Extraction of tocopherol-enriched oils from Kalahari melon and roselle seeds by supercritical fluid extraction (SFE-CO2).

Tocopherol-enriched oil was extracted by supercritical fluid extraction of carbon dioxide (SFE-CO2) from Kalahari melon and roselle seeds. The SFE-CO2 process was optimised using response surface methodology(RSM) with central composite design (CCD). Three SFE-CO2 parameters namely extracting pressu...

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Main Authors: Kar, Lin Nyam, Tan, Chin Ping, Karim, Roselina, Lai, Oi Ming, Long, Kamariah, Che Man, Yaakob
Format: Article
Language:English
English
Published: Elsevier Ltd 2010
Subjects:
Online Access:http://psasir.upm.edu.my/id/eprint/14684/
http://psasir.upm.edu.my/id/eprint/14684/1/Extraction%20of%20tocopherol.pdf
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author Kar, Lin Nyam
Tan, Chin Ping
Karim, Roselina
Lai, Oi Ming
Long, Kamariah
Che Man, Yaakob
author_facet Kar, Lin Nyam
Tan, Chin Ping
Karim, Roselina
Lai, Oi Ming
Long, Kamariah
Che Man, Yaakob
author_sort Kar, Lin Nyam
building UPM Institutional Repository
collection Online Access
description Tocopherol-enriched oil was extracted by supercritical fluid extraction of carbon dioxide (SFE-CO2) from Kalahari melon and roselle seeds. The SFE-CO2 process was optimised using response surface methodology(RSM) with central composite design (CCD). Three SFE-CO2 parameters namely extracting pressure,extracting temperature, and flow rate of carbon dioxide were examined. The optimal SFE-CO2 conditions were determined and the quadratic response surfaces were drawn from the mathematical models. The optimal SFE-CO2 conditions for the extraction tocopherol-enriched oil from Kalahari melon seeds were: extracting pressure 290 bar, extracting temperature 58C, and flow rate of carbon dioxide 20 ml/min. The optimum conditions for roselle seeds were extracting pressure 200 bar, extracting temperature 80C, and flow rate of carbon dioxide 20 ml/min. These optimum conditions yielded tocopherol concentration of 274.74 and 89.75 mg/100 g oil from Kalahari seed and roselle seed, respectively. No significant(P > 0.05) differences were obtained between the experimental and predicted values.
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spelling upm-146842015-09-22T07:25:55Z http://psasir.upm.edu.my/id/eprint/14684/ Extraction of tocopherol-enriched oils from Kalahari melon and roselle seeds by supercritical fluid extraction (SFE-CO2). Kar, Lin Nyam Tan, Chin Ping Karim, Roselina Lai, Oi Ming Long, Kamariah Che Man, Yaakob Tocopherol-enriched oil was extracted by supercritical fluid extraction of carbon dioxide (SFE-CO2) from Kalahari melon and roselle seeds. The SFE-CO2 process was optimised using response surface methodology(RSM) with central composite design (CCD). Three SFE-CO2 parameters namely extracting pressure,extracting temperature, and flow rate of carbon dioxide were examined. The optimal SFE-CO2 conditions were determined and the quadratic response surfaces were drawn from the mathematical models. The optimal SFE-CO2 conditions for the extraction tocopherol-enriched oil from Kalahari melon seeds were: extracting pressure 290 bar, extracting temperature 58C, and flow rate of carbon dioxide 20 ml/min. The optimum conditions for roselle seeds were extracting pressure 200 bar, extracting temperature 80C, and flow rate of carbon dioxide 20 ml/min. These optimum conditions yielded tocopherol concentration of 274.74 and 89.75 mg/100 g oil from Kalahari seed and roselle seed, respectively. No significant(P > 0.05) differences were obtained between the experimental and predicted values. Elsevier Ltd 2010 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/14684/1/Extraction%20of%20tocopherol.pdf Kar, Lin Nyam and Tan, Chin Ping and Karim, Roselina and Lai, Oi Ming and Long, Kamariah and Che Man, Yaakob (2010) Extraction of tocopherol-enriched oils from Kalahari melon and roselle seeds by supercritical fluid extraction (SFE-CO2). Food Chemistry, 119 (3). pp. 1278-1283. ISSN 0308-8146 http://dx.doi.org/10.1016/j.foodchem.2009.08.007 Supercritical fluid extraction Tocopherol Roselle doi:10.1016/j.foodchem.2009.08.007 English
spellingShingle Supercritical fluid extraction
Tocopherol
Roselle
Kar, Lin Nyam
Tan, Chin Ping
Karim, Roselina
Lai, Oi Ming
Long, Kamariah
Che Man, Yaakob
Extraction of tocopherol-enriched oils from Kalahari melon and roselle seeds by supercritical fluid extraction (SFE-CO2).
title Extraction of tocopherol-enriched oils from Kalahari melon and roselle seeds by supercritical fluid extraction (SFE-CO2).
title_full Extraction of tocopherol-enriched oils from Kalahari melon and roselle seeds by supercritical fluid extraction (SFE-CO2).
title_fullStr Extraction of tocopherol-enriched oils from Kalahari melon and roselle seeds by supercritical fluid extraction (SFE-CO2).
title_full_unstemmed Extraction of tocopherol-enriched oils from Kalahari melon and roselle seeds by supercritical fluid extraction (SFE-CO2).
title_short Extraction of tocopherol-enriched oils from Kalahari melon and roselle seeds by supercritical fluid extraction (SFE-CO2).
title_sort extraction of tocopherol-enriched oils from kalahari melon and roselle seeds by supercritical fluid extraction (sfe-co2).
topic Supercritical fluid extraction
Tocopherol
Roselle
url http://psasir.upm.edu.my/id/eprint/14684/
http://psasir.upm.edu.my/id/eprint/14684/
http://psasir.upm.edu.my/id/eprint/14684/
http://psasir.upm.edu.my/id/eprint/14684/1/Extraction%20of%20tocopherol.pdf