Green biosynthesis and characterization of magnetic iron oxide (Fe3O4) nanoparticles using seaweed (Sargassum muticum) aqueous extract

The synthesis of nanoparticles has become a matter of great interest in recent times due to their various advantageous properties and applications in a variety of fields. The exploitation of different plant materials for the biosynthesis of nanoparticles is considered a green technology because it d...

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Main Authors: Mahdavi, Mahnaz, Namvar, Farideh, Ahmad @ Ayob, Mansor, Mohamad, Rosfarizan
Format: Article
Language:English
Published: MDPI 2013
Online Access:http://psasir.upm.edu.my/id/eprint/28034/
http://psasir.upm.edu.my/id/eprint/28034/1/Green%20Biosynthesis%20and%20Characterization%20of%20Magnetic%20Iron%20Oxide%20%28Fe3O4%29%20Nanoparticles%20Using%20Seaweed%20%28Sargassum%20muticum%29%20Aqueous%20Extract.pdf
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author Mahdavi, Mahnaz
Namvar, Farideh
Ahmad @ Ayob, Mansor
Mohamad, Rosfarizan
author_facet Mahdavi, Mahnaz
Namvar, Farideh
Ahmad @ Ayob, Mansor
Mohamad, Rosfarizan
author_sort Mahdavi, Mahnaz
building UPM Institutional Repository
collection Online Access
description The synthesis of nanoparticles has become a matter of great interest in recent times due to their various advantageous properties and applications in a variety of fields. The exploitation of different plant materials for the biosynthesis of nanoparticles is considered a green technology because it does not involve any harmful chemicals. In this study, iron oxide nanoparticles (Fe3O4-NPs) were synthesized using a rapid, single step and completely green biosynthetic method by reduction of ferric chloride solution with brown seaweed (BS, Sargassum muticum) water extract containing sulphated polysaccharides as a main factor which acts as reducing agent and efficient stabilizer. The structural and properties of the Fe3O4-NPs were investigated by X-ray diffraction, Fourier transform infrared spectroscopy, field emission scanning electron microscopy (FESEM), energy dispersive X-ray fluorescence spectrometry (EDXRF), vibrating sample magnetometry (VSM) and transmission electron microscopy. The average particle diameter as determined by TEM was found to be 18 ± 4 nm. X-ray diffraction showed that the nanoparticles are crystalline in nature, with a cubic shape. The nanoparticles synthesized through this biosynthesis method can potentially useful in various applications.
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spelling upm-280342016-03-07T07:58:29Z http://psasir.upm.edu.my/id/eprint/28034/ Green biosynthesis and characterization of magnetic iron oxide (Fe3O4) nanoparticles using seaweed (Sargassum muticum) aqueous extract Mahdavi, Mahnaz Namvar, Farideh Ahmad @ Ayob, Mansor Mohamad, Rosfarizan The synthesis of nanoparticles has become a matter of great interest in recent times due to their various advantageous properties and applications in a variety of fields. The exploitation of different plant materials for the biosynthesis of nanoparticles is considered a green technology because it does not involve any harmful chemicals. In this study, iron oxide nanoparticles (Fe3O4-NPs) were synthesized using a rapid, single step and completely green biosynthetic method by reduction of ferric chloride solution with brown seaweed (BS, Sargassum muticum) water extract containing sulphated polysaccharides as a main factor which acts as reducing agent and efficient stabilizer. The structural and properties of the Fe3O4-NPs were investigated by X-ray diffraction, Fourier transform infrared spectroscopy, field emission scanning electron microscopy (FESEM), energy dispersive X-ray fluorescence spectrometry (EDXRF), vibrating sample magnetometry (VSM) and transmission electron microscopy. The average particle diameter as determined by TEM was found to be 18 ± 4 nm. X-ray diffraction showed that the nanoparticles are crystalline in nature, with a cubic shape. The nanoparticles synthesized through this biosynthesis method can potentially useful in various applications. MDPI 2013 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/28034/1/Green%20Biosynthesis%20and%20Characterization%20of%20Magnetic%20Iron%20Oxide%20%28Fe3O4%29%20Nanoparticles%20Using%20Seaweed%20%28Sargassum%20muticum%29%20Aqueous%20Extract.pdf Mahdavi, Mahnaz and Namvar, Farideh and Ahmad @ Ayob, Mansor and Mohamad, Rosfarizan (2013) Green biosynthesis and characterization of magnetic iron oxide (Fe3O4) nanoparticles using seaweed (Sargassum muticum) aqueous extract. Molecules, 18 (5). pp. 5954-5964. ISSN 1420-3049 http://www.mdpi.com/1420-3049/18/5/5954 10.3390/molecules18055954
spellingShingle Mahdavi, Mahnaz
Namvar, Farideh
Ahmad @ Ayob, Mansor
Mohamad, Rosfarizan
Green biosynthesis and characterization of magnetic iron oxide (Fe3O4) nanoparticles using seaweed (Sargassum muticum) aqueous extract
title Green biosynthesis and characterization of magnetic iron oxide (Fe3O4) nanoparticles using seaweed (Sargassum muticum) aqueous extract
title_full Green biosynthesis and characterization of magnetic iron oxide (Fe3O4) nanoparticles using seaweed (Sargassum muticum) aqueous extract
title_fullStr Green biosynthesis and characterization of magnetic iron oxide (Fe3O4) nanoparticles using seaweed (Sargassum muticum) aqueous extract
title_full_unstemmed Green biosynthesis and characterization of magnetic iron oxide (Fe3O4) nanoparticles using seaweed (Sargassum muticum) aqueous extract
title_short Green biosynthesis and characterization of magnetic iron oxide (Fe3O4) nanoparticles using seaweed (Sargassum muticum) aqueous extract
title_sort green biosynthesis and characterization of magnetic iron oxide (fe3o4) nanoparticles using seaweed (sargassum muticum) aqueous extract
url http://psasir.upm.edu.my/id/eprint/28034/
http://psasir.upm.edu.my/id/eprint/28034/
http://psasir.upm.edu.my/id/eprint/28034/
http://psasir.upm.edu.my/id/eprint/28034/1/Green%20Biosynthesis%20and%20Characterization%20of%20Magnetic%20Iron%20Oxide%20%28Fe3O4%29%20Nanoparticles%20Using%20Seaweed%20%28Sargassum%20muticum%29%20Aqueous%20Extract.pdf