Influence of sintering temperature on the structural, magnetic and dielectric properties of Ni0.8Zn0.2Fe2O4 synthesized by co-precipitation route.

The polycrystalline Ni–Zn ferrite powder with the chemical formula Ni0.8Zn0.2Fe2O4 has been synthesized using co-precipitation route. The toroidal and pellet form samples were sintered at various temperatures from 700 to 1300 °C/5 h in steps of 200 °C. The structures of samples were studied by means...

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Main Authors: Jahanbin, Tania, Hashim, Mansor, Matori, Khamirul Amin, Waje, Samaila Bawa
Format: Article
Language:English
English
Published: Elsevier 2010
Online Access:http://psasir.upm.edu.my/id/eprint/15217/
http://psasir.upm.edu.my/id/eprint/15217/1/Influence%20of%20sintering%20temperature%20on%20the%20structural.pdf
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author Jahanbin, Tania
Hashim, Mansor
Matori, Khamirul Amin
Waje, Samaila Bawa
author_facet Jahanbin, Tania
Hashim, Mansor
Matori, Khamirul Amin
Waje, Samaila Bawa
author_sort Jahanbin, Tania
building UPM Institutional Repository
collection Online Access
description The polycrystalline Ni–Zn ferrite powder with the chemical formula Ni0.8Zn0.2Fe2O4 has been synthesized using co-precipitation route. The toroidal and pellet form samples were sintered at various temperatures from 700 to 1300 °C/5 h in steps of 200 °C. The structures of samples were studied by means of X-ray diffraction (XRD), scanning electron microscopy (SEM) and the energy dispersive X-ray spectroscopy (EDXS). The magnetic and dielectric measurements were carried out using a vibrating sample magnetometer (VSM) and the impedance analyzer, respectively. The highest density of 4.48 g cm−3 was obtained for the sample sintered at 1300 °C. It was found that the initial permeability increased from 4 to 17 and the RLF was in the order of 10−3 to 10−4 in the frequency range of 1.0 MHz to 1.0 GHz. The dielectric constant and dielectric loss were lower compared to the reported values for conventional solid state technique. The electrical resistivity is in the order of 108 Ω cm. Therefore, low relative loss factor and high resistivity make these ferrites particularly useful as inductor and transformer materials for high frequency applications.
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spelling upm-152172015-10-08T02:23:20Z http://psasir.upm.edu.my/id/eprint/15217/ Influence of sintering temperature on the structural, magnetic and dielectric properties of Ni0.8Zn0.2Fe2O4 synthesized by co-precipitation route. Jahanbin, Tania Hashim, Mansor Matori, Khamirul Amin Waje, Samaila Bawa The polycrystalline Ni–Zn ferrite powder with the chemical formula Ni0.8Zn0.2Fe2O4 has been synthesized using co-precipitation route. The toroidal and pellet form samples were sintered at various temperatures from 700 to 1300 °C/5 h in steps of 200 °C. The structures of samples were studied by means of X-ray diffraction (XRD), scanning electron microscopy (SEM) and the energy dispersive X-ray spectroscopy (EDXS). The magnetic and dielectric measurements were carried out using a vibrating sample magnetometer (VSM) and the impedance analyzer, respectively. The highest density of 4.48 g cm−3 was obtained for the sample sintered at 1300 °C. It was found that the initial permeability increased from 4 to 17 and the RLF was in the order of 10−3 to 10−4 in the frequency range of 1.0 MHz to 1.0 GHz. The dielectric constant and dielectric loss were lower compared to the reported values for conventional solid state technique. The electrical resistivity is in the order of 108 Ω cm. Therefore, low relative loss factor and high resistivity make these ferrites particularly useful as inductor and transformer materials for high frequency applications. Elsevier 2010 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/15217/1/Influence%20of%20sintering%20temperature%20on%20the%20structural.pdf Jahanbin, Tania and Hashim, Mansor and Matori, Khamirul Amin and Waje, Samaila Bawa (2010) Influence of sintering temperature on the structural, magnetic and dielectric properties of Ni0.8Zn0.2Fe2O4 synthesized by co-precipitation route. Journal of Alloys and Compounds, 503 (1). pp. 111-117. ISSN 0925-8388 10.1016/j.jallcom.2010.04.212 English
spellingShingle Jahanbin, Tania
Hashim, Mansor
Matori, Khamirul Amin
Waje, Samaila Bawa
Influence of sintering temperature on the structural, magnetic and dielectric properties of Ni0.8Zn0.2Fe2O4 synthesized by co-precipitation route.
title Influence of sintering temperature on the structural, magnetic and dielectric properties of Ni0.8Zn0.2Fe2O4 synthesized by co-precipitation route.
title_full Influence of sintering temperature on the structural, magnetic and dielectric properties of Ni0.8Zn0.2Fe2O4 synthesized by co-precipitation route.
title_fullStr Influence of sintering temperature on the structural, magnetic and dielectric properties of Ni0.8Zn0.2Fe2O4 synthesized by co-precipitation route.
title_full_unstemmed Influence of sintering temperature on the structural, magnetic and dielectric properties of Ni0.8Zn0.2Fe2O4 synthesized by co-precipitation route.
title_short Influence of sintering temperature on the structural, magnetic and dielectric properties of Ni0.8Zn0.2Fe2O4 synthesized by co-precipitation route.
title_sort influence of sintering temperature on the structural, magnetic and dielectric properties of ni0.8zn0.2fe2o4 synthesized by co-precipitation route.
url http://psasir.upm.edu.my/id/eprint/15217/
http://psasir.upm.edu.my/id/eprint/15217/
http://psasir.upm.edu.my/id/eprint/15217/1/Influence%20of%20sintering%20temperature%20on%20the%20structural.pdf