Layered double hydroxide as carrier of herbicide, 2-methyl-4-chlorophenoxy acetic acid : physicochemical characterization and controlled release properties

A new organic-inorganic hybrid nanocomposite Zn-Al-MCPA layered double hydroxide was prepared by intercalation of 2-methyl-4-chlorophenoxy acetic acid (MCPA), into Zn-Al-layered double hydroxide (ZAL) at various concentration of MCPA ranging from 0.1 to 0.7. The pH of the formulation was kept consta...

Full description

Bibliographic Details
Main Authors: Sheikh Mohd Ghazali, Sheikh Ahmad Izaddin, Hussein, Mohd Zobir, Sarijo, Siti Halimah
Format: Article
Language:English
English
Published: American Scientific Publishers 2013
Online Access:http://psasir.upm.edu.my/id/eprint/30046/
http://psasir.upm.edu.my/id/eprint/30046/1/Layered%20double%20hydroxide%20as%20carrier%20of%20herbicide.pdf
_version_ 1848846567776190464
author Sheikh Mohd Ghazali, Sheikh Ahmad Izaddin
Hussein, Mohd Zobir
Sarijo, Siti Halimah
author_facet Sheikh Mohd Ghazali, Sheikh Ahmad Izaddin
Hussein, Mohd Zobir
Sarijo, Siti Halimah
author_sort Sheikh Mohd Ghazali, Sheikh Ahmad Izaddin
building UPM Institutional Repository
collection Online Access
description A new organic-inorganic hybrid nanocomposite Zn-Al-MCPA layered double hydroxide was prepared by intercalation of 2-methyl-4-chlorophenoxy acetic acid (MCPA), into Zn-Al-layered double hydroxide (ZAL) at various concentration of MCPA ranging from 0.1 to 0.7. The pH of the formulation was kept constant at 7.5. Well-ordered hybrid nanocomposite was obtained with 0.4 M MCPA with an expansion of basal spacing from 8.9 Å in the ZAL s resemblance peaks of to 19.7 Å in the resulting nanocomposite. The FTIR spectra of the nanocomposite shows resemblance peaks of the MCPA and Zn-Al-layered double hydroxide indicates the inclusion of MCPA into the layered double hydroxide with loading of MCPA found to be 45% (w/w). The release of MCPA into various aqueous solution was found to be dependent on the anion in the aqueous solution, in the order of phosphate > sulphate > nitrate with the percentage release of 80%, 44% and 8%, respectively. This study shows that Zn-Al-layered double hydroxide can be used as a host carrier for herbicide, MCPA with controlled release capability.
first_indexed 2025-11-15T09:04:46Z
format Article
id upm-30046
institution Universiti Putra Malaysia
institution_category Local University
language English
English
last_indexed 2025-11-15T09:04:46Z
publishDate 2013
publisher American Scientific Publishers
recordtype eprints
repository_type Digital Repository
spelling upm-300462016-02-05T01:15:28Z http://psasir.upm.edu.my/id/eprint/30046/ Layered double hydroxide as carrier of herbicide, 2-methyl-4-chlorophenoxy acetic acid : physicochemical characterization and controlled release properties Sheikh Mohd Ghazali, Sheikh Ahmad Izaddin Hussein, Mohd Zobir Sarijo, Siti Halimah A new organic-inorganic hybrid nanocomposite Zn-Al-MCPA layered double hydroxide was prepared by intercalation of 2-methyl-4-chlorophenoxy acetic acid (MCPA), into Zn-Al-layered double hydroxide (ZAL) at various concentration of MCPA ranging from 0.1 to 0.7. The pH of the formulation was kept constant at 7.5. Well-ordered hybrid nanocomposite was obtained with 0.4 M MCPA with an expansion of basal spacing from 8.9 Å in the ZAL s resemblance peaks of to 19.7 Å in the resulting nanocomposite. The FTIR spectra of the nanocomposite shows resemblance peaks of the MCPA and Zn-Al-layered double hydroxide indicates the inclusion of MCPA into the layered double hydroxide with loading of MCPA found to be 45% (w/w). The release of MCPA into various aqueous solution was found to be dependent on the anion in the aqueous solution, in the order of phosphate > sulphate > nitrate with the percentage release of 80%, 44% and 8%, respectively. This study shows that Zn-Al-layered double hydroxide can be used as a host carrier for herbicide, MCPA with controlled release capability. American Scientific Publishers 2013 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/30046/1/Layered%20double%20hydroxide%20as%20carrier%20of%20herbicide.pdf Sheikh Mohd Ghazali, Sheikh Ahmad Izaddin and Hussein, Mohd Zobir and Sarijo, Siti Halimah (2013) Layered double hydroxide as carrier of herbicide, 2-methyl-4-chlorophenoxy acetic acid : physicochemical characterization and controlled release properties. Advanced Science Letters, 19 (11). pp. 3355-3360. ISSN 1936-6612 10.1166/asl.2013.5142 English
spellingShingle Sheikh Mohd Ghazali, Sheikh Ahmad Izaddin
Hussein, Mohd Zobir
Sarijo, Siti Halimah
Layered double hydroxide as carrier of herbicide, 2-methyl-4-chlorophenoxy acetic acid : physicochemical characterization and controlled release properties
title Layered double hydroxide as carrier of herbicide, 2-methyl-4-chlorophenoxy acetic acid : physicochemical characterization and controlled release properties
title_full Layered double hydroxide as carrier of herbicide, 2-methyl-4-chlorophenoxy acetic acid : physicochemical characterization and controlled release properties
title_fullStr Layered double hydroxide as carrier of herbicide, 2-methyl-4-chlorophenoxy acetic acid : physicochemical characterization and controlled release properties
title_full_unstemmed Layered double hydroxide as carrier of herbicide, 2-methyl-4-chlorophenoxy acetic acid : physicochemical characterization and controlled release properties
title_short Layered double hydroxide as carrier of herbicide, 2-methyl-4-chlorophenoxy acetic acid : physicochemical characterization and controlled release properties
title_sort layered double hydroxide as carrier of herbicide, 2-methyl-4-chlorophenoxy acetic acid : physicochemical characterization and controlled release properties
url http://psasir.upm.edu.my/id/eprint/30046/
http://psasir.upm.edu.my/id/eprint/30046/
http://psasir.upm.edu.my/id/eprint/30046/1/Layered%20double%20hydroxide%20as%20carrier%20of%20herbicide.pdf