Use of Box-Behnken design in the preparation of mesoporous carbon coated monolith - BET surface area

Preparation of fiirfuryl alcohol based activated carbon monolith is reported. The effects of the preparation parameters like carbonization temperature, concentration of polyethylene glycol (PEG) and molecular weight of PEG on surface area are investigated. Based on Box-Behnken design, a quadratic mo...

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Main Authors: Darmadi, Choong, Thomas Shean Yaw, Chuah, Teong Guan, Yap, Taufiq Yun Hin, Thaib, Anwar
Format: Article
Language:English
Published: International Congress of Chemistry and Environment 2011
Online Access:http://psasir.upm.edu.my/id/eprint/23061/
http://psasir.upm.edu.my/id/eprint/23061/1/Use%20of%20Box-Behnken%20design%20in%20the%20preparation%20of%20mesoporous%20carbon%20coated%20monolith%20-%20BET%20surface%20area.pdf
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author Darmadi,
Choong, Thomas Shean Yaw
Chuah, Teong Guan
Yap, Taufiq Yun Hin
Thaib, Anwar
author_facet Darmadi,
Choong, Thomas Shean Yaw
Chuah, Teong Guan
Yap, Taufiq Yun Hin
Thaib, Anwar
author_sort Darmadi,
building UPM Institutional Repository
collection Online Access
description Preparation of fiirfuryl alcohol based activated carbon monolith is reported. The effects of the preparation parameters like carbonization temperature, concentration of polyethylene glycol (PEG) and molecular weight of PEG on surface area are investigated. Based on Box-Behnken design, a quadratic model is developed to correlate the preparation parameters to surface area. From the analysis of variance. (ANOVA), carbonization temperature, concentration of polyethylene glycol (PEG) and molecular weight of PEG are identified the dominant parameters in controlling the surface area. The maximum surface area found from the liSM is 58'5.6m'Vg at carbonization temperature of 660°C and concentration of PEG of 31% vol. with molecular weight of PEG of 1000 g/mol.
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institution Universiti Putra Malaysia
institution_category Local University
language English
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publishDate 2011
publisher International Congress of Chemistry and Environment
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spelling upm-230612016-11-28T04:01:33Z http://psasir.upm.edu.my/id/eprint/23061/ Use of Box-Behnken design in the preparation of mesoporous carbon coated monolith - BET surface area Darmadi, Choong, Thomas Shean Yaw Chuah, Teong Guan Yap, Taufiq Yun Hin Thaib, Anwar Preparation of fiirfuryl alcohol based activated carbon monolith is reported. The effects of the preparation parameters like carbonization temperature, concentration of polyethylene glycol (PEG) and molecular weight of PEG on surface area are investigated. Based on Box-Behnken design, a quadratic model is developed to correlate the preparation parameters to surface area. From the analysis of variance. (ANOVA), carbonization temperature, concentration of polyethylene glycol (PEG) and molecular weight of PEG are identified the dominant parameters in controlling the surface area. The maximum surface area found from the liSM is 58'5.6m'Vg at carbonization temperature of 660°C and concentration of PEG of 31% vol. with molecular weight of PEG of 1000 g/mol. International Congress of Chemistry and Environment 2011-06 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/23061/1/Use%20of%20Box-Behnken%20design%20in%20the%20preparation%20of%20mesoporous%20carbon%20coated%20monolith%20-%20BET%20surface%20area.pdf Darmadi, and Choong, Thomas Shean Yaw and Chuah, Teong Guan and Yap, Taufiq Yun Hin and Thaib, Anwar (2011) Use of Box-Behnken design in the preparation of mesoporous carbon coated monolith - BET surface area. Research Journal of Chemistry and Environment, 15 (2). pp. 1-5. ISSN 0972-0626; ESSN: 2278-4527
spellingShingle Darmadi,
Choong, Thomas Shean Yaw
Chuah, Teong Guan
Yap, Taufiq Yun Hin
Thaib, Anwar
Use of Box-Behnken design in the preparation of mesoporous carbon coated monolith - BET surface area
title Use of Box-Behnken design in the preparation of mesoporous carbon coated monolith - BET surface area
title_full Use of Box-Behnken design in the preparation of mesoporous carbon coated monolith - BET surface area
title_fullStr Use of Box-Behnken design in the preparation of mesoporous carbon coated monolith - BET surface area
title_full_unstemmed Use of Box-Behnken design in the preparation of mesoporous carbon coated monolith - BET surface area
title_short Use of Box-Behnken design in the preparation of mesoporous carbon coated monolith - BET surface area
title_sort use of box-behnken design in the preparation of mesoporous carbon coated monolith - bet surface area
url http://psasir.upm.edu.my/id/eprint/23061/
http://psasir.upm.edu.my/id/eprint/23061/1/Use%20of%20Box-Behnken%20design%20in%20the%20preparation%20of%20mesoporous%20carbon%20coated%20monolith%20-%20BET%20surface%20area.pdf