Analysis of pork adulteration in beef meatball using Fourier transform infrared (FTIR) spectroscopy.

Meatball is one of the favorite foods in Indonesia. The adulteration of pork in beef meatball is frequently occurring. This study was aimed to develop a fast and non destructive technique for the detection and quantification of pork in beef meatball using Fourier transform infrared (FTIR) spectrosco...

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Main Authors: Abdul Rohman, Sismindari, Che Man, Yaakob, Erwanto, Yuny
Format: Article
Language:English
Published: Elsevier 2011
Online Access:http://psasir.upm.edu.my/id/eprint/24065/
http://psasir.upm.edu.my/id/eprint/24065/1/Analysis%20of%20pork%20adulteration%20in%20beef%20meatball%20using%20Fourier%20transform%20infrared.pdf
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author Abdul Rohman,
Sismindari,
Che Man, Yaakob
Erwanto, Yuny
author_facet Abdul Rohman,
Sismindari,
Che Man, Yaakob
Erwanto, Yuny
author_sort Abdul Rohman,
building UPM Institutional Repository
collection Online Access
description Meatball is one of the favorite foods in Indonesia. The adulteration of pork in beef meatball is frequently occurring. This study was aimed to develop a fast and non destructive technique for the detection and quantification of pork in beef meatball using Fourier transform infrared (FTIR) spectroscopy and partial least square (PLS) calibration. The spectral bands associated with pork fat (PF), beef fat (BF), and their mixtures in meatball formulation were scanned, interpreted, and identified by relating them to those spectroscopically representative to pure PF and BF. For quantitative analysis, PLS regression was used to develop a calibration model at the selected fingerprint regions of 1200–1000 cm−1. The equation obtained for the relationship between actual PF value and FTIR predicted values in PLS calibration model was y = 0.999x + 0.004, with coefficient of determination (R2) and root mean square error of calibration are 0.999 and 0.442, respectively. The PLS calibration model was subsequently used for the prediction of independent samples using laboratory made meatball samples containing the mixtures of BF and PF. Using 4 principal components, root mean square error of prediction is 0.742. The results showed that FTIR spectroscopy can be used for the detection and quantification of pork in beef meatball formulation for Halal verification purposes.
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spelling upm-240652016-02-10T02:49:22Z http://psasir.upm.edu.my/id/eprint/24065/ Analysis of pork adulteration in beef meatball using Fourier transform infrared (FTIR) spectroscopy. Abdul Rohman, Sismindari, Che Man, Yaakob Erwanto, Yuny Meatball is one of the favorite foods in Indonesia. The adulteration of pork in beef meatball is frequently occurring. This study was aimed to develop a fast and non destructive technique for the detection and quantification of pork in beef meatball using Fourier transform infrared (FTIR) spectroscopy and partial least square (PLS) calibration. The spectral bands associated with pork fat (PF), beef fat (BF), and their mixtures in meatball formulation were scanned, interpreted, and identified by relating them to those spectroscopically representative to pure PF and BF. For quantitative analysis, PLS regression was used to develop a calibration model at the selected fingerprint regions of 1200–1000 cm−1. The equation obtained for the relationship between actual PF value and FTIR predicted values in PLS calibration model was y = 0.999x + 0.004, with coefficient of determination (R2) and root mean square error of calibration are 0.999 and 0.442, respectively. The PLS calibration model was subsequently used for the prediction of independent samples using laboratory made meatball samples containing the mixtures of BF and PF. Using 4 principal components, root mean square error of prediction is 0.742. The results showed that FTIR spectroscopy can be used for the detection and quantification of pork in beef meatball formulation for Halal verification purposes. Elsevier 2011 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/24065/1/Analysis%20of%20pork%20adulteration%20in%20beef%20meatball%20using%20Fourier%20transform%20infrared.pdf Abdul Rohman, and Sismindari, and Che Man, Yaakob and Erwanto, Yuny (2011) Analysis of pork adulteration in beef meatball using Fourier transform infrared (FTIR) spectroscopy. Meat Science, 88 (1). pp. 91-95. ISSN 0309-1740 http://dx.doi.org/10.1016/j.meatsci.2010.12.007 10.1016/j.meatsci.2010.12.007
spellingShingle Abdul Rohman,
Sismindari,
Che Man, Yaakob
Erwanto, Yuny
Analysis of pork adulteration in beef meatball using Fourier transform infrared (FTIR) spectroscopy.
title Analysis of pork adulteration in beef meatball using Fourier transform infrared (FTIR) spectroscopy.
title_full Analysis of pork adulteration in beef meatball using Fourier transform infrared (FTIR) spectroscopy.
title_fullStr Analysis of pork adulteration in beef meatball using Fourier transform infrared (FTIR) spectroscopy.
title_full_unstemmed Analysis of pork adulteration in beef meatball using Fourier transform infrared (FTIR) spectroscopy.
title_short Analysis of pork adulteration in beef meatball using Fourier transform infrared (FTIR) spectroscopy.
title_sort analysis of pork adulteration in beef meatball using fourier transform infrared (ftir) spectroscopy.
url http://psasir.upm.edu.my/id/eprint/24065/
http://psasir.upm.edu.my/id/eprint/24065/
http://psasir.upm.edu.my/id/eprint/24065/
http://psasir.upm.edu.my/id/eprint/24065/1/Analysis%20of%20pork%20adulteration%20in%20beef%20meatball%20using%20Fourier%20transform%20infrared.pdf