Microstructural changes of carbonaceous monoliths synthesized via hydrothermal method

Carbonaceous monoliths were successfully synthesized via a facile hydrothermal processing route using phenol as a carbon precursor. The x-ray diffraction (XRD) patterns revealed distinguishable (002) and (100) planes of graphite at approximately 2θ = 23° and 44°, respectively. The fourier transform...

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Main Authors: Lim, Hong Ngee, Kassim, Anuar, Lim, Su Pei, Nizar, N. S. Rastam, Huang, Nay Ming
Format: Article
Language:English
Published: Sociedad Chilena de Quimica 2011
Online Access:http://psasir.upm.edu.my/id/eprint/25253/
http://psasir.upm.edu.my/id/eprint/25253/1/Microstructural%20changes%20of%20carbonaceous%20monoliths%20synthesized%20via%20hydrothermal%20method.pdf
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author Lim, Hong Ngee
Kassim, Anuar
Lim, Su Pei
Nizar, N. S. Rastam
Huang, Nay Ming
author_facet Lim, Hong Ngee
Kassim, Anuar
Lim, Su Pei
Nizar, N. S. Rastam
Huang, Nay Ming
author_sort Lim, Hong Ngee
building UPM Institutional Repository
collection Online Access
description Carbonaceous monoliths were successfully synthesized via a facile hydrothermal processing route using phenol as a carbon precursor. The x-ray diffraction (XRD) patterns revealed distinguishable (002) and (100) planes of graphite at approximately 2θ = 23° and 44°, respectively. The fourier transform infrared (FTIR) spectroscopy corresponded to the chemical bonds of graphite, which were C=C and C-H. The carbonaceous monoliths exhibited interesting morphological changes as a result of varying the type of polymer which acted as a structure directing agent, mass of polymer, mass of phenol and hydrothermal temperature before and after calcination.
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institution Universiti Putra Malaysia
institution_category Local University
language English
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publishDate 2011
publisher Sociedad Chilena de Quimica
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spelling upm-252532016-03-16T03:42:27Z http://psasir.upm.edu.my/id/eprint/25253/ Microstructural changes of carbonaceous monoliths synthesized via hydrothermal method Lim, Hong Ngee Kassim, Anuar Lim, Su Pei Nizar, N. S. Rastam Huang, Nay Ming Carbonaceous monoliths were successfully synthesized via a facile hydrothermal processing route using phenol as a carbon precursor. The x-ray diffraction (XRD) patterns revealed distinguishable (002) and (100) planes of graphite at approximately 2θ = 23° and 44°, respectively. The fourier transform infrared (FTIR) spectroscopy corresponded to the chemical bonds of graphite, which were C=C and C-H. The carbonaceous monoliths exhibited interesting morphological changes as a result of varying the type of polymer which acted as a structure directing agent, mass of polymer, mass of phenol and hydrothermal temperature before and after calcination. Sociedad Chilena de Quimica 2011 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/25253/1/Microstructural%20changes%20of%20carbonaceous%20monoliths%20synthesized%20via%20hydrothermal%20method.pdf Lim, Hong Ngee and Kassim, Anuar and Lim, Su Pei and Nizar, N. S. Rastam and Huang, Nay Ming (2011) Microstructural changes of carbonaceous monoliths synthesized via hydrothermal method. Journal of the Chilean Chemical Society, 56 (1). pp. 584-586. ISSN 0717-9324; ESSN: 0717-9707 http://www.scielo.cl/scielo.php?script=sci_abstract&pid=S0717-97072011000100013&lng=en&nrm=iso&tlng=en 10.4067/S0717-97072011000100013
spellingShingle Lim, Hong Ngee
Kassim, Anuar
Lim, Su Pei
Nizar, N. S. Rastam
Huang, Nay Ming
Microstructural changes of carbonaceous monoliths synthesized via hydrothermal method
title Microstructural changes of carbonaceous monoliths synthesized via hydrothermal method
title_full Microstructural changes of carbonaceous monoliths synthesized via hydrothermal method
title_fullStr Microstructural changes of carbonaceous monoliths synthesized via hydrothermal method
title_full_unstemmed Microstructural changes of carbonaceous monoliths synthesized via hydrothermal method
title_short Microstructural changes of carbonaceous monoliths synthesized via hydrothermal method
title_sort microstructural changes of carbonaceous monoliths synthesized via hydrothermal method
url http://psasir.upm.edu.my/id/eprint/25253/
http://psasir.upm.edu.my/id/eprint/25253/
http://psasir.upm.edu.my/id/eprint/25253/
http://psasir.upm.edu.my/id/eprint/25253/1/Microstructural%20changes%20of%20carbonaceous%20monoliths%20synthesized%20via%20hydrothermal%20method.pdf