Analysis of lard in cream cosmetics formulations using FT-IR spectroscopy and chemometrics

Typically, cream preparation is composed from complex mixtures; therefore its analysis is rather difficult. The presence of lard (LD) in any personal care products is prohibited to be used by the Followers of Islam. In this study, Fourier transform infrared (FT-IR) spectroscopy combined with partial...

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Main Authors: Che Man, Yaakob, Abdul Rohman
Format: Article
Language:English
Published: IDOSI Publications 2011
Online Access:http://psasir.upm.edu.my/id/eprint/24163/
http://psasir.upm.edu.my/id/eprint/24163/1/Analysis%20of%20lard%20in%20cream%20cosmetics%20formulations%20using%20FT.pdf
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author Che Man, Yaakob
Abdul Rohman,
author_facet Che Man, Yaakob
Abdul Rohman,
author_sort Che Man, Yaakob
building UPM Institutional Repository
collection Online Access
description Typically, cream preparation is composed from complex mixtures; therefore its analysis is rather difficult. The presence of lard (LD) in any personal care products is prohibited to be used by the Followers of Islam. In this study, Fourier transform infrared (FT-IR) spectroscopy combined with partial least square (PLS) and discriminant analysis (DA) was developed for the quantification and classification of LD in cream formulations. PLS and DA were performed at two frequency regions of 3,020 – 2,995 and 1,200 – 1,000 cm. 1 The PLS calibration model obtained for the relationship between actual (x-axis) and FT-IR predicted (y-axis) values of LD was y = 0.997x + 0.065, with coefficient of determination (R ) and root mean square error of 2 calibration (RMSEC) of 0.997 and 0.808% (v/v), respectively. In addition, DA can successfully classify creams containing LD in its formulation using 9 principal components. FT-IR can be used as a potential analytical technique to quantify and to classify LD in cream preparations with total analysis time at about 3 min/one sample measurement.
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spelling upm-241632016-02-10T05:16:50Z http://psasir.upm.edu.my/id/eprint/24163/ Analysis of lard in cream cosmetics formulations using FT-IR spectroscopy and chemometrics Che Man, Yaakob Abdul Rohman, Typically, cream preparation is composed from complex mixtures; therefore its analysis is rather difficult. The presence of lard (LD) in any personal care products is prohibited to be used by the Followers of Islam. In this study, Fourier transform infrared (FT-IR) spectroscopy combined with partial least square (PLS) and discriminant analysis (DA) was developed for the quantification and classification of LD in cream formulations. PLS and DA were performed at two frequency regions of 3,020 – 2,995 and 1,200 – 1,000 cm. 1 The PLS calibration model obtained for the relationship between actual (x-axis) and FT-IR predicted (y-axis) values of LD was y = 0.997x + 0.065, with coefficient of determination (R ) and root mean square error of 2 calibration (RMSEC) of 0.997 and 0.808% (v/v), respectively. In addition, DA can successfully classify creams containing LD in its formulation using 9 principal components. FT-IR can be used as a potential analytical technique to quantify and to classify LD in cream preparations with total analysis time at about 3 min/one sample measurement. IDOSI Publications 2011 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/24163/1/Analysis%20of%20lard%20in%20cream%20cosmetics%20formulations%20using%20FT.pdf Che Man, Yaakob and Abdul Rohman, (2011) Analysis of lard in cream cosmetics formulations using FT-IR spectroscopy and chemometrics. Middle-East Journal of Scientific Research, 7 (5). pp. 726-732. ISSN 1990-9233 http://www.idosi.org/mejsr/mejsr7%285%2911/16.pdf
spellingShingle Che Man, Yaakob
Abdul Rohman,
Analysis of lard in cream cosmetics formulations using FT-IR spectroscopy and chemometrics
title Analysis of lard in cream cosmetics formulations using FT-IR spectroscopy and chemometrics
title_full Analysis of lard in cream cosmetics formulations using FT-IR spectroscopy and chemometrics
title_fullStr Analysis of lard in cream cosmetics formulations using FT-IR spectroscopy and chemometrics
title_full_unstemmed Analysis of lard in cream cosmetics formulations using FT-IR spectroscopy and chemometrics
title_short Analysis of lard in cream cosmetics formulations using FT-IR spectroscopy and chemometrics
title_sort analysis of lard in cream cosmetics formulations using ft-ir spectroscopy and chemometrics
url http://psasir.upm.edu.my/id/eprint/24163/
http://psasir.upm.edu.my/id/eprint/24163/
http://psasir.upm.edu.my/id/eprint/24163/1/Analysis%20of%20lard%20in%20cream%20cosmetics%20formulations%20using%20FT.pdf