Modified electrode for electrochemical analysis.

The electrochemical sensor for As(III) were developed by using carbon nanotube/amino acid modified platinum electrode using cyclic voltammetry. Experimental conditions such as pH, supporting electrolyte and scan rate were optimized. It was observed that the modified electrode has significantly super...

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Main Authors: Yusof, Nor Azah, Daud, Nurulhaidah
Format: Patent
Published: 2009
Online Access:http://psasir.upm.edu.my/id/eprint/27669/
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author Yusof, Nor Azah
Daud, Nurulhaidah
author_facet Yusof, Nor Azah
Daud, Nurulhaidah
author_sort Yusof, Nor Azah
building UPM Institutional Repository
collection Online Access
description The electrochemical sensor for As(III) were developed by using carbon nanotube/amino acid modified platinum electrode using cyclic voltammetry. Experimental conditions such as pH, supporting electrolyte and scan rate were optimized. It was observed that the modified electrode has significantly superior analytical performance in determination as As(III) compared to the unmodified electrode. The determination of As(III) by using modified electrode was reproducible with R.S.D of 7.33%. Determination of As(III) was observed to be free interference at pH 4 acetate buffer. The electrocatalytic redox peak current of As(III) showed a linear response towards different concentration of As(III) and linear calibration cuves were obtained. The sensitivity expressed as the slope of the linear regon of the calibration curve. This method was also examined for determination of As(III) in some real samples, such as industrial waste water from wood industry and electroplating industry.
first_indexed 2025-11-15T08:54:14Z
format Patent
id upm-27669
institution Universiti Putra Malaysia
institution_category Local University
last_indexed 2025-11-15T08:54:14Z
publishDate 2009
recordtype eprints
repository_type Digital Repository
spelling upm-276692014-04-01T08:13:59Z http://psasir.upm.edu.my/id/eprint/27669/ Modified electrode for electrochemical analysis. Yusof, Nor Azah Daud, Nurulhaidah The electrochemical sensor for As(III) were developed by using carbon nanotube/amino acid modified platinum electrode using cyclic voltammetry. Experimental conditions such as pH, supporting electrolyte and scan rate were optimized. It was observed that the modified electrode has significantly superior analytical performance in determination as As(III) compared to the unmodified electrode. The determination of As(III) by using modified electrode was reproducible with R.S.D of 7.33%. Determination of As(III) was observed to be free interference at pH 4 acetate buffer. The electrocatalytic redox peak current of As(III) showed a linear response towards different concentration of As(III) and linear calibration cuves were obtained. The sensitivity expressed as the slope of the linear regon of the calibration curve. This method was also examined for determination of As(III) in some real samples, such as industrial waste water from wood industry and electroplating industry. 2009-07-07 Patent NonPeerReviewed Nor Azah Yusof (2009) Modified electrode for electrochemical analysis. UNSPECIFIED.
spellingShingle Yusof, Nor Azah
Daud, Nurulhaidah
Modified electrode for electrochemical analysis.
title Modified electrode for electrochemical analysis.
title_full Modified electrode for electrochemical analysis.
title_fullStr Modified electrode for electrochemical analysis.
title_full_unstemmed Modified electrode for electrochemical analysis.
title_short Modified electrode for electrochemical analysis.
title_sort modified electrode for electrochemical analysis.
url http://psasir.upm.edu.my/id/eprint/27669/