Compositional and thermal analysis of RBD palm oil adulterated with lipase-catalyzed interesterified lard

A study was conducted to determine the presence of enzymatically-randomized lard (ERLD) as an adulterant in RBD palm oil using three different analytical techniques, namely gas liquid chromatography (GLC), reversed phase high performance liquid chromatography (RP-HPLC) and differential scanning calo...

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Main Authors: Marikkar, J.M.N, Lai, O.M, Ghazali, H.M, Che Man, Y.B
Format: Article
Published: Elsevier 2002
Online Access:http://psasir.upm.edu.my/id/eprint/112492/
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author Marikkar, J.M.N
Lai, O.M
Ghazali, H.M
Che Man, Y.B
author_facet Marikkar, J.M.N
Lai, O.M
Ghazali, H.M
Che Man, Y.B
author_sort Marikkar, J.M.N
building UPM Institutional Repository
collection Online Access
description A study was conducted to determine the presence of enzymatically-randomized lard (ERLD) as an adulterant in RBD palm oil using three different analytical techniques, namely gas liquid chromatography (GLC), reversed phase high performance liquid chromatography (RP-HPLC) and differential scanning calorimetry (DSC). Lard extracted from the adipose tissues of pig was enzymatically interesterified using non-specific lipase from Pseudomonas sp. Compositional and thermal characteristics of ERLD were compared with those of genuine lard (GLD). RBD palm oil samples, adulterated separately with various levels of GLD and ERLD, were analyzed using GLC, HPLC and DSC. Neither GLC nor HPLC showed any characteristic adulteration peaks to enable RBD palm oil, adulterated with either GLD or ERLD, to be distinguished from those adulterated with chicken fat (CF). However, DSC provided a better means for identification of lard, with a detection limit of 1%.
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spelling upm-1124922025-02-19T00:05:56Z http://psasir.upm.edu.my/id/eprint/112492/ Compositional and thermal analysis of RBD palm oil adulterated with lipase-catalyzed interesterified lard Marikkar, J.M.N Lai, O.M Ghazali, H.M Che Man, Y.B A study was conducted to determine the presence of enzymatically-randomized lard (ERLD) as an adulterant in RBD palm oil using three different analytical techniques, namely gas liquid chromatography (GLC), reversed phase high performance liquid chromatography (RP-HPLC) and differential scanning calorimetry (DSC). Lard extracted from the adipose tissues of pig was enzymatically interesterified using non-specific lipase from Pseudomonas sp. Compositional and thermal characteristics of ERLD were compared with those of genuine lard (GLD). RBD palm oil samples, adulterated separately with various levels of GLD and ERLD, were analyzed using GLC, HPLC and DSC. Neither GLC nor HPLC showed any characteristic adulteration peaks to enable RBD palm oil, adulterated with either GLD or ERLD, to be distinguished from those adulterated with chicken fat (CF). However, DSC provided a better means for identification of lard, with a detection limit of 1%. Elsevier 2002 Article PeerReviewed Marikkar, J.M.N and Lai, O.M and Ghazali, H.M and Che Man, Y.B (2002) Compositional and thermal analysis of RBD palm oil adulterated with lipase-catalyzed interesterified lard. Food Chemistry, 76 (2). pp. 249-258. ISSN 0308-8146; eISSN: 1873-7072 https://linkinghub.elsevier.com/retrieve/pii/S0308814601002576 10.1016/s0308-8146(01)00257-6
spellingShingle Marikkar, J.M.N
Lai, O.M
Ghazali, H.M
Che Man, Y.B
Compositional and thermal analysis of RBD palm oil adulterated with lipase-catalyzed interesterified lard
title Compositional and thermal analysis of RBD palm oil adulterated with lipase-catalyzed interesterified lard
title_full Compositional and thermal analysis of RBD palm oil adulterated with lipase-catalyzed interesterified lard
title_fullStr Compositional and thermal analysis of RBD palm oil adulterated with lipase-catalyzed interesterified lard
title_full_unstemmed Compositional and thermal analysis of RBD palm oil adulterated with lipase-catalyzed interesterified lard
title_short Compositional and thermal analysis of RBD palm oil adulterated with lipase-catalyzed interesterified lard
title_sort compositional and thermal analysis of rbd palm oil adulterated with lipase-catalyzed interesterified lard
url http://psasir.upm.edu.my/id/eprint/112492/
http://psasir.upm.edu.my/id/eprint/112492/
http://psasir.upm.edu.my/id/eprint/112492/