Fabrication and characterization of 1D brushite nanomaterials via sucrose ester reverse microemulsion
In the present study, 1-dimensional (1D) brushite nanomaterials were fabricated through sucrose ester based reverse microemulsion for the first time. X-ray diffraction patterns revealed that the nanomaterials possessed brushite crystal phase with trace amount of hydroxyapatite. The size and morpholo...
| Main Authors: | , , , , , , |
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| Format: | Article |
| Language: | English |
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Elsevier
2009
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| Online Access: | http://psasir.upm.edu.my/id/eprint/14686/ http://psasir.upm.edu.my/id/eprint/14686/1/Fabrication%20and%20characterization%20of%201D%20brushite%20nanomaterials%20via%20sucrose%20ester%20reverse%20microemulsion.pdf |
| _version_ | 1848842463041552384 |
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| author | Lim, Hong Ngee Kassim, Anuar Huang, Nay Ming Hashim, Rauzah Radiman, Shahidan Khiew, Poi Sim Chiu, Wee Siong |
| author_facet | Lim, Hong Ngee Kassim, Anuar Huang, Nay Ming Hashim, Rauzah Radiman, Shahidan Khiew, Poi Sim Chiu, Wee Siong |
| author_sort | Lim, Hong Ngee |
| building | UPM Institutional Repository |
| collection | Online Access |
| description | In the present study, 1-dimensional (1D) brushite nanomaterials were fabricated through sucrose ester based reverse microemulsion for the first time. X-ray diffraction patterns revealed that the nanomaterials possessed brushite crystal phase with trace amount of hydroxyapatite. The size and morphology of brushite crystals were governed by the changes in the aqueous-to-sucrose ester weight ratio at low initial reactant concentration, giving rise to rod-like and fibre-like 1D nanomaterials. Brushite nanorods and nanofibres with average diameters of 25.53 ± 4.60 nm (aspect ratio ∼ 6) and 76.18 ± 19.74 nm (aspect ratio ∼ 40), respectively, had been synthesized. As the reactant concentration increased, it became the key factor in controlling nucleation and crystal growth, rendering the aqueous-to-sucrose ester ratio unimportant. Formation mechanism of various morphologies of brushite crystals is postulated. |
| first_indexed | 2025-11-15T07:59:32Z |
| format | Article |
| id | upm-14686 |
| institution | Universiti Putra Malaysia |
| institution_category | Local University |
| language | English |
| last_indexed | 2025-11-15T07:59:32Z |
| publishDate | 2009 |
| publisher | Elsevier |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | upm-146862016-03-21T08:45:23Z http://psasir.upm.edu.my/id/eprint/14686/ Fabrication and characterization of 1D brushite nanomaterials via sucrose ester reverse microemulsion Lim, Hong Ngee Kassim, Anuar Huang, Nay Ming Hashim, Rauzah Radiman, Shahidan Khiew, Poi Sim Chiu, Wee Siong In the present study, 1-dimensional (1D) brushite nanomaterials were fabricated through sucrose ester based reverse microemulsion for the first time. X-ray diffraction patterns revealed that the nanomaterials possessed brushite crystal phase with trace amount of hydroxyapatite. The size and morphology of brushite crystals were governed by the changes in the aqueous-to-sucrose ester weight ratio at low initial reactant concentration, giving rise to rod-like and fibre-like 1D nanomaterials. Brushite nanorods and nanofibres with average diameters of 25.53 ± 4.60 nm (aspect ratio ∼ 6) and 76.18 ± 19.74 nm (aspect ratio ∼ 40), respectively, had been synthesized. As the reactant concentration increased, it became the key factor in controlling nucleation and crystal growth, rendering the aqueous-to-sucrose ester ratio unimportant. Formation mechanism of various morphologies of brushite crystals is postulated. Elsevier 2009-09 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/14686/1/Fabrication%20and%20characterization%20of%201D%20brushite%20nanomaterials%20via%20sucrose%20ester%20reverse%20microemulsion.pdf Lim, Hong Ngee and Kassim, Anuar and Huang, Nay Ming and Hashim, Rauzah and Radiman, Shahidan and Khiew, Poi Sim and Chiu, Wee Siong (2009) Fabrication and characterization of 1D brushite nanomaterials via sucrose ester reverse microemulsion. Ceramics International, 35 (7). pp. 2891-2897. ISSN 0272-8842; ESSN: 1873-3956 10.1016/j.ceramint.2009.03.044 |
| spellingShingle | Lim, Hong Ngee Kassim, Anuar Huang, Nay Ming Hashim, Rauzah Radiman, Shahidan Khiew, Poi Sim Chiu, Wee Siong Fabrication and characterization of 1D brushite nanomaterials via sucrose ester reverse microemulsion |
| title | Fabrication and characterization of 1D brushite nanomaterials via sucrose ester reverse microemulsion |
| title_full | Fabrication and characterization of 1D brushite nanomaterials via sucrose ester reverse microemulsion |
| title_fullStr | Fabrication and characterization of 1D brushite nanomaterials via sucrose ester reverse microemulsion |
| title_full_unstemmed | Fabrication and characterization of 1D brushite nanomaterials via sucrose ester reverse microemulsion |
| title_short | Fabrication and characterization of 1D brushite nanomaterials via sucrose ester reverse microemulsion |
| title_sort | fabrication and characterization of 1d brushite nanomaterials via sucrose ester reverse microemulsion |
| url | http://psasir.upm.edu.my/id/eprint/14686/ http://psasir.upm.edu.my/id/eprint/14686/ http://psasir.upm.edu.my/id/eprint/14686/1/Fabrication%20and%20characterization%20of%201D%20brushite%20nanomaterials%20via%20sucrose%20ester%20reverse%20microemulsion.pdf |