Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics
Melt-quenching bioglass-ceramics with the following chemical composition have been prepared 44SLS11Na2CO324ES6P2O56CaF29Al2O3 (wt%). The bioglass-ceramics were sintered at 650 °C, 750 °C, 850 °C, and 950 °C. The aim was to identify the optimal sintering temperature before glass crystallization. The...
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Springer
2024
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| Online Access: | http://psasir.upm.edu.my/id/eprint/115026/ |
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| author | Ismail, Nur Quratul Aini Sa’at, Nor Kamilah Mohd Zaid, Mohd Hafiz Zainuddin, Norhazlin Mayzan, Mohd Zul Hilmi |
| author_facet | Ismail, Nur Quratul Aini Sa’at, Nor Kamilah Mohd Zaid, Mohd Hafiz Zainuddin, Norhazlin Mayzan, Mohd Zul Hilmi |
| author_sort | Ismail, Nur Quratul Aini |
| building | UPM Institutional Repository |
| collection | Online Access |
| description | Melt-quenching bioglass-ceramics with the following chemical composition have been prepared 44SLS11Na2CO324ES6P2O56CaF29Al2O3 (wt%). The bioglass-ceramics were sintered at 650 °C, 750 °C, 850 °C, and 950 °C. The aim was to identify the optimal sintering temperature before glass crystallization. The physical properties were characterized by density and linear shrinkage. To characterize the structure properties, X-ray diffraction (XRD), scanning electron microscopy (SEM), and Fourier transform infrared spectroscopy (FTIR) were utilized. The high composition of Si and Ca in soda lime silica (SLS) glass and eggshells (ES), respectively, encourage the utilization of waste materials in the production of bioglass-ceramics. The results showed that at a sintering temperature of 950 °C, the crystallization of fluorapatite was the main phase. Moreover, the high density and optimum linear shrinkage were obtained as the sintering temperature increased. Additionally, grain growth and densification took place at this temperature. The compressive strength of bioglass-ceramics is influenced by sintering temperature and the optimal compressive strength is 136.58 MPa. © Australian Ceramic Society 2024. |
| first_indexed | 2025-11-15T14:24:12Z |
| format | Article |
| id | upm-115026 |
| institution | Universiti Putra Malaysia |
| institution_category | Local University |
| last_indexed | 2025-11-15T14:24:12Z |
| publishDate | 2024 |
| publisher | Springer |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | upm-1150262025-02-17T07:51:10Z http://psasir.upm.edu.my/id/eprint/115026/ Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics Ismail, Nur Quratul Aini Sa’at, Nor Kamilah Mohd Zaid, Mohd Hafiz Zainuddin, Norhazlin Mayzan, Mohd Zul Hilmi Melt-quenching bioglass-ceramics with the following chemical composition have been prepared 44SLS11Na2CO324ES6P2O56CaF29Al2O3 (wt%). The bioglass-ceramics were sintered at 650 °C, 750 °C, 850 °C, and 950 °C. The aim was to identify the optimal sintering temperature before glass crystallization. The physical properties were characterized by density and linear shrinkage. To characterize the structure properties, X-ray diffraction (XRD), scanning electron microscopy (SEM), and Fourier transform infrared spectroscopy (FTIR) were utilized. The high composition of Si and Ca in soda lime silica (SLS) glass and eggshells (ES), respectively, encourage the utilization of waste materials in the production of bioglass-ceramics. The results showed that at a sintering temperature of 950 °C, the crystallization of fluorapatite was the main phase. Moreover, the high density and optimum linear shrinkage were obtained as the sintering temperature increased. Additionally, grain growth and densification took place at this temperature. The compressive strength of bioglass-ceramics is influenced by sintering temperature and the optimal compressive strength is 136.58 MPa. © Australian Ceramic Society 2024. Springer 2024 Article PeerReviewed Ismail, Nur Quratul Aini and Sa’at, Nor Kamilah and Mohd Zaid, Mohd Hafiz and Zainuddin, Norhazlin and Mayzan, Mohd Zul Hilmi (2024) Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics. Journal of the Australian Ceramic Society, 60 (5). pp. 1419-1426. ISSN 2510-1560; eISSN: 2510-1579 https://link.springer.com/article/10.1007/s41779-024-01049-z?error=cookies_not_supported&code=e8e56dbe-79f2-49d0-8866-45e24f597657 10.1007/s41779-024-01049-z |
| spellingShingle | Ismail, Nur Quratul Aini Sa’at, Nor Kamilah Mohd Zaid, Mohd Hafiz Zainuddin, Norhazlin Mayzan, Mohd Zul Hilmi Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics |
| title | Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics |
| title_full | Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics |
| title_fullStr | Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics |
| title_full_unstemmed | Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics |
| title_short | Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics |
| title_sort | effect of temperature variations on the fabrication of sls-na2co3-es-p2o5-caf2-al2o3 based bioglass-ceramics |
| url | http://psasir.upm.edu.my/id/eprint/115026/ http://psasir.upm.edu.my/id/eprint/115026/ http://psasir.upm.edu.my/id/eprint/115026/ |