Electrochemical oxidation of paracetamol mediated by nanoparticles bismuth oxide modified glassy carbon electrode.

Nanoparticles of bismuth oxide (Bi2O3) have been mechanically attached on the surface of a glassy carbon electrode. Electrochemical performance of nanoparticles of Bi2O3/GC modified electrode shows stable response with enhanced selectivity and sensitivity. Voltammetric determination of the oxidatio...

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Main Authors: Mohammed Zidan, Tan, Wee Tee, Abdullah, Abdul Halim, Zainal, Zulkarnain, Goh, Joo Kheng
Format: Article
Language:English
English
Published: Electrochemical Science Group 2011
Online Access:http://psasir.upm.edu.my/id/eprint/24776/
http://psasir.upm.edu.my/id/eprint/24776/1/Electrochemical%20oxidation%20of%20paracetamol%20mediated%20by%20nanoparticles%20bismuth%20oxide%20modified%20glassy%20carbon%20electrode.pdf
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author Mohammed Zidan,
Tan, Wee Tee
Abdullah, Abdul Halim
Zainal, Zulkarnain
Goh, Joo Kheng
author_facet Mohammed Zidan,
Tan, Wee Tee
Abdullah, Abdul Halim
Zainal, Zulkarnain
Goh, Joo Kheng
author_sort Mohammed Zidan,
building UPM Institutional Repository
collection Online Access
description Nanoparticles of bismuth oxide (Bi2O3) have been mechanically attached on the surface of a glassy carbon electrode. Electrochemical performance of nanoparticles of Bi2O3/GC modified electrode shows stable response with enhanced selectivity and sensitivity. Voltammetric determination of the oxidation of paracetamol in 0.1 M KH2PO4 electrolyte solution by solid phase voltammetry has shown electrocatalyzing effect. Observation revealed a high peak toward the origin of paracetamol oxidation current, which showed 2.0 times increment as compared to bare GC electrode. The sensitivity under conditions of cyclic voltammetry is significantly dependent on pH and temperature. The variation of scan rate study shows that the system undergoes diffusion-controlled process. Calibration plot reveals linearity from the range 5.0 × 10-7 to 1.5 × 10-3M with a correlation coefficient of 0.994. The detection limit was estimated to be 2.0 × 10-7 M. Based on interference studies, most amino acids have negligibly affected the current response of paracetamol. Practically, nanoparticles of bismuth oxide (Bi2O3) modified GC electrode could be used for the determination of parecetamol in blood plasma samples.
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spelling upm-247762015-10-16T07:30:38Z http://psasir.upm.edu.my/id/eprint/24776/ Electrochemical oxidation of paracetamol mediated by nanoparticles bismuth oxide modified glassy carbon electrode. Mohammed Zidan, Tan, Wee Tee Abdullah, Abdul Halim Zainal, Zulkarnain Goh, Joo Kheng Nanoparticles of bismuth oxide (Bi2O3) have been mechanically attached on the surface of a glassy carbon electrode. Electrochemical performance of nanoparticles of Bi2O3/GC modified electrode shows stable response with enhanced selectivity and sensitivity. Voltammetric determination of the oxidation of paracetamol in 0.1 M KH2PO4 electrolyte solution by solid phase voltammetry has shown electrocatalyzing effect. Observation revealed a high peak toward the origin of paracetamol oxidation current, which showed 2.0 times increment as compared to bare GC electrode. The sensitivity under conditions of cyclic voltammetry is significantly dependent on pH and temperature. The variation of scan rate study shows that the system undergoes diffusion-controlled process. Calibration plot reveals linearity from the range 5.0 × 10-7 to 1.5 × 10-3M with a correlation coefficient of 0.994. The detection limit was estimated to be 2.0 × 10-7 M. Based on interference studies, most amino acids have negligibly affected the current response of paracetamol. Practically, nanoparticles of bismuth oxide (Bi2O3) modified GC electrode could be used for the determination of parecetamol in blood plasma samples. Electrochemical Science Group 2011-02 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/24776/1/Electrochemical%20oxidation%20of%20paracetamol%20mediated%20by%20nanoparticles%20bismuth%20oxide%20modified%20glassy%20carbon%20electrode.pdf Mohammed Zidan, and Tan, Wee Tee and Abdullah, Abdul Halim and Zainal, Zulkarnain and Goh, Joo Kheng (2011) Electrochemical oxidation of paracetamol mediated by nanoparticles bismuth oxide modified glassy carbon electrode. International Journal of Electrochemical Science, 6 (2). pp. 279-288. ISSN 1452-3981 http://www.electrochemsci.org/ English
spellingShingle Mohammed Zidan,
Tan, Wee Tee
Abdullah, Abdul Halim
Zainal, Zulkarnain
Goh, Joo Kheng
Electrochemical oxidation of paracetamol mediated by nanoparticles bismuth oxide modified glassy carbon electrode.
title Electrochemical oxidation of paracetamol mediated by nanoparticles bismuth oxide modified glassy carbon electrode.
title_full Electrochemical oxidation of paracetamol mediated by nanoparticles bismuth oxide modified glassy carbon electrode.
title_fullStr Electrochemical oxidation of paracetamol mediated by nanoparticles bismuth oxide modified glassy carbon electrode.
title_full_unstemmed Electrochemical oxidation of paracetamol mediated by nanoparticles bismuth oxide modified glassy carbon electrode.
title_short Electrochemical oxidation of paracetamol mediated by nanoparticles bismuth oxide modified glassy carbon electrode.
title_sort electrochemical oxidation of paracetamol mediated by nanoparticles bismuth oxide modified glassy carbon electrode.
url http://psasir.upm.edu.my/id/eprint/24776/
http://psasir.upm.edu.my/id/eprint/24776/
http://psasir.upm.edu.my/id/eprint/24776/1/Electrochemical%20oxidation%20of%20paracetamol%20mediated%20by%20nanoparticles%20bismuth%20oxide%20modified%20glassy%20carbon%20electrode.pdf