Green electrosynthesis strategies of SnO catalysts for enhanced photodegradation of 2,4-dichlorophenol

The electrogeneration of SnO using an environmentally friendly approach was assessed by utilizing three different electrolytes: N,N-dimethylformamide (DMF), plant extract (PE), and a combination of PE with a deep eutectic solvent (PE-DES). The catalysts were characterized through FTIR, XRD, BET surf...

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Main Authors: Torlaema, T. A.M., Jaafar, Nur Farhana, Mutalib, A. A.A., Lahuri, A. H.
Format: Article
Language:English
Published: John Wiley and Sons Inc 2025
Subjects:
Online Access:http://psasir.upm.edu.my/id/eprint/119259/
http://psasir.upm.edu.my/id/eprint/119259/1/119259.pdf
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author Torlaema, T. A.M.
Jaafar, Nur Farhana
Mutalib, A. A.A.
Lahuri, A. H.
author_facet Torlaema, T. A.M.
Jaafar, Nur Farhana
Mutalib, A. A.A.
Lahuri, A. H.
author_sort Torlaema, T. A.M.
building UPM Institutional Repository
collection Online Access
description The electrogeneration of SnO using an environmentally friendly approach was assessed by utilizing three different electrolytes: N,N-dimethylformamide (DMF), plant extract (PE), and a combination of PE with a deep eutectic solvent (PE-DES). The catalysts were characterized through FTIR, XRD, BET surface area analysis, and UV–Vis DRS to determine their structural and optical properties. The photocatalytic degradation of 2,4-dichlorophenol (2,4-DCP) was then evaluated for each catalyst under visible light exposure. At pH 3, SnO-PE-DES exhibited the highest degradation rate of 99.22%, making it the most efficient catalyst. SnO-DMF showed a degradation efficiency of 93.81%, while commercial SnO achieved 86.60%. The degradation efficiency of SnO-PE alone was only 23.46%, but incorporating DES significantly improved its performance. This enhancement is attributed to DES's ability to promote a more organized SnO structure, increasing the surface area and improving interactions with 2,4-DCP molecules. Due to its environmentally friendly synthesis and outstanding photocatalytic activity, SnO-PE-DES was selected for further optimization studies. This catalyst demonstrates great potential for photocatalytic applications in wastewater treatment. Its impressive performance under visible light, coupled with its eco-friendly synthesis, makes it a promising candidate for large-scale environmental remediation projects powered by solar energy.
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spelling upm-1192592025-08-14T08:02:34Z http://psasir.upm.edu.my/id/eprint/119259/ Green electrosynthesis strategies of SnO catalysts for enhanced photodegradation of 2,4-dichlorophenol Torlaema, T. A.M. Jaafar, Nur Farhana Mutalib, A. A.A. Lahuri, A. H. The electrogeneration of SnO using an environmentally friendly approach was assessed by utilizing three different electrolytes: N,N-dimethylformamide (DMF), plant extract (PE), and a combination of PE with a deep eutectic solvent (PE-DES). The catalysts were characterized through FTIR, XRD, BET surface area analysis, and UV–Vis DRS to determine their structural and optical properties. The photocatalytic degradation of 2,4-dichlorophenol (2,4-DCP) was then evaluated for each catalyst under visible light exposure. At pH 3, SnO-PE-DES exhibited the highest degradation rate of 99.22%, making it the most efficient catalyst. SnO-DMF showed a degradation efficiency of 93.81%, while commercial SnO achieved 86.60%. The degradation efficiency of SnO-PE alone was only 23.46%, but incorporating DES significantly improved its performance. This enhancement is attributed to DES's ability to promote a more organized SnO structure, increasing the surface area and improving interactions with 2,4-DCP molecules. Due to its environmentally friendly synthesis and outstanding photocatalytic activity, SnO-PE-DES was selected for further optimization studies. This catalyst demonstrates great potential for photocatalytic applications in wastewater treatment. Its impressive performance under visible light, coupled with its eco-friendly synthesis, makes it a promising candidate for large-scale environmental remediation projects powered by solar energy. John Wiley and Sons Inc 2025 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/119259/1/119259.pdf Torlaema, T. A.M. and Jaafar, Nur Farhana and Mutalib, A. A.A. and Lahuri, A. H. (2025) Green electrosynthesis strategies of SnO catalysts for enhanced photodegradation of 2,4-dichlorophenol. Journal of the Chinese Chemical Society, 72 (5). pp. 498-512. ISSN 0009-4536; eISSN: 2192-6549 https://onlinelibrary.wiley.com/doi/10.1002/jccs.70014 Chemistry 10.1002/jccs.70014
spellingShingle Chemistry
Torlaema, T. A.M.
Jaafar, Nur Farhana
Mutalib, A. A.A.
Lahuri, A. H.
Green electrosynthesis strategies of SnO catalysts for enhanced photodegradation of 2,4-dichlorophenol
title Green electrosynthesis strategies of SnO catalysts for enhanced photodegradation of 2,4-dichlorophenol
title_full Green electrosynthesis strategies of SnO catalysts for enhanced photodegradation of 2,4-dichlorophenol
title_fullStr Green electrosynthesis strategies of SnO catalysts for enhanced photodegradation of 2,4-dichlorophenol
title_full_unstemmed Green electrosynthesis strategies of SnO catalysts for enhanced photodegradation of 2,4-dichlorophenol
title_short Green electrosynthesis strategies of SnO catalysts for enhanced photodegradation of 2,4-dichlorophenol
title_sort green electrosynthesis strategies of sno catalysts for enhanced photodegradation of 2,4-dichlorophenol
topic Chemistry
url http://psasir.upm.edu.my/id/eprint/119259/
http://psasir.upm.edu.my/id/eprint/119259/
http://psasir.upm.edu.my/id/eprint/119259/
http://psasir.upm.edu.my/id/eprint/119259/1/119259.pdf