Physicochemical characterization of pulp and nanofibers from kenaf stem

The aim of this study was to isolate cellulose nanofibers from kenaf (Hibiscus cannabinus) stem using chemo-mechanical treatments. The fiber purification method included pulping and bleaching processes whereas the mechanical treatments employed to isolate kenaf nanofibers were grinding and high pres...

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Main Authors: Jonoobi, Mehdi, Harun, Jalaluddin, Md. Tahir, Paridah, Alireza, Shakeri, Osman Al-Edrus, Syeed Saifulazry, Makinejad, Majid Davoodi
Format: Article
Language:English
Published: Elsevier 2011
Online Access:http://psasir.upm.edu.my/id/eprint/23889/
http://psasir.upm.edu.my/id/eprint/23889/1/Physicochemical%20characterization%20of%20pulp%20and%20nanofibers%20from%20kenaf%20stem.pdf
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author Jonoobi, Mehdi
Harun, Jalaluddin
Md. Tahir, Paridah
Alireza, Shakeri
Osman Al-Edrus, Syeed Saifulazry
Makinejad, Majid Davoodi
author_facet Jonoobi, Mehdi
Harun, Jalaluddin
Md. Tahir, Paridah
Alireza, Shakeri
Osman Al-Edrus, Syeed Saifulazry
Makinejad, Majid Davoodi
author_sort Jonoobi, Mehdi
building UPM Institutional Repository
collection Online Access
description The aim of this study was to isolate cellulose nanofibers from kenaf (Hibiscus cannabinus) stem using chemo-mechanical treatments. The fiber purification method included pulping and bleaching processes whereas the mechanical treatments employed to isolate kenaf nanofibers were grinding and high pressure homogenizing. Kenaf nanofibers were found to have diameters in the range of 15-80 nm while most nanofibers have diameters within the range 15-25 nm. Fourier transform infrared spectroscopy (FTIR) showed that the chemical treatments removed lignin and most of the hemicelluloses from the fibers. The thermal characteristics of the fibers were analyzed using the technique of thermogravimetric analysis (TGA) which demonstrated that these characteristics were enhanced noticeably both for the bleached pulp and nanofibers. On the other hand, the X-ray analysis indicated that both chemical and mechanical treatments can improve the crystallinity of fibers.
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publisher Elsevier
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spelling upm-238892016-03-01T07:15:04Z http://psasir.upm.edu.my/id/eprint/23889/ Physicochemical characterization of pulp and nanofibers from kenaf stem Jonoobi, Mehdi Harun, Jalaluddin Md. Tahir, Paridah Alireza, Shakeri Osman Al-Edrus, Syeed Saifulazry Makinejad, Majid Davoodi The aim of this study was to isolate cellulose nanofibers from kenaf (Hibiscus cannabinus) stem using chemo-mechanical treatments. The fiber purification method included pulping and bleaching processes whereas the mechanical treatments employed to isolate kenaf nanofibers were grinding and high pressure homogenizing. Kenaf nanofibers were found to have diameters in the range of 15-80 nm while most nanofibers have diameters within the range 15-25 nm. Fourier transform infrared spectroscopy (FTIR) showed that the chemical treatments removed lignin and most of the hemicelluloses from the fibers. The thermal characteristics of the fibers were analyzed using the technique of thermogravimetric analysis (TGA) which demonstrated that these characteristics were enhanced noticeably both for the bleached pulp and nanofibers. On the other hand, the X-ray analysis indicated that both chemical and mechanical treatments can improve the crystallinity of fibers. Elsevier 2011-04 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/23889/1/Physicochemical%20characterization%20of%20pulp%20and%20nanofibers%20from%20kenaf%20stem.pdf Jonoobi, Mehdi and Harun, Jalaluddin and Md. Tahir, Paridah and Alireza, Shakeri and Osman Al-Edrus, Syeed Saifulazry and Makinejad, Majid Davoodi (2011) Physicochemical characterization of pulp and nanofibers from kenaf stem. Materials Letters, 65 (7). pp. 1098-1100. ISSN 0167-577X; ESSN: 1873-4979 http://www.sciencedirect.com/science/article/pii/S0167577X10007044 10.1016/j.matlet.2010.08.054
spellingShingle Jonoobi, Mehdi
Harun, Jalaluddin
Md. Tahir, Paridah
Alireza, Shakeri
Osman Al-Edrus, Syeed Saifulazry
Makinejad, Majid Davoodi
Physicochemical characterization of pulp and nanofibers from kenaf stem
title Physicochemical characterization of pulp and nanofibers from kenaf stem
title_full Physicochemical characterization of pulp and nanofibers from kenaf stem
title_fullStr Physicochemical characterization of pulp and nanofibers from kenaf stem
title_full_unstemmed Physicochemical characterization of pulp and nanofibers from kenaf stem
title_short Physicochemical characterization of pulp and nanofibers from kenaf stem
title_sort physicochemical characterization of pulp and nanofibers from kenaf stem
url http://psasir.upm.edu.my/id/eprint/23889/
http://psasir.upm.edu.my/id/eprint/23889/
http://psasir.upm.edu.my/id/eprint/23889/
http://psasir.upm.edu.my/id/eprint/23889/1/Physicochemical%20characterization%20of%20pulp%20and%20nanofibers%20from%20kenaf%20stem.pdf