Advanced fabrication of complex biopolymer microcapsules via RSM-optimized supercritical carbon dioxide solution-enhanced dispersion: a comparative analysis of various microencapsulation techniques
This work aimed to enhance hemp seed oil encapsulation within a hemp seed protein-alginate complex by optimizing parameters in the solution-enhanced dispersion process, employing supercritical carbon dioxide (SEDS) without reliance on organic solvents or elevated temperatures. By response surface me...
| Main Authors: | , , , , , , , |
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| Format: | Article |
| Language: | English |
| Published: |
Elsevier
2024
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| Online Access: | http://psasir.upm.edu.my/id/eprint/119354/ http://psasir.upm.edu.my/id/eprint/119354/1/119354.pdf |
| _version_ | 1848867942455836672 |
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| author | Gholivand, Somayeh Tan, Tai Boon Mat Yusoff, Masni Choy, Hew Weng Teow, Shuh Jun Wang, Yong Liu, Yuanfa Tan, Chin Ping |
| author_facet | Gholivand, Somayeh Tan, Tai Boon Mat Yusoff, Masni Choy, Hew Weng Teow, Shuh Jun Wang, Yong Liu, Yuanfa Tan, Chin Ping |
| author_sort | Gholivand, Somayeh |
| building | UPM Institutional Repository |
| collection | Online Access |
| description | This work aimed to enhance hemp seed oil encapsulation within a hemp seed protein-alginate complex by optimizing parameters in the solution-enhanced dispersion process, employing supercritical carbon dioxide (SEDS) without reliance on organic solvents or elevated temperatures. By response surface methodology (RSM), the microencapsulation efficacy (MEE), particle size (PS) and peroxide value (PV) was determined with respect to three parameters; temperature (°C), pressure (bar) and feed flow rate (mL/min). The optimum conditions were predicted at temperature (40 °C), pressure (150 bar) and feed flow rate (2 mL/min) to offer an MEE of 89.47%, PS of 7.81 μm and PV of 2.91 (meq/kg oil). In addition, the SEDS method was compared with spray- and freeze-drying for encapsulating hemp seed oil. The findings demonstrated SEDS' superiority, exhibiting exceptional attributes such as the highest MEE, smallest PS and the production of spherical, smooth microcapsules. This highlights its effectiveness in comparison to spray- and freeze-drying methods. |
| first_indexed | 2025-11-15T14:44:31Z |
| format | Article |
| id | upm-119354 |
| institution | Universiti Putra Malaysia |
| institution_category | Local University |
| language | English |
| last_indexed | 2025-11-15T14:44:31Z |
| publishDate | 2024 |
| publisher | Elsevier |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | upm-1193542025-09-11T06:49:22Z http://psasir.upm.edu.my/id/eprint/119354/ Advanced fabrication of complex biopolymer microcapsules via RSM-optimized supercritical carbon dioxide solution-enhanced dispersion: a comparative analysis of various microencapsulation techniques Gholivand, Somayeh Tan, Tai Boon Mat Yusoff, Masni Choy, Hew Weng Teow, Shuh Jun Wang, Yong Liu, Yuanfa Tan, Chin Ping This work aimed to enhance hemp seed oil encapsulation within a hemp seed protein-alginate complex by optimizing parameters in the solution-enhanced dispersion process, employing supercritical carbon dioxide (SEDS) without reliance on organic solvents or elevated temperatures. By response surface methodology (RSM), the microencapsulation efficacy (MEE), particle size (PS) and peroxide value (PV) was determined with respect to three parameters; temperature (°C), pressure (bar) and feed flow rate (mL/min). The optimum conditions were predicted at temperature (40 °C), pressure (150 bar) and feed flow rate (2 mL/min) to offer an MEE of 89.47%, PS of 7.81 μm and PV of 2.91 (meq/kg oil). In addition, the SEDS method was compared with spray- and freeze-drying for encapsulating hemp seed oil. The findings demonstrated SEDS' superiority, exhibiting exceptional attributes such as the highest MEE, smallest PS and the production of spherical, smooth microcapsules. This highlights its effectiveness in comparison to spray- and freeze-drying methods. Elsevier 2024 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/119354/1/119354.pdf Gholivand, Somayeh and Tan, Tai Boon and Mat Yusoff, Masni and Choy, Hew Weng and Teow, Shuh Jun and Wang, Yong and Liu, Yuanfa and Tan, Chin Ping (2024) Advanced fabrication of complex biopolymer microcapsules via RSM-optimized supercritical carbon dioxide solution-enhanced dispersion: a comparative analysis of various microencapsulation techniques. Food Chemistry, 452. art. no. 139591. pp. 1-13. ISSN 0308-8146; eISSN: 1873-7072 https://linkinghub.elsevier.com/retrieve/pii/S030881462401241X 10.1016/j.foodchem.2024.139591 |
| spellingShingle | Gholivand, Somayeh Tan, Tai Boon Mat Yusoff, Masni Choy, Hew Weng Teow, Shuh Jun Wang, Yong Liu, Yuanfa Tan, Chin Ping Advanced fabrication of complex biopolymer microcapsules via RSM-optimized supercritical carbon dioxide solution-enhanced dispersion: a comparative analysis of various microencapsulation techniques |
| title | Advanced fabrication of complex biopolymer microcapsules via RSM-optimized supercritical carbon dioxide solution-enhanced dispersion: a comparative analysis of various microencapsulation techniques |
| title_full | Advanced fabrication of complex biopolymer microcapsules via RSM-optimized supercritical carbon dioxide solution-enhanced dispersion: a comparative analysis of various microencapsulation techniques |
| title_fullStr | Advanced fabrication of complex biopolymer microcapsules via RSM-optimized supercritical carbon dioxide solution-enhanced dispersion: a comparative analysis of various microencapsulation techniques |
| title_full_unstemmed | Advanced fabrication of complex biopolymer microcapsules via RSM-optimized supercritical carbon dioxide solution-enhanced dispersion: a comparative analysis of various microencapsulation techniques |
| title_short | Advanced fabrication of complex biopolymer microcapsules via RSM-optimized supercritical carbon dioxide solution-enhanced dispersion: a comparative analysis of various microencapsulation techniques |
| title_sort | advanced fabrication of complex biopolymer microcapsules via rsm-optimized supercritical carbon dioxide solution-enhanced dispersion: a comparative analysis of various microencapsulation techniques |
| url | http://psasir.upm.edu.my/id/eprint/119354/ http://psasir.upm.edu.my/id/eprint/119354/ http://psasir.upm.edu.my/id/eprint/119354/ http://psasir.upm.edu.my/id/eprint/119354/1/119354.pdf |