N-Doped rGO-like carbon prepared from coconut shell: structure and specific capacitance

An rGO−like carbon compound has been synthesized from biomass, i.e., old coconut shell, by a carbonization process followed by heating at 400°C for 5 h. The nitrogen doping was achieved by adding the urea (CH4N2O) and stirring at 70°C for 14 h. The morphology and structure of the rGO-like carbon wer...

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Main Authors: Khambali, Imam, Priyanto, Budhi, Asih, Retno, Anjelh Baqiya, Malik, Mahyiddin Ramli, Muhammad, Huda Osman, Nurul, Tunmee, Sarayut, Nakajima, Hideki, Triwikantoro, ., Zainuri, Mochamad, Darminto, .
Format: Article
Published: Tech Science Press 2022
Online Access:http://psasir.upm.edu.my/id/eprint/108642/
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author Khambali, Imam
Priyanto, Budhi
Asih, Retno
Anjelh Baqiya, Malik
Mahyiddin Ramli, Muhammad
Huda Osman, Nurul
Tunmee, Sarayut
Nakajima, Hideki
Triwikantoro, .
Zainuri, Mochamad
Darminto, .
author_facet Khambali, Imam
Priyanto, Budhi
Asih, Retno
Anjelh Baqiya, Malik
Mahyiddin Ramli, Muhammad
Huda Osman, Nurul
Tunmee, Sarayut
Nakajima, Hideki
Triwikantoro, .
Zainuri, Mochamad
Darminto, .
author_sort Khambali, Imam
building UPM Institutional Repository
collection Online Access
description An rGO−like carbon compound has been synthesized from biomass, i.e., old coconut shell, by a carbonization process followed by heating at 400°C for 5 h. The nitrogen doping was achieved by adding the urea (CH4N2O) and stirring at 70°C for 14 h. The morphology and structure of the rGO-like carbon were investigated by electron microscopies and Raman spectroscopy. The presence of C-N functional groups was analyzed by Fourier transform infrared and synchrotron X-ray photoemission spectroscopy, while the particle and the specific capacitance were measured by particle sizer and cyclic voltammetry. The highest specific capacitance of 72.78 F/g is achieved by the sample with 20 urea, having the smallest particles size and the largest surface area. The corresponding sample has shown to be constituted by the appropriate amount of C–N pyrrolic and pyridinic defects.
first_indexed 2025-11-15T14:00:42Z
format Article
id upm-108642
institution Universiti Putra Malaysia
institution_category Local University
last_indexed 2025-11-15T14:00:42Z
publishDate 2022
publisher Tech Science Press
recordtype eprints
repository_type Digital Repository
spelling upm-1086422024-09-26T08:11:37Z http://psasir.upm.edu.my/id/eprint/108642/ N-Doped rGO-like carbon prepared from coconut shell: structure and specific capacitance Khambali, Imam Priyanto, Budhi Asih, Retno Anjelh Baqiya, Malik Mahyiddin Ramli, Muhammad Huda Osman, Nurul Tunmee, Sarayut Nakajima, Hideki Triwikantoro, . Zainuri, Mochamad Darminto, . An rGO−like carbon compound has been synthesized from biomass, i.e., old coconut shell, by a carbonization process followed by heating at 400°C for 5 h. The nitrogen doping was achieved by adding the urea (CH4N2O) and stirring at 70°C for 14 h. The morphology and structure of the rGO-like carbon were investigated by electron microscopies and Raman spectroscopy. The presence of C-N functional groups was analyzed by Fourier transform infrared and synchrotron X-ray photoemission spectroscopy, while the particle and the specific capacitance were measured by particle sizer and cyclic voltammetry. The highest specific capacitance of 72.78 F/g is achieved by the sample with 20 urea, having the smallest particles size and the largest surface area. The corresponding sample has shown to be constituted by the appropriate amount of C–N pyrrolic and pyridinic defects. Tech Science Press 2022-12-01 Article PeerReviewed Khambali, Imam and Priyanto, Budhi and Asih, Retno and Anjelh Baqiya, Malik and Mahyiddin Ramli, Muhammad and Huda Osman, Nurul and Tunmee, Sarayut and Nakajima, Hideki and Triwikantoro, . and Zainuri, Mochamad and Darminto, . (2022) N-Doped rGO-like carbon prepared from coconut shell: structure and specific capacitance. Journal of Renewable Materials, 11 (4). 1823 - 1833. ISSN 2164-6325; ESSN: 2164-6341 https://www.techscience.com/jrm/v11n4/50690 10.32604/jrm.2023.025026
spellingShingle Khambali, Imam
Priyanto, Budhi
Asih, Retno
Anjelh Baqiya, Malik
Mahyiddin Ramli, Muhammad
Huda Osman, Nurul
Tunmee, Sarayut
Nakajima, Hideki
Triwikantoro, .
Zainuri, Mochamad
Darminto, .
N-Doped rGO-like carbon prepared from coconut shell: structure and specific capacitance
title N-Doped rGO-like carbon prepared from coconut shell: structure and specific capacitance
title_full N-Doped rGO-like carbon prepared from coconut shell: structure and specific capacitance
title_fullStr N-Doped rGO-like carbon prepared from coconut shell: structure and specific capacitance
title_full_unstemmed N-Doped rGO-like carbon prepared from coconut shell: structure and specific capacitance
title_short N-Doped rGO-like carbon prepared from coconut shell: structure and specific capacitance
title_sort n-doped rgo-like carbon prepared from coconut shell: structure and specific capacitance
url http://psasir.upm.edu.my/id/eprint/108642/
http://psasir.upm.edu.my/id/eprint/108642/
http://psasir.upm.edu.my/id/eprint/108642/