Facile synthesis and adsorptive removal of rhodamine b dye from aqueous medium using green synthesized nanocomposite

Reduced graphene oxide (rGO) and zinc oxide nanoparticles (ZnO NPs) were synthesized using modified Hummer's method and green approach from Carica papaya leaf extract (CPLE), respectively. ZnO NPs were then loaded onto rGO using a straightforward ultrasonic method to synthesize Zinc oxide-reduc...

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Main Authors: Gbawoquiya, Flomo L., Rachna, Kumari, Narayanan, Shankara S., Singh, Pramod K., Shankar, Shiv, Mohd Noor, Ikhwan Syafiq, Yahya, Muhd Zu Azhan
Format: Article
Language:English
Published: Engineers Society for Corrosion 2024
Online Access:http://psasir.upm.edu.my/id/eprint/116693/
http://psasir.upm.edu.my/id/eprint/116693/1/116693.pdf
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author Gbawoquiya, Flomo L.
Rachna, Kumari
Narayanan, Shankara S.
Singh, Pramod K.
Shankar, Shiv
Mohd Noor, Ikhwan Syafiq
Yahya, Muhd Zu Azhan
author_facet Gbawoquiya, Flomo L.
Rachna, Kumari
Narayanan, Shankara S.
Singh, Pramod K.
Shankar, Shiv
Mohd Noor, Ikhwan Syafiq
Yahya, Muhd Zu Azhan
author_sort Gbawoquiya, Flomo L.
building UPM Institutional Repository
collection Online Access
description Reduced graphene oxide (rGO) and zinc oxide nanoparticles (ZnO NPs) were synthesized using modified Hummer's method and green approach from Carica papaya leaf extract (CPLE), respectively. ZnO NPs were then loaded onto rGO using a straightforward ultrasonic method to synthesize Zinc oxide-reduced graphene oxide nanocomposite (ZnO-rGO NC). Fourier Transform Infrared Spectroscopy (FTIR), Field Emission Scanning Electron Microscopy (FESEM), and X-ray diffraction (XRD) techniques were used to characterize the synthesized nanoparticles and composite respectively. The nanocomposite was used to remove Rhodamine B dye (RhB) from aqueous solution. The effects of temperature, pH, adsorbent dosage, initial dye concentration, and contact time were investigated. Testing was done on the Freundlich and Langmuir isotherm models as well and the thermodynamics parameters were computed. The effects of ZnO NPs, rGO, and ZnO-rGO NC independently on dye removal in a comparative analysis were carried out and resulteds were presented. In an aqueous medium, the nanocomposite demonstrated high removal efficiency as an adsorbent for removing RhB dye at 99% compared to ZnO NPs at 60%. ZnO-rGO NC proved to be an effective adsorbent compare to ZnO NPs.
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spelling upm-1166932025-04-15T02:38:33Z http://psasir.upm.edu.my/id/eprint/116693/ Facile synthesis and adsorptive removal of rhodamine b dye from aqueous medium using green synthesized nanocomposite Gbawoquiya, Flomo L. Rachna, Kumari Narayanan, Shankara S. Singh, Pramod K. Shankar, Shiv Mohd Noor, Ikhwan Syafiq Yahya, Muhd Zu Azhan Reduced graphene oxide (rGO) and zinc oxide nanoparticles (ZnO NPs) were synthesized using modified Hummer's method and green approach from Carica papaya leaf extract (CPLE), respectively. ZnO NPs were then loaded onto rGO using a straightforward ultrasonic method to synthesize Zinc oxide-reduced graphene oxide nanocomposite (ZnO-rGO NC). Fourier Transform Infrared Spectroscopy (FTIR), Field Emission Scanning Electron Microscopy (FESEM), and X-ray diffraction (XRD) techniques were used to characterize the synthesized nanoparticles and composite respectively. The nanocomposite was used to remove Rhodamine B dye (RhB) from aqueous solution. The effects of temperature, pH, adsorbent dosage, initial dye concentration, and contact time were investigated. Testing was done on the Freundlich and Langmuir isotherm models as well and the thermodynamics parameters were computed. The effects of ZnO NPs, rGO, and ZnO-rGO NC independently on dye removal in a comparative analysis were carried out and resulteds were presented. In an aqueous medium, the nanocomposite demonstrated high removal efficiency as an adsorbent for removing RhB dye at 99% compared to ZnO NPs at 60%. ZnO-rGO NC proved to be an effective adsorbent compare to ZnO NPs. Engineers Society for Corrosion 2024-09-21 Article PeerReviewed text en cc_by_4 http://psasir.upm.edu.my/id/eprint/116693/1/116693.pdf Gbawoquiya, Flomo L. and Rachna, Kumari and Narayanan, Shankara S. and Singh, Pramod K. and Shankar, Shiv and Mohd Noor, Ikhwan Syafiq and Yahya, Muhd Zu Azhan (2024) Facile synthesis and adsorptive removal of rhodamine b dye from aqueous medium using green synthesized nanocomposite. Materials Protection, 65 (3). pp. 452-465. ISSN 0351-9465; eISSN: 2466-2585 https://www.zastita-materijala.org/index.php/home/article/view/1201 10.62638/ZasMat1201
spellingShingle Gbawoquiya, Flomo L.
Rachna, Kumari
Narayanan, Shankara S.
Singh, Pramod K.
Shankar, Shiv
Mohd Noor, Ikhwan Syafiq
Yahya, Muhd Zu Azhan
Facile synthesis and adsorptive removal of rhodamine b dye from aqueous medium using green synthesized nanocomposite
title Facile synthesis and adsorptive removal of rhodamine b dye from aqueous medium using green synthesized nanocomposite
title_full Facile synthesis and adsorptive removal of rhodamine b dye from aqueous medium using green synthesized nanocomposite
title_fullStr Facile synthesis and adsorptive removal of rhodamine b dye from aqueous medium using green synthesized nanocomposite
title_full_unstemmed Facile synthesis and adsorptive removal of rhodamine b dye from aqueous medium using green synthesized nanocomposite
title_short Facile synthesis and adsorptive removal of rhodamine b dye from aqueous medium using green synthesized nanocomposite
title_sort facile synthesis and adsorptive removal of rhodamine b dye from aqueous medium using green synthesized nanocomposite
url http://psasir.upm.edu.my/id/eprint/116693/
http://psasir.upm.edu.my/id/eprint/116693/
http://psasir.upm.edu.my/id/eprint/116693/
http://psasir.upm.edu.my/id/eprint/116693/1/116693.pdf