Homogenizer-intensified room temperature emollient ester isoamyl oleate production
The present study reports a successful experiment to produce emollient ester isoamyl oleate (IAO) in room temperature conditions. The process was conducted under mild conditions without external heating. A factorial design was applied to study the effects of molar ratio, catalyst concentration, and...
| Main Authors: | , , , , , , , , |
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| Format: | Article |
| Language: | English |
| Published: |
Elsevier B.V.
2025
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| Online Access: | http://psasir.upm.edu.my/id/eprint/120917/ http://psasir.upm.edu.my/id/eprint/120917/1/120917.pdf |
| _version_ | 1848868246129737728 |
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| author | Tarigan, Juliati Br Santoso, Aman Sitepu, Eko K. Supeno, Minto Peranginangin, Sabarmin Sihotang, John P. Tarigan, Gloria M. Chaidir, David Taufiq-Yap, Y. H. |
| author_facet | Tarigan, Juliati Br Santoso, Aman Sitepu, Eko K. Supeno, Minto Peranginangin, Sabarmin Sihotang, John P. Tarigan, Gloria M. Chaidir, David Taufiq-Yap, Y. H. |
| author_sort | Tarigan, Juliati Br |
| building | UPM Institutional Repository |
| collection | Online Access |
| description | The present study reports a successful experiment to produce emollient ester isoamyl oleate (IAO) in room temperature conditions. The process was conducted under mild conditions without external heating. A factorial design was applied to study the effects of molar ratio, catalyst concentration, and rotational speed over different reaction times. The highest IAO conversion (99.3 %) was achieved within just 5 min at room temperature using a 1: 3 M ratio, 0.1 M catalyst concentration, and 4000 rpm rotational speed. The reaction was completed rapidly due to enhanced mass transfer and mixing. Compared to conventional reflux and microwave-assisted methods, the homogenizer-assisted process reduced energy consumption by up to 93 % and reaction time by over 90 %. This approach demonstrates a promising green alternative for ester production with significant energy and time savings. |
| first_indexed | 2025-11-15T14:49:20Z |
| format | Article |
| id | upm-120917 |
| institution | Universiti Putra Malaysia |
| institution_category | Local University |
| language | English |
| last_indexed | 2025-11-15T14:49:20Z |
| publishDate | 2025 |
| publisher | Elsevier B.V. |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | upm-1209172025-10-15T07:34:34Z http://psasir.upm.edu.my/id/eprint/120917/ Homogenizer-intensified room temperature emollient ester isoamyl oleate production Tarigan, Juliati Br Santoso, Aman Sitepu, Eko K. Supeno, Minto Peranginangin, Sabarmin Sihotang, John P. Tarigan, Gloria M. Chaidir, David Taufiq-Yap, Y. H. The present study reports a successful experiment to produce emollient ester isoamyl oleate (IAO) in room temperature conditions. The process was conducted under mild conditions without external heating. A factorial design was applied to study the effects of molar ratio, catalyst concentration, and rotational speed over different reaction times. The highest IAO conversion (99.3 %) was achieved within just 5 min at room temperature using a 1: 3 M ratio, 0.1 M catalyst concentration, and 4000 rpm rotational speed. The reaction was completed rapidly due to enhanced mass transfer and mixing. Compared to conventional reflux and microwave-assisted methods, the homogenizer-assisted process reduced energy consumption by up to 93 % and reaction time by over 90 %. This approach demonstrates a promising green alternative for ester production with significant energy and time savings. Elsevier B.V. 2025 Article PeerReviewed text en cc_by_nc_4 http://psasir.upm.edu.my/id/eprint/120917/1/120917.pdf Tarigan, Juliati Br and Santoso, Aman and Sitepu, Eko K. and Supeno, Minto and Peranginangin, Sabarmin and Sihotang, John P. and Tarigan, Gloria M. and Chaidir, David and Taufiq-Yap, Y. H. (2025) Homogenizer-intensified room temperature emollient ester isoamyl oleate production. Results in Chemistry, 17. art. no. 102659. pp. 1-6. ISSN 2211-7156 https://linkinghub.elsevier.com/retrieve/pii/S2211715625006423 10.1016/j.rechem.2025.102659 |
| spellingShingle | Tarigan, Juliati Br Santoso, Aman Sitepu, Eko K. Supeno, Minto Peranginangin, Sabarmin Sihotang, John P. Tarigan, Gloria M. Chaidir, David Taufiq-Yap, Y. H. Homogenizer-intensified room temperature emollient ester isoamyl oleate production |
| title | Homogenizer-intensified room temperature emollient ester isoamyl oleate production |
| title_full | Homogenizer-intensified room temperature emollient ester isoamyl oleate production |
| title_fullStr | Homogenizer-intensified room temperature emollient ester isoamyl oleate production |
| title_full_unstemmed | Homogenizer-intensified room temperature emollient ester isoamyl oleate production |
| title_short | Homogenizer-intensified room temperature emollient ester isoamyl oleate production |
| title_sort | homogenizer-intensified room temperature emollient ester isoamyl oleate production |
| url | http://psasir.upm.edu.my/id/eprint/120917/ http://psasir.upm.edu.my/id/eprint/120917/ http://psasir.upm.edu.my/id/eprint/120917/ http://psasir.upm.edu.my/id/eprint/120917/1/120917.pdf |