Effect of calcination temperature on the characteristics of MoV oxides prepared via reflux method

In this study, MoV mixed oxides with a molar ratio of 10:3 were prepared by reflux method. The samples were subjected to various calcination temperatures in order to investigate the physicochemical properties of the oxide affected by the parameter. Samples were characterised by XRD, TG/DTA, BET sur...

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Main Authors: Tan, Yee Wean, Ramli, Irmawati, Yap, Taufiq Yun Hin
Format: Article
Language:English
Published: Malaysian Analytical Sciences Society 2007
Online Access:http://psasir.upm.edu.my/id/eprint/11938/
http://psasir.upm.edu.my/id/eprint/11938/1/Effect%20of%20calcination%20temperature%20on%20the%20characteristics%20of%20MoV%20oxides%20prepared%20via%20reflux%20method.pdf
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author Tan, Yee Wean
Ramli, Irmawati
Yap, Taufiq Yun Hin
author_facet Tan, Yee Wean
Ramli, Irmawati
Yap, Taufiq Yun Hin
author_sort Tan, Yee Wean
building UPM Institutional Repository
collection Online Access
description In this study, MoV mixed oxides with a molar ratio of 10:3 were prepared by reflux method. The samples were subjected to various calcination temperatures in order to investigate the physicochemical properties of the oxide affected by the parameter. Samples were characterised by XRD, TG/DTA, BET surface area, SEM and TPR. By imposing various calcination temperatures, phase evolutions were observed. However, these changes do not significantly affect the morphology, surface area, particle size and reducibility of the oxide. Still, the best calcination temperature can be chosen to arrive at the effective catalyst necessary for the desired catalytic reaction.
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institution Universiti Putra Malaysia
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publisher Malaysian Analytical Sciences Society
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spelling upm-119382016-11-25T09:13:54Z http://psasir.upm.edu.my/id/eprint/11938/ Effect of calcination temperature on the characteristics of MoV oxides prepared via reflux method Tan, Yee Wean Ramli, Irmawati Yap, Taufiq Yun Hin In this study, MoV mixed oxides with a molar ratio of 10:3 were prepared by reflux method. The samples were subjected to various calcination temperatures in order to investigate the physicochemical properties of the oxide affected by the parameter. Samples were characterised by XRD, TG/DTA, BET surface area, SEM and TPR. By imposing various calcination temperatures, phase evolutions were observed. However, these changes do not significantly affect the morphology, surface area, particle size and reducibility of the oxide. Still, the best calcination temperature can be chosen to arrive at the effective catalyst necessary for the desired catalytic reaction. Malaysian Analytical Sciences Society 2007 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/11938/1/Effect%20of%20calcination%20temperature%20on%20the%20characteristics%20of%20MoV%20oxides%20prepared%20via%20reflux%20method.pdf Tan, Yee Wean and Ramli, Irmawati and Yap, Taufiq Yun Hin (2007) Effect of calcination temperature on the characteristics of MoV oxides prepared via reflux method. The Malaysian Journal of Analytical Sciences, 11 (1). pp. 145-153. ISSN 1394-2506 http://www.ukm.my/mjas/new_mjas/
spellingShingle Tan, Yee Wean
Ramli, Irmawati
Yap, Taufiq Yun Hin
Effect of calcination temperature on the characteristics of MoV oxides prepared via reflux method
title Effect of calcination temperature on the characteristics of MoV oxides prepared via reflux method
title_full Effect of calcination temperature on the characteristics of MoV oxides prepared via reflux method
title_fullStr Effect of calcination temperature on the characteristics of MoV oxides prepared via reflux method
title_full_unstemmed Effect of calcination temperature on the characteristics of MoV oxides prepared via reflux method
title_short Effect of calcination temperature on the characteristics of MoV oxides prepared via reflux method
title_sort effect of calcination temperature on the characteristics of mov oxides prepared via reflux method
url http://psasir.upm.edu.my/id/eprint/11938/
http://psasir.upm.edu.my/id/eprint/11938/
http://psasir.upm.edu.my/id/eprint/11938/1/Effect%20of%20calcination%20temperature%20on%20the%20characteristics%20of%20MoV%20oxides%20prepared%20via%20reflux%20method.pdf