Synthesis and characterization of barium hexaferrites derived from steel waste by ammonium nitrate salt melt synthesis

In this paper, a series of barium hexaferrite BaFe12O19 with different powder to salt ratio (1:3, 1:4, 1:5) were prepared using ammonium salt melt technique. Iron oxide were process from steel waste product were mixed with barium carbonate, used as starting materials to produce barium hexaferrites....

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Main Authors: Che Muda, Nor Nadhirah, Azis, Raba'ah Syahidah, Hashim, Mansor, Hassan, Jumiah, Sulaiman, Sakinah, Daud, Noruzaman, Mohd Sharani, Nuraine Mariana, Azizan, Abddul Halim, Musa, Makiyyu Abdullahi
Format: Article
Language:English
Published: Malaysian Solid State Science and Technology Society 2015
Online Access:http://psasir.upm.edu.my/id/eprint/17391/
http://psasir.upm.edu.my/id/eprint/17391/1/Synthesis%20and%20characterization%20of%20barium%20hexaferrites%20derived%20from%20steel%20waste%20by%20ammonium%20nitrate%20salt%20melt%20synthesis.pdf
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author Che Muda, Nor Nadhirah
Azis, Raba'ah Syahidah
Hashim, Mansor
Hassan, Jumiah
Sulaiman, Sakinah
Daud, Noruzaman
Mohd Sharani, Nuraine Mariana
Azizan, Abddul Halim
Musa, Makiyyu Abdullahi
author_facet Che Muda, Nor Nadhirah
Azis, Raba'ah Syahidah
Hashim, Mansor
Hassan, Jumiah
Sulaiman, Sakinah
Daud, Noruzaman
Mohd Sharani, Nuraine Mariana
Azizan, Abddul Halim
Musa, Makiyyu Abdullahi
author_sort Che Muda, Nor Nadhirah
building UPM Institutional Repository
collection Online Access
description In this paper, a series of barium hexaferrite BaFe12O19 with different powder to salt ratio (1:3, 1:4, 1:5) were prepared using ammonium salt melt technique. Iron oxide were process from steel waste product were mixed with barium carbonate, used as starting materials to produce barium hexaferrites. The ammonium nitrates in this experiment act as oxidizing agent in this synthesis. The BaFe12O19 powders were sintered at 1300°C for six hours and characterized using X-ray diffraction (XRD), Fourier transform Infrared (FTIR), Vibrating Sample Magnetometer (VSM) and Field emission Scanning Microscope (FeSEM) to investigate its crystallography, magnetic properties and morphology. The maximum coercivity and saturation magnetization obtained for sample ratio 1:3 of 1017 G and 90.9 emu/g, respectively. Increase the salt ratio decrease the coercivity and saturation magnetization values.
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publishDate 2015
publisher Malaysian Solid State Science and Technology Society
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spelling upm-173912016-04-12T01:11:05Z http://psasir.upm.edu.my/id/eprint/17391/ Synthesis and characterization of barium hexaferrites derived from steel waste by ammonium nitrate salt melt synthesis Che Muda, Nor Nadhirah Azis, Raba'ah Syahidah Hashim, Mansor Hassan, Jumiah Sulaiman, Sakinah Daud, Noruzaman Mohd Sharani, Nuraine Mariana Azizan, Abddul Halim Musa, Makiyyu Abdullahi In this paper, a series of barium hexaferrite BaFe12O19 with different powder to salt ratio (1:3, 1:4, 1:5) were prepared using ammonium salt melt technique. Iron oxide were process from steel waste product were mixed with barium carbonate, used as starting materials to produce barium hexaferrites. The ammonium nitrates in this experiment act as oxidizing agent in this synthesis. The BaFe12O19 powders were sintered at 1300°C for six hours and characterized using X-ray diffraction (XRD), Fourier transform Infrared (FTIR), Vibrating Sample Magnetometer (VSM) and Field emission Scanning Microscope (FeSEM) to investigate its crystallography, magnetic properties and morphology. The maximum coercivity and saturation magnetization obtained for sample ratio 1:3 of 1017 G and 90.9 emu/g, respectively. Increase the salt ratio decrease the coercivity and saturation magnetization values. Malaysian Solid State Science and Technology Society 2015 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/17391/1/Synthesis%20and%20characterization%20of%20barium%20hexaferrites%20derived%20from%20steel%20waste%20by%20ammonium%20nitrate%20salt%20melt%20synthesis.pdf Che Muda, Nor Nadhirah and Azis, Raba'ah Syahidah and Hashim, Mansor and Hassan, Jumiah and Sulaiman, Sakinah and Daud, Noruzaman and Mohd Sharani, Nuraine Mariana and Azizan, Abddul Halim and Musa, Makiyyu Abdullahi (2015) Synthesis and characterization of barium hexaferrites derived from steel waste by ammonium nitrate salt melt synthesis. Journal of Solid State Science and Technology Letters, 16 (1-2). pp. 73-77. ISSN 0128-8393 http://letters.masshp.net/volume-16-no-1-2-2015/
spellingShingle Che Muda, Nor Nadhirah
Azis, Raba'ah Syahidah
Hashim, Mansor
Hassan, Jumiah
Sulaiman, Sakinah
Daud, Noruzaman
Mohd Sharani, Nuraine Mariana
Azizan, Abddul Halim
Musa, Makiyyu Abdullahi
Synthesis and characterization of barium hexaferrites derived from steel waste by ammonium nitrate salt melt synthesis
title Synthesis and characterization of barium hexaferrites derived from steel waste by ammonium nitrate salt melt synthesis
title_full Synthesis and characterization of barium hexaferrites derived from steel waste by ammonium nitrate salt melt synthesis
title_fullStr Synthesis and characterization of barium hexaferrites derived from steel waste by ammonium nitrate salt melt synthesis
title_full_unstemmed Synthesis and characterization of barium hexaferrites derived from steel waste by ammonium nitrate salt melt synthesis
title_short Synthesis and characterization of barium hexaferrites derived from steel waste by ammonium nitrate salt melt synthesis
title_sort synthesis and characterization of barium hexaferrites derived from steel waste by ammonium nitrate salt melt synthesis
url http://psasir.upm.edu.my/id/eprint/17391/
http://psasir.upm.edu.my/id/eprint/17391/
http://psasir.upm.edu.my/id/eprint/17391/1/Synthesis%20and%20characterization%20of%20barium%20hexaferrites%20derived%20from%20steel%20waste%20by%20ammonium%20nitrate%20salt%20melt%20synthesis.pdf