Electrodeposition of high hardness and high corrosion resistance Cr-C coating using trivalent chromium bath

This study presents a novel approach to optimizing Cr-C coatings to achieve enhanced microhardness and corrosion resistance, focusing on the interplay between deposition parameters and coating microstructure. Unlike prior studies that often emphasize limited parameter variations, this research provi...

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Main Authors: Tey, Eydar, Zainal, Zulkarnain, Lim, Kean Pah, Ismail, Ismayadi
Format: Article
Language:English
Published: Springer 2025
Online Access:http://psasir.upm.edu.my/id/eprint/115680/
http://psasir.upm.edu.my/id/eprint/115680/1/115680.pdf
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author Tey, Eydar
Zainal, Zulkarnain
Lim, Kean Pah
Ismail, Ismayadi
author_facet Tey, Eydar
Zainal, Zulkarnain
Lim, Kean Pah
Ismail, Ismayadi
author_sort Tey, Eydar
building UPM Institutional Repository
collection Online Access
description This study presents a novel approach to optimizing Cr-C coatings to achieve enhanced microhardness and corrosion resistance, focusing on the interplay between deposition parameters and coating microstructure. Unlike prior studies that often emphasize limited parameter variations, this research provides a comprehensive analysis of the effects of current density, pH, bath temperature, and deposition time on the microstructure and properties of Cr-C coatings. Advanced characterization techniques, including X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), energy-dispersive X-ray spectroscopy (EDX), Vickers microhardness testing, and potentiodynamic polarization scans, were employed to investigate the crystalline structure, surface morphology, composition, mechanical hardness, and corrosion behavior. The key innovation lies in correlating these parameters to achieve coatings with compact grain growth and uniform morphology, resulting in exceptional performance. The study identifies optimal deposition conditions at a current density of 20 A/dm2, pH 1.5, bath temperature of 35 °C, and deposition time of 60 minutes, which yielded the highest hardness and superior corrosion resistance. These findings significantly advance the understanding of Cr-C coating processes and their potential applications in industries demanding high durability and corrosion resistance.
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spelling upm-1156802025-03-11T05:22:52Z http://psasir.upm.edu.my/id/eprint/115680/ Electrodeposition of high hardness and high corrosion resistance Cr-C coating using trivalent chromium bath Tey, Eydar Zainal, Zulkarnain Lim, Kean Pah Ismail, Ismayadi This study presents a novel approach to optimizing Cr-C coatings to achieve enhanced microhardness and corrosion resistance, focusing on the interplay between deposition parameters and coating microstructure. Unlike prior studies that often emphasize limited parameter variations, this research provides a comprehensive analysis of the effects of current density, pH, bath temperature, and deposition time on the microstructure and properties of Cr-C coatings. Advanced characterization techniques, including X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), energy-dispersive X-ray spectroscopy (EDX), Vickers microhardness testing, and potentiodynamic polarization scans, were employed to investigate the crystalline structure, surface morphology, composition, mechanical hardness, and corrosion behavior. The key innovation lies in correlating these parameters to achieve coatings with compact grain growth and uniform morphology, resulting in exceptional performance. The study identifies optimal deposition conditions at a current density of 20 A/dm2, pH 1.5, bath temperature of 35 °C, and deposition time of 60 minutes, which yielded the highest hardness and superior corrosion resistance. These findings significantly advance the understanding of Cr-C coating processes and their potential applications in industries demanding high durability and corrosion resistance. Springer 2025-01-16 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/115680/1/115680.pdf Tey, Eydar and Zainal, Zulkarnain and Lim, Kean Pah and Ismail, Ismayadi (2025) Electrodeposition of high hardness and high corrosion resistance Cr-C coating using trivalent chromium bath. Journal of Materials Engineering and Performance. pp. 1-13. ISSN 1059-9495; eISSN: 1544-1024 https://link.springer.com/article/10.1007/s11665-025-10637-4?error=cookies_not_supported&code=d05fd147-9b7b-4d9c-8ba6-76e9b58d3fdc 10.1007/s11665-025-10637-4
spellingShingle Tey, Eydar
Zainal, Zulkarnain
Lim, Kean Pah
Ismail, Ismayadi
Electrodeposition of high hardness and high corrosion resistance Cr-C coating using trivalent chromium bath
title Electrodeposition of high hardness and high corrosion resistance Cr-C coating using trivalent chromium bath
title_full Electrodeposition of high hardness and high corrosion resistance Cr-C coating using trivalent chromium bath
title_fullStr Electrodeposition of high hardness and high corrosion resistance Cr-C coating using trivalent chromium bath
title_full_unstemmed Electrodeposition of high hardness and high corrosion resistance Cr-C coating using trivalent chromium bath
title_short Electrodeposition of high hardness and high corrosion resistance Cr-C coating using trivalent chromium bath
title_sort electrodeposition of high hardness and high corrosion resistance cr-c coating using trivalent chromium bath
url http://psasir.upm.edu.my/id/eprint/115680/
http://psasir.upm.edu.my/id/eprint/115680/
http://psasir.upm.edu.my/id/eprint/115680/
http://psasir.upm.edu.my/id/eprint/115680/1/115680.pdf