Synthesis and properties of Layered Organic–inorganic Hybrid Material: Zn-Al Layered Double Hydroxide–dioctyl Sulfosuccinate Nanocomposite
A layered organic-inorganic hybrid nanocomposite was prepared by using a surfactant, dioctyl sulphosuccinate (DSS) as a guest in Zn-Al layered double hydroxide (LDH) inorganic host by a self-assembly technique. The ZnAl ratio of the mother liquor was kept constant at 4 at the beginning of the synthe...
| Main Authors: | , |
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| Format: | Article |
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Springer
2000
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| Online Access: | http://psasir.upm.edu.my/id/eprint/112415/ |
| _version_ | 1848865936980836352 |
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| author | Hussein, Mohd Zobir Hwa, Tan Kim |
| author_facet | Hussein, Mohd Zobir Hwa, Tan Kim |
| author_sort | Hussein, Mohd Zobir |
| building | UPM Institutional Repository |
| collection | Online Access |
| description | A layered organic-inorganic hybrid nanocomposite was prepared by using a surfactant, dioctyl sulphosuccinate (DSS) as a guest in Zn-Al layered double hydroxide (LDH) inorganic host by a self-assembly technique. The ZnAl ratio of the mother liquor was kept constant at 4 at the beginning of the synthesis. Powder X-ray diffractogram shows that the basal spacing of the Zn-Al LDH with sulphate as the intergallery anion (ZASUL) expanded from 11.0 to 26.3 Å to accommodate the DSS surfactant anion for the formation of the Zn-Al LDH-DSS layered organicinorganic hybrid nanocomposite (ZADON). It was also found that the BET surface area reduced by about 90%, from 22.5 to 2.2 m2/g, for ZASUL and ZADON, respectively if 0. 1 M DSS was used for the synthesis of the latter. |
| first_indexed | 2025-11-15T14:12:38Z |
| format | Article |
| id | upm-112415 |
| institution | Universiti Putra Malaysia |
| institution_category | Local University |
| last_indexed | 2025-11-15T14:12:38Z |
| publishDate | 2000 |
| publisher | Springer |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | upm-1124152025-02-19T07:10:12Z http://psasir.upm.edu.my/id/eprint/112415/ Synthesis and properties of Layered Organic–inorganic Hybrid Material: Zn-Al Layered Double Hydroxide–dioctyl Sulfosuccinate Nanocomposite Hussein, Mohd Zobir Hwa, Tan Kim A layered organic-inorganic hybrid nanocomposite was prepared by using a surfactant, dioctyl sulphosuccinate (DSS) as a guest in Zn-Al layered double hydroxide (LDH) inorganic host by a self-assembly technique. The ZnAl ratio of the mother liquor was kept constant at 4 at the beginning of the synthesis. Powder X-ray diffractogram shows that the basal spacing of the Zn-Al LDH with sulphate as the intergallery anion (ZASUL) expanded from 11.0 to 26.3 Å to accommodate the DSS surfactant anion for the formation of the Zn-Al LDH-DSS layered organicinorganic hybrid nanocomposite (ZADON). It was also found that the BET surface area reduced by about 90%, from 22.5 to 2.2 m2/g, for ZASUL and ZADON, respectively if 0. 1 M DSS was used for the synthesis of the latter. Springer 2000 Article PeerReviewed Hussein, Mohd Zobir and Hwa, Tan Kim (2000) Synthesis and properties of Layered Organic–inorganic Hybrid Material: Zn-Al Layered Double Hydroxide–dioctyl Sulfosuccinate Nanocomposite. Journal of Nanoparticle Research, 2 (3). pp. 293-298. ISSN 1388-0764; eISSN: 1572-896X https://link.springer.com/article/10.1023/A:1010013201391?error=cookies_not_supported&code=f0c12066-0b34-4ba9-a35c-f7390267c961 10.1023/a:1010013201391 |
| spellingShingle | Hussein, Mohd Zobir Hwa, Tan Kim Synthesis and properties of Layered Organic–inorganic Hybrid Material: Zn-Al Layered Double Hydroxide–dioctyl Sulfosuccinate Nanocomposite |
| title | Synthesis and properties of Layered Organic–inorganic Hybrid Material: Zn-Al Layered Double Hydroxide–dioctyl Sulfosuccinate Nanocomposite |
| title_full | Synthesis and properties of Layered Organic–inorganic Hybrid Material: Zn-Al Layered Double Hydroxide–dioctyl Sulfosuccinate Nanocomposite |
| title_fullStr | Synthesis and properties of Layered Organic–inorganic Hybrid Material: Zn-Al Layered Double Hydroxide–dioctyl Sulfosuccinate Nanocomposite |
| title_full_unstemmed | Synthesis and properties of Layered Organic–inorganic Hybrid Material: Zn-Al Layered Double Hydroxide–dioctyl Sulfosuccinate Nanocomposite |
| title_short | Synthesis and properties of Layered Organic–inorganic Hybrid Material: Zn-Al Layered Double Hydroxide–dioctyl Sulfosuccinate Nanocomposite |
| title_sort | synthesis and properties of layered organic–inorganic hybrid material: zn-al layered double hydroxide–dioctyl sulfosuccinate nanocomposite |
| url | http://psasir.upm.edu.my/id/eprint/112415/ http://psasir.upm.edu.my/id/eprint/112415/ http://psasir.upm.edu.my/id/eprint/112415/ |