Detection of animal fat contaminations in sunflower oil by differential scanning calorimetry.

In this study, the use of differential scanning calorimetric heating thermograms was investigated to detect the presence of lard, beef tallow, and chicken fat as contaminants in sunflower oil. Sunflower oil samples spiked separately with lard, beef tallow, and chicken fat in levels ranging from 1 to...

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Main Authors: Mohammed Nazrim Marikkar, Jalaldeen, Mat Hashim, Dzulkifly, Mohd Zaki, Nor Nadiha, Che Man, Yaakob
Format: Article
Language:English
English
Published: Taylor & Francis 2012
Online Access:http://psasir.upm.edu.my/id/eprint/24097/
http://psasir.upm.edu.my/id/eprint/24097/1/Detection%20of%20animal%20fat%20contaminations%20in%20sunflower%20oil%20by%20differential%20scanning%20calorimetry.pdf
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author Mohammed Nazrim Marikkar, Jalaldeen
Mat Hashim, Dzulkifly
Mohd Zaki, Nor Nadiha
Che Man, Yaakob
author_facet Mohammed Nazrim Marikkar, Jalaldeen
Mat Hashim, Dzulkifly
Mohd Zaki, Nor Nadiha
Che Man, Yaakob
author_sort Mohammed Nazrim Marikkar, Jalaldeen
building UPM Institutional Repository
collection Online Access
description In this study, the use of differential scanning calorimetric heating thermograms was investigated to detect the presence of lard, beef tallow, and chicken fat as contaminants in sunflower oil. Sunflower oil samples spiked separately with lard, beef tallow, and chicken fat in levels ranging from 1 to 20% (w/w) were analyzed using high performance liquid chromatography to get triacyl-glycerol profiles and differential scanning calorimetric to obtain their heating profiles. The results showed that below 20% (w/w) level of contamination, both lard and beef tallow in sunflower oil can be detected using characteristic contaminant peaks appearing in the higher temperature region (0-50°C) of differential scanning calorimetric curve. However, chicken fat contamination in sunflower oil did not show any characteristic peaks in this region, but caused changes only in the exiting thermal transitions in the low temperature region of the differential scanning calorimetric curve. Based on the characteristic differences in the peak size, shape, and position, it was also possible to make a distinction between lard and beef tallow contaminations in sunflower oil.
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publishDate 2012
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spelling upm-240972015-10-09T07:49:25Z http://psasir.upm.edu.my/id/eprint/24097/ Detection of animal fat contaminations in sunflower oil by differential scanning calorimetry. Mohammed Nazrim Marikkar, Jalaldeen Mat Hashim, Dzulkifly Mohd Zaki, Nor Nadiha Che Man, Yaakob In this study, the use of differential scanning calorimetric heating thermograms was investigated to detect the presence of lard, beef tallow, and chicken fat as contaminants in sunflower oil. Sunflower oil samples spiked separately with lard, beef tallow, and chicken fat in levels ranging from 1 to 20% (w/w) were analyzed using high performance liquid chromatography to get triacyl-glycerol profiles and differential scanning calorimetric to obtain their heating profiles. The results showed that below 20% (w/w) level of contamination, both lard and beef tallow in sunflower oil can be detected using characteristic contaminant peaks appearing in the higher temperature region (0-50°C) of differential scanning calorimetric curve. However, chicken fat contamination in sunflower oil did not show any characteristic peaks in this region, but caused changes only in the exiting thermal transitions in the low temperature region of the differential scanning calorimetric curve. Based on the characteristic differences in the peak size, shape, and position, it was also possible to make a distinction between lard and beef tallow contaminations in sunflower oil. Taylor & Francis 2012 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/24097/1/Detection%20of%20animal%20fat%20contaminations%20in%20sunflower%20oil%20by%20differential%20scanning%20calorimetry.pdf Mohammed Nazrim Marikkar, Jalaldeen and Mat Hashim, Dzulkifly and Mohd Zaki, Nor Nadiha and Che Man, Yaakob (2012) Detection of animal fat contaminations in sunflower oil by differential scanning calorimetry. International Journal of Food Properties, 15 (3). pp. 683-690. ISSN 1094-2912; ESSN: 1532-2386 10.1080/10942912.2010.498544 English
spellingShingle Mohammed Nazrim Marikkar, Jalaldeen
Mat Hashim, Dzulkifly
Mohd Zaki, Nor Nadiha
Che Man, Yaakob
Detection of animal fat contaminations in sunflower oil by differential scanning calorimetry.
title Detection of animal fat contaminations in sunflower oil by differential scanning calorimetry.
title_full Detection of animal fat contaminations in sunflower oil by differential scanning calorimetry.
title_fullStr Detection of animal fat contaminations in sunflower oil by differential scanning calorimetry.
title_full_unstemmed Detection of animal fat contaminations in sunflower oil by differential scanning calorimetry.
title_short Detection of animal fat contaminations in sunflower oil by differential scanning calorimetry.
title_sort detection of animal fat contaminations in sunflower oil by differential scanning calorimetry.
url http://psasir.upm.edu.my/id/eprint/24097/
http://psasir.upm.edu.my/id/eprint/24097/
http://psasir.upm.edu.my/id/eprint/24097/1/Detection%20of%20animal%20fat%20contaminations%20in%20sunflower%20oil%20by%20differential%20scanning%20calorimetry.pdf