Stability studies of papaya pectinesterase

Stability studies were carned out on the purilied papaya (Curiro pupqa L. var. UM~UI) pectincsterase (EC 3.1. I. I1 1. The enzyme preparation was stabk at 4’C in 0-02~ sodium phosphate butTer (pH 7.5) solution containing 0.2~ N&l and O-O% sodium azide and the loss in activity was less than 5%...

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Main Authors: Asbi, B.A, Ghazali, H.M, Yaakob, Che Man, Selamat, Jinap
Format: Article
Language:English
Published: 1995
Online Access:http://psasir.upm.edu.my/id/eprint/115029/
http://psasir.upm.edu.my/id/eprint/115029/1/115029.pdf
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author Asbi, B.A
Ghazali, H.M
Yaakob, Che Man
Selamat, Jinap
author_facet Asbi, B.A
Ghazali, H.M
Yaakob, Che Man
Selamat, Jinap
author_sort Asbi, B.A
building UPM Institutional Repository
collection Online Access
description Stability studies were carned out on the purilied papaya (Curiro pupqa L. var. UM~UI) pectincsterase (EC 3.1. I. I1 1. The enzyme preparation was stabk at 4’C in 0-02~ sodium phosphate butTer (pH 7.5) solution containing 0.2~ N&l and O-O% sodium azide and the loss in activity was less than 5% after storage (or I year. The thermoslability studia showed that enzyme was more heat-stable at pH 7-5 thao at pH 4. After heating al 60°C for 5 min. 65 6 and 82% activity still remained at pH 4 and pH 7-5. respectively. Ii war completely inactivated by heating for 5 mitt at 70 and 75°C al pH 4 and pH 7.5, respectively. The D values (time to inactivate W%, or the enzyme) at 55.60, 65 and 70°C at pH 4.0 were estimated 10 bo 112.14. 23.78.8.33 and I.71 min. respectively. Lower inactivalion rates were ohscrvcd for pH 7.5. whh lhe D values ranging from 143.27 to I.67 min for tcmper4tures between 60 and 7W. The 2 values, which indicate lhc rise in temperature necessary *o obarvc a IO-times faster rdte of heat-inaclivdtion. were estimated lo he 7%‘C and S,38’C at pH 7.5 and pH 40. respectively. The inactivation energies and Qlo values were calculated as 256.9 W/m01 and 15.59 at pH 4.0 and 284.76 kllmol and 19.21 at pH 7 5. respectively. pH stability arudics showed that the enzyme was stable from pH Cl I abler exposure of ihe enzyme LO these pHs far 24 h at 3WC. More than 85% of the activity was retained in all of these casts. However. at pH I and 12. the enzyme was unstable nnd it complctcly lost ib activity after 24 h of incubation at 30°C.
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spelling upm-1150292025-02-17T09:22:07Z http://psasir.upm.edu.my/id/eprint/115029/ Stability studies of papaya pectinesterase Asbi, B.A Ghazali, H.M Yaakob, Che Man Selamat, Jinap Stability studies were carned out on the purilied papaya (Curiro pupqa L. var. UM~UI) pectincsterase (EC 3.1. I. I1 1. The enzyme preparation was stabk at 4’C in 0-02~ sodium phosphate butTer (pH 7.5) solution containing 0.2~ N&l and O-O% sodium azide and the loss in activity was less than 5% after storage (or I year. The thermoslability studia showed that enzyme was more heat-stable at pH 7-5 thao at pH 4. After heating al 60°C for 5 min. 65 6 and 82% activity still remained at pH 4 and pH 7-5. respectively. Ii war completely inactivated by heating for 5 mitt at 70 and 75°C al pH 4 and pH 7.5, respectively. The D values (time to inactivate W%, or the enzyme) at 55.60, 65 and 70°C at pH 4.0 were estimated 10 bo 112.14. 23.78.8.33 and I.71 min. respectively. Lower inactivalion rates were ohscrvcd for pH 7.5. whh lhe D values ranging from 143.27 to I.67 min for tcmper4tures between 60 and 7W. The 2 values, which indicate lhc rise in temperature necessary *o obarvc a IO-times faster rdte of heat-inaclivdtion. were estimated lo he 7%‘C and S,38’C at pH 7.5 and pH 40. respectively. The inactivation energies and Qlo values were calculated as 256.9 W/m01 and 15.59 at pH 4.0 and 284.76 kllmol and 19.21 at pH 7 5. respectively. pH stability arudics showed that the enzyme was stable from pH Cl I abler exposure of ihe enzyme LO these pHs far 24 h at 3WC. More than 85% of the activity was retained in all of these casts. However. at pH I and 12. the enzyme was unstable nnd it complctcly lost ib activity after 24 h of incubation at 30°C. 1995 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/115029/1/115029.pdf Asbi, B.A and Ghazali, H.M and Yaakob, Che Man and Selamat, Jinap (1995) Stability studies of papaya pectinesterase. Food Chemistry, 53 (4). pp. 391-396. DOI Title User Action Timestamp 10.1016/0308-8146(95)99833-L
spellingShingle Asbi, B.A
Ghazali, H.M
Yaakob, Che Man
Selamat, Jinap
Stability studies of papaya pectinesterase
title Stability studies of papaya pectinesterase
title_full Stability studies of papaya pectinesterase
title_fullStr Stability studies of papaya pectinesterase
title_full_unstemmed Stability studies of papaya pectinesterase
title_short Stability studies of papaya pectinesterase
title_sort stability studies of papaya pectinesterase
url http://psasir.upm.edu.my/id/eprint/115029/
http://psasir.upm.edu.my/id/eprint/115029/
http://psasir.upm.edu.my/id/eprint/115029/1/115029.pdf