Optimization of supercritical CO2 extraction of Anastatica hierochuntica.

Response surface methodology (RSM) was applied to optimize the variables affecting the supercritical carbon dioxide (SC-CO2) extraction of non-polar compounds from Anastatica hierochuntica using the Central Composite Design technique (CCD). Independent variables were temperature (32–46 °C) and press...

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Main Authors: N.A., Nik Norulaini, O., Anuar, F.M.A., Abbas, M.O., Fatehah, A.K., Mohd Omar, F., Sahena, Sarker , Zaidul Islam
Format: Article
Language:English
English
Published: Institution of Chemical Engineers 2009
Online Access:http://psasir.upm.edu.my/id/eprint/15987/
http://psasir.upm.edu.my/id/eprint/15987/1/Optimization%20of%20supercritical%20CO2%20extraction%20of%20Anastatica%20hierochuntica.pdf
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author N.A., Nik Norulaini
O., Anuar
F.M.A., Abbas
M.O., Fatehah
A.K., Mohd Omar
F., Sahena
Sarker , Zaidul Islam
author_facet N.A., Nik Norulaini
O., Anuar
F.M.A., Abbas
M.O., Fatehah
A.K., Mohd Omar
F., Sahena
Sarker , Zaidul Islam
author_sort N.A., Nik Norulaini
building UPM Institutional Repository
collection Online Access
description Response surface methodology (RSM) was applied to optimize the variables affecting the supercritical carbon dioxide (SC-CO2) extraction of non-polar compounds from Anastatica hierochuntica using the Central Composite Design technique (CCD). Independent variables were temperature (32–46 °C) and pressure (22–46 MPa). Dependent variables were the percentage of the content of hexadecanoic acid, 9,12-octadecadienoic acid, heneicosane and heptacosane. Pressure was the most significant parameter that affected the content of the compounds. The hexadecanoic and 9,12-octadecadienoic content decreased while heneicosane and heptacosane increased with pressure. A number of choices can be run either at low pressure and low temperature or at low pressure and high temperature in order to optimize extraction of the selected compounds. Extraction either at low temperature (33 °C) and low pressure (25.6 MPa), or at high temperature (42 °C) and low pressure (22.0 MPa) maximized the yield of hexadecanoic, 9,12-octedecanoic, heneicosane and heptacosane.
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spelling upm-159872015-12-18T07:42:16Z http://psasir.upm.edu.my/id/eprint/15987/ Optimization of supercritical CO2 extraction of Anastatica hierochuntica. N.A., Nik Norulaini O., Anuar F.M.A., Abbas M.O., Fatehah A.K., Mohd Omar F., Sahena Sarker , Zaidul Islam Response surface methodology (RSM) was applied to optimize the variables affecting the supercritical carbon dioxide (SC-CO2) extraction of non-polar compounds from Anastatica hierochuntica using the Central Composite Design technique (CCD). Independent variables were temperature (32–46 °C) and pressure (22–46 MPa). Dependent variables were the percentage of the content of hexadecanoic acid, 9,12-octadecadienoic acid, heneicosane and heptacosane. Pressure was the most significant parameter that affected the content of the compounds. The hexadecanoic and 9,12-octadecadienoic content decreased while heneicosane and heptacosane increased with pressure. A number of choices can be run either at low pressure and low temperature or at low pressure and high temperature in order to optimize extraction of the selected compounds. Extraction either at low temperature (33 °C) and low pressure (25.6 MPa), or at high temperature (42 °C) and low pressure (22.0 MPa) maximized the yield of hexadecanoic, 9,12-octedecanoic, heneicosane and heptacosane. Institution of Chemical Engineers 2009 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/15987/1/Optimization%20of%20supercritical%20CO2%20extraction%20of%20Anastatica%20hierochuntica.pdf N.A., Nik Norulaini and O., Anuar and F.M.A., Abbas and M.O., Fatehah and A.K., Mohd Omar and F., Sahena and Sarker , Zaidul Islam (2009) Optimization of supercritical CO2 extraction of Anastatica hierochuntica. Food and Bioproducts Processing, 87 (2). pp. 152-158. ISSN 0960-3085 10.1016/j.fbp.2008.09.001 English
spellingShingle N.A., Nik Norulaini
O., Anuar
F.M.A., Abbas
M.O., Fatehah
A.K., Mohd Omar
F., Sahena
Sarker , Zaidul Islam
Optimization of supercritical CO2 extraction of Anastatica hierochuntica.
title Optimization of supercritical CO2 extraction of Anastatica hierochuntica.
title_full Optimization of supercritical CO2 extraction of Anastatica hierochuntica.
title_fullStr Optimization of supercritical CO2 extraction of Anastatica hierochuntica.
title_full_unstemmed Optimization of supercritical CO2 extraction of Anastatica hierochuntica.
title_short Optimization of supercritical CO2 extraction of Anastatica hierochuntica.
title_sort optimization of supercritical co2 extraction of anastatica hierochuntica.
url http://psasir.upm.edu.my/id/eprint/15987/
http://psasir.upm.edu.my/id/eprint/15987/
http://psasir.upm.edu.my/id/eprint/15987/1/Optimization%20of%20supercritical%20CO2%20extraction%20of%20Anastatica%20hierochuntica.pdf