Antihypertensive, antidiabetic, and antioxidant properties of novel Azolla pinnata fern protein hydrolysates: inhibition mechanism, stability, profiling, and molecular docking

The Azolla pinnata fern protein was enzymatically hydrolysed with Alcalase, Flavourzyme, and Papain at varying degrees of hydrolysis (10, 20, and 30%) to generate multi-biologically active protein hydrolysates. The extensively hydrolysed (30%) Alcalase-generated hydrolysate (AFPH-AE) was most active...

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Main Authors: Qoms, Mohammed S., Arulrajah, Brisha, Wan Ibadullah, Wan Zunairah, Ramli, Nurul Shazini, Shamsudin, Rosnah, Chau, De Ming, Saari, Nazamid
Format: Article
Language:English
Published: Springer 2024
Online Access:http://psasir.upm.edu.my/id/eprint/116419/
http://psasir.upm.edu.my/id/eprint/116419/1/116419.pdf
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author Qoms, Mohammed S.
Arulrajah, Brisha
Wan Ibadullah, Wan Zunairah
Ramli, Nurul Shazini
Shamsudin, Rosnah
Chau, De Ming
Saari, Nazamid
author_facet Qoms, Mohammed S.
Arulrajah, Brisha
Wan Ibadullah, Wan Zunairah
Ramli, Nurul Shazini
Shamsudin, Rosnah
Chau, De Ming
Saari, Nazamid
author_sort Qoms, Mohammed S.
building UPM Institutional Repository
collection Online Access
description The Azolla pinnata fern protein was enzymatically hydrolysed with Alcalase, Flavourzyme, and Papain at varying degrees of hydrolysis (10, 20, and 30%) to generate multi-biologically active protein hydrolysates. The extensively hydrolysed (30%) Alcalase-generated hydrolysate (AFPH-AE) was most active demonstrating antihypertensive (ACE inhibition), antidiabetic (DPP-IV, α-glucosidase, and α-amylase inhibition), and antioxidant (DPPH, ABTS, and FRAP) activities. AFPH-AE exhibited an uncompetitive inhibition mode against ACE and α-glucosidase, a mixed inhibition mode against α-amylase, and a noncompetitive inhibition mode against DPP-IV. This hydrolysate was highly stable under different food processing conditions including pH 5, 7, and 8, NaCl up to 150 mM, and a high temperature of 100 °C. The low molecular weight fraction (< 3 kDa) exhibited high biological activities, and a total of 15 low molecular weight bioactive peptides were identified. Molecular docking revealed that the peptide-enzyme interactions were mainly mediated via hydrogen bonds and hydrophobic interactions. Overall, these findings reveal the potential of AFPH-AE as a functional and/or nutraceutical ingredient with multifunctional antihypertensive, antidiabetic, and antioxidant effects.
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spelling upm-1164192025-04-09T04:01:55Z http://psasir.upm.edu.my/id/eprint/116419/ Antihypertensive, antidiabetic, and antioxidant properties of novel Azolla pinnata fern protein hydrolysates: inhibition mechanism, stability, profiling, and molecular docking Qoms, Mohammed S. Arulrajah, Brisha Wan Ibadullah, Wan Zunairah Ramli, Nurul Shazini Shamsudin, Rosnah Chau, De Ming Saari, Nazamid The Azolla pinnata fern protein was enzymatically hydrolysed with Alcalase, Flavourzyme, and Papain at varying degrees of hydrolysis (10, 20, and 30%) to generate multi-biologically active protein hydrolysates. The extensively hydrolysed (30%) Alcalase-generated hydrolysate (AFPH-AE) was most active demonstrating antihypertensive (ACE inhibition), antidiabetic (DPP-IV, α-glucosidase, and α-amylase inhibition), and antioxidant (DPPH, ABTS, and FRAP) activities. AFPH-AE exhibited an uncompetitive inhibition mode against ACE and α-glucosidase, a mixed inhibition mode against α-amylase, and a noncompetitive inhibition mode against DPP-IV. This hydrolysate was highly stable under different food processing conditions including pH 5, 7, and 8, NaCl up to 150 mM, and a high temperature of 100 °C. The low molecular weight fraction (< 3 kDa) exhibited high biological activities, and a total of 15 low molecular weight bioactive peptides were identified. Molecular docking revealed that the peptide-enzyme interactions were mainly mediated via hydrogen bonds and hydrophobic interactions. Overall, these findings reveal the potential of AFPH-AE as a functional and/or nutraceutical ingredient with multifunctional antihypertensive, antidiabetic, and antioxidant effects. Springer 2024-04-27 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/116419/1/116419.pdf Qoms, Mohammed S. and Arulrajah, Brisha and Wan Ibadullah, Wan Zunairah and Ramli, Nurul Shazini and Shamsudin, Rosnah and Chau, De Ming and Saari, Nazamid (2024) Antihypertensive, antidiabetic, and antioxidant properties of novel Azolla pinnata fern protein hydrolysates: inhibition mechanism, stability, profiling, and molecular docking. Food and Bioprocess Technology, 17 (12). pp. 4806-4823. ISSN 1935-5130; eISSN: 1935-5149 https://link.springer.com/article/10.1007/s11947-024-03412-1?error=cookies_not_supported&code=eb3e3255-970e-4b58-b8cc-34316ec66bc1 10.1007/s11947-024-03412-1
spellingShingle Qoms, Mohammed S.
Arulrajah, Brisha
Wan Ibadullah, Wan Zunairah
Ramli, Nurul Shazini
Shamsudin, Rosnah
Chau, De Ming
Saari, Nazamid
Antihypertensive, antidiabetic, and antioxidant properties of novel Azolla pinnata fern protein hydrolysates: inhibition mechanism, stability, profiling, and molecular docking
title Antihypertensive, antidiabetic, and antioxidant properties of novel Azolla pinnata fern protein hydrolysates: inhibition mechanism, stability, profiling, and molecular docking
title_full Antihypertensive, antidiabetic, and antioxidant properties of novel Azolla pinnata fern protein hydrolysates: inhibition mechanism, stability, profiling, and molecular docking
title_fullStr Antihypertensive, antidiabetic, and antioxidant properties of novel Azolla pinnata fern protein hydrolysates: inhibition mechanism, stability, profiling, and molecular docking
title_full_unstemmed Antihypertensive, antidiabetic, and antioxidant properties of novel Azolla pinnata fern protein hydrolysates: inhibition mechanism, stability, profiling, and molecular docking
title_short Antihypertensive, antidiabetic, and antioxidant properties of novel Azolla pinnata fern protein hydrolysates: inhibition mechanism, stability, profiling, and molecular docking
title_sort antihypertensive, antidiabetic, and antioxidant properties of novel azolla pinnata fern protein hydrolysates: inhibition mechanism, stability, profiling, and molecular docking
url http://psasir.upm.edu.my/id/eprint/116419/
http://psasir.upm.edu.my/id/eprint/116419/
http://psasir.upm.edu.my/id/eprint/116419/
http://psasir.upm.edu.my/id/eprint/116419/1/116419.pdf