σ-Bonded organochromium(III) complexes. 3. decomposition in acid solution of chromium(III) complexes containing pyridylmethyl and polydentate amine ligands

The decomposition of σ-bonded (pyridylmethyl)chromium complexes, 2- and 3-NC5H4CH2CrLn(L = dap (1,3-diaminopropane), dien (diethylenetriamine), trien (triethylenetetramine), and [15]aneN4(tetraazacyclopentadecane)), was investigated in aqueous perchloric acid under aerobic conditions. Except for L =...

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Main Authors: Crouse, Karen, Goh, Lai-Yoong
Format: Article
Published: ACS Publications 1986
Online Access:http://psasir.upm.edu.my/id/eprint/114995/
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author Crouse, Karen
Goh, Lai-Yoong
author_facet Crouse, Karen
Goh, Lai-Yoong
author_sort Crouse, Karen
building UPM Institutional Repository
collection Online Access
description The decomposition of σ-bonded (pyridylmethyl)chromium complexes, 2- and 3-NC5H4CH2CrLn(L = dap (1,3-diaminopropane), dien (diethylenetriamine), trien (triethylenetetramine), and [15]aneN4(tetraazacyclopentadecane)), was investigated in aqueous perchloric acid under aerobic conditions. Except for L = 15[ane]N4, Cr-C bond scission was preceded by complete aquation in the case of the 2-isomers and partial aquation for the 3-isomers. The aquation rates were compared with those of inorganic chromium complexes containing similar amine ligands. Kinetic data for the Cr-C bond cleavage were correlated with those for the analogous ethylenediamine (en) and aquo (H20) systems. The activation parameters and product studies are in support of a homolytic pathway for the Cr-C bond cleavage.
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spelling upm-1149952025-02-14T02:29:21Z http://psasir.upm.edu.my/id/eprint/114995/ σ-Bonded organochromium(III) complexes. 3. decomposition in acid solution of chromium(III) complexes containing pyridylmethyl and polydentate amine ligands Crouse, Karen Goh, Lai-Yoong The decomposition of σ-bonded (pyridylmethyl)chromium complexes, 2- and 3-NC5H4CH2CrLn(L = dap (1,3-diaminopropane), dien (diethylenetriamine), trien (triethylenetetramine), and [15]aneN4(tetraazacyclopentadecane)), was investigated in aqueous perchloric acid under aerobic conditions. Except for L = 15[ane]N4, Cr-C bond scission was preceded by complete aquation in the case of the 2-isomers and partial aquation for the 3-isomers. The aquation rates were compared with those of inorganic chromium complexes containing similar amine ligands. Kinetic data for the Cr-C bond cleavage were correlated with those for the analogous ethylenediamine (en) and aquo (H20) systems. The activation parameters and product studies are in support of a homolytic pathway for the Cr-C bond cleavage. ACS Publications 1986-02 Article PeerReviewed Crouse, Karen and Goh, Lai-Yoong (1986) σ-Bonded organochromium(III) complexes. 3. decomposition in acid solution of chromium(III) complexes containing pyridylmethyl and polydentate amine ligands. Inorganic Chemistry, 25 (4). pp. 478-484. ISSN 0020-1669; eISSN: 1520-510X https://pubs.acs.org/doi/abs/10.1021/ic00224a017 10.1021/ic00224a017
spellingShingle Crouse, Karen
Goh, Lai-Yoong
σ-Bonded organochromium(III) complexes. 3. decomposition in acid solution of chromium(III) complexes containing pyridylmethyl and polydentate amine ligands
title σ-Bonded organochromium(III) complexes. 3. decomposition in acid solution of chromium(III) complexes containing pyridylmethyl and polydentate amine ligands
title_full σ-Bonded organochromium(III) complexes. 3. decomposition in acid solution of chromium(III) complexes containing pyridylmethyl and polydentate amine ligands
title_fullStr σ-Bonded organochromium(III) complexes. 3. decomposition in acid solution of chromium(III) complexes containing pyridylmethyl and polydentate amine ligands
title_full_unstemmed σ-Bonded organochromium(III) complexes. 3. decomposition in acid solution of chromium(III) complexes containing pyridylmethyl and polydentate amine ligands
title_short σ-Bonded organochromium(III) complexes. 3. decomposition in acid solution of chromium(III) complexes containing pyridylmethyl and polydentate amine ligands
title_sort σ-bonded organochromium(iii) complexes. 3. decomposition in acid solution of chromium(iii) complexes containing pyridylmethyl and polydentate amine ligands
url http://psasir.upm.edu.my/id/eprint/114995/
http://psasir.upm.edu.my/id/eprint/114995/
http://psasir.upm.edu.my/id/eprint/114995/