Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions

Over the years, recent advancements have provided new insights into the functionalisation and synthesis of graphene oxide-based materials for sample preparation applications, utilising deep eutectic solvents (DESs). The demand for efficient, selective, innovative, and simple sample preparation of co...

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Main Authors: Emmanuel Ibukun, Aduloju, Yahaya, Noorfatimah, Husaini Mohamed, Ahmad, Semail, Nadhiratul-Farihin, Abd Hamid, Muhammad Ariffuddin, Nadhirah Mohamad Zain, Nur, Anuar Kamaruddin, Mohammad, Hong Loh, Saw, Kamaruzaman, Sazlinda
Format: Article
Language:English
Published: Elsevier 2024
Online Access:http://psasir.upm.edu.my/id/eprint/115320/
http://psasir.upm.edu.my/id/eprint/115320/1/115320.pdf
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author Emmanuel Ibukun, Aduloju
Yahaya, Noorfatimah
Husaini Mohamed, Ahmad
Semail, Nadhiratul-Farihin
Abd Hamid, Muhammad Ariffuddin
Nadhirah Mohamad Zain, Nur
Anuar Kamaruddin, Mohammad
Hong Loh, Saw
Kamaruzaman, Sazlinda
author_facet Emmanuel Ibukun, Aduloju
Yahaya, Noorfatimah
Husaini Mohamed, Ahmad
Semail, Nadhiratul-Farihin
Abd Hamid, Muhammad Ariffuddin
Nadhirah Mohamad Zain, Nur
Anuar Kamaruddin, Mohammad
Hong Loh, Saw
Kamaruzaman, Sazlinda
author_sort Emmanuel Ibukun, Aduloju
building UPM Institutional Repository
collection Online Access
description Over the years, recent advancements have provided new insights into the functionalisation and synthesis of graphene oxide-based materials for sample preparation applications, utilising deep eutectic solvents (DESs). The demand for efficient, selective, innovative, and simple sample preparation of contaminants and pollutants from various matrices has rapidly focused on dispersive and magnetic solid-phase extraction. This study summarises the use of graphene oxide and reduced graphene materials in DES-based synthesis and functionalisation, along with their physicochemical characteristics and applications in dispersive and magnetic solid-phase extraction. The majority of DESs have demonstrated significant enhancements in the extraction of targeted analytes by increasing the effective surface area for active sites and introducing desired functionalities. Upon reviewing the existing literature, it was observed that DESs were functionalised either during or after the production of graphene materials. The findings highlight that dispersive and magnetic solid-phase extraction, incorporated with DES-functionalised graphene adsorbents, offer superior advantages for routine sample pretreatment of analytes, leading to enhanced analytical performance.
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publisher Elsevier
recordtype eprints
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spelling upm-1153202025-03-10T08:26:13Z http://psasir.upm.edu.my/id/eprint/115320/ Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions Emmanuel Ibukun, Aduloju Yahaya, Noorfatimah Husaini Mohamed, Ahmad Semail, Nadhiratul-Farihin Abd Hamid, Muhammad Ariffuddin Nadhirah Mohamad Zain, Nur Anuar Kamaruddin, Mohammad Hong Loh, Saw Kamaruzaman, Sazlinda Over the years, recent advancements have provided new insights into the functionalisation and synthesis of graphene oxide-based materials for sample preparation applications, utilising deep eutectic solvents (DESs). The demand for efficient, selective, innovative, and simple sample preparation of contaminants and pollutants from various matrices has rapidly focused on dispersive and magnetic solid-phase extraction. This study summarises the use of graphene oxide and reduced graphene materials in DES-based synthesis and functionalisation, along with their physicochemical characteristics and applications in dispersive and magnetic solid-phase extraction. The majority of DESs have demonstrated significant enhancements in the extraction of targeted analytes by increasing the effective surface area for active sites and introducing desired functionalities. Upon reviewing the existing literature, it was observed that DESs were functionalised either during or after the production of graphene materials. The findings highlight that dispersive and magnetic solid-phase extraction, incorporated with DES-functionalised graphene adsorbents, offer superior advantages for routine sample pretreatment of analytes, leading to enhanced analytical performance. Elsevier 2024 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/115320/1/115320.pdf Emmanuel Ibukun, Aduloju and Yahaya, Noorfatimah and Husaini Mohamed, Ahmad and Semail, Nadhiratul-Farihin and Abd Hamid, Muhammad Ariffuddin and Nadhirah Mohamad Zain, Nur and Anuar Kamaruddin, Mohammad and Hong Loh, Saw and Kamaruzaman, Sazlinda (2024) Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions. Microchemical Journal, 199. art. no. 110111. pp. 1-16. ISSN 0026-265X; eISSN: 0026-265X https://linkinghub.elsevier.com/retrieve/pii/S0026265X24002236 10.1016/j.microc.2024.110111
spellingShingle Emmanuel Ibukun, Aduloju
Yahaya, Noorfatimah
Husaini Mohamed, Ahmad
Semail, Nadhiratul-Farihin
Abd Hamid, Muhammad Ariffuddin
Nadhirah Mohamad Zain, Nur
Anuar Kamaruddin, Mohammad
Hong Loh, Saw
Kamaruzaman, Sazlinda
Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions
title Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions
title_full Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions
title_fullStr Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions
title_full_unstemmed Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions
title_short Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions
title_sort recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions
url http://psasir.upm.edu.my/id/eprint/115320/
http://psasir.upm.edu.my/id/eprint/115320/
http://psasir.upm.edu.my/id/eprint/115320/
http://psasir.upm.edu.my/id/eprint/115320/1/115320.pdf