm.edu.my/id/eprint/30472/ Analysis of chicken fat as adulterant in butter using Fourier transform infrared spectroscopy and chemometrics Ahmad Fadzlillah, Nurrulhidayah Abdul Rohman, Ismail, Amin Mustafa, Shuhaimi Khatib, Alfi Butter may be adulterated with cheaper animal fats, such as chicken fat (CF). Thus, the detection and quantification of butter adulteration with CF was monitored using Fourier transform infrared (FTIR) spectroscopy, combined with chemometric of partial least square (PLS) at the frequency regions of 1200-1000cm–1. FTIR measurements were made on pure butter and that adulterated with varying concentrations of CF (0-100% w/w in butter). PLS calibration exhibits a good relationship between actual and FTIR predicted values of CF with a coefficient of determination (R2) of 0.981. The root means standard error of calibration (RMSEC) and during cross validation (RMSECV) obtained using six principal components (PCs) are 2.08 and 4.33% v/v, respectively. Consejo Superior de Investigaciones Cientificas 2013 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/30472/1/Analysis%20of%20chicken%20fat%20as%20adulterant%20in%20butter%20using%20Fourier%20transform%20infrared%20spectroscopy%20and%20chemometrics.pdf Ahmad Fadzlillah, Nurrulhidayah and Abdul Rohman, and Ismail, Amin and Mustafa, Shuhaimi and Khatib, Alfi (2013) Analysis of chicken fat as adulterant in butter using Fourier transform infrared spectroscopy and chemometrics. Grasas y Aceites, 64 (4). pp. 349-355. ISSN 0017-3495; ESSN: 1988-4214 http://dx.doi.org/10.3989/gya.072812 10.3989/gya.072812
spellingShingle Ahmad Fadzlillah, Nurrulhidayah
Abdul Rohman,
Ismail, Amin
Mustafa, Shuhaimi
Khatib, Alfi
Analysis of chicken fat as adulterant in butter using Fourier transform infrared spectroscopy and chemometrics
title Analysis of chicken fat as adulterant in butter using Fourier transform infrared spectroscopy and chemometrics
title_full Analysis of chicken fat as adulterant in butter using Fourier transform infrared spectroscopy and chemometrics
title_fullStr Analysis of chicken fat as adulterant in butter using Fourier transform infrared spectroscopy and chemometrics
title_full_unstemmed Analysis of chicken fat as adulterant in butter using Fourier transform infrared spectroscopy and chemometrics
title_short Analysis of chicken fat as adulterant in butter using Fourier transform infrared spectroscopy and chemometrics
title_sort analysis of chicken fat as adulterant in butter using fourier transform infrared spectroscopy and chemometrics
url http://psasir.upm.edu.my/id/eprint/30472/
http://psasir.upm.edu.my/id/eprint/30472/
http://psasir.upm.edu.my/id/eprint/30472/
http://psasir.upm.edu.my/id/eprint/30472/1/Analysis%20of%20chicken%20fat%20as%20adulterant%20in%20butter%20using%20Fourier%20transform%20infrared%20spectroscopy%20and%20chemometrics.pdf