Modelling pellet size and shape evolution during the breakage stage in spheronisation

In the breakage stage of extrusion-spheronisation, initially cylindrical extrudates undergo simultaneous breakage and rounding on a rotating friction plate. This sets the starting conditions (number of pellets, size and shape distributions) for the subsequent, lengthy, rounding stage. The simultaneo...

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Main Authors: Whelan-Smith, J., How, M. S., Rough, S. L., Wang, L., Wilson, D. I.
Format: Article
Language:English
Published: Elsevier BV 2024
Online Access:http://psasir.upm.edu.my/id/eprint/106093/
http://psasir.upm.edu.my/id/eprint/106093/1/1-s2.0-S0032591024001074-main.pdf
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author Whelan-Smith, J.
How, M. S.
Rough, S. L.
Wang, L.
Wilson, D. I.
author_facet Whelan-Smith, J.
How, M. S.
Rough, S. L.
Wang, L.
Wilson, D. I.
author_sort Whelan-Smith, J.
building UPM Institutional Repository
collection Online Access
description In the breakage stage of extrusion-spheronisation, initially cylindrical extrudates undergo simultaneous breakage and rounding on a rotating friction plate. This sets the starting conditions (number of pellets, size and shape distributions) for the subsequent, lengthy, rounding stage. The simultaneous evolution of pellet size and shape during the initial stages of spheronisation has not been considered in depth. Wang et al. (2021) AIChEJ, 67(6), e17247 investigated the breakage of 2 mm diameter microcrystalline cellulose/water extrudates and modelled the evolution of length using a 1-D population balance model. Here the data (over 17,000 images) were reanalysed and classified by both length and shape (8 shape classes). Their model was extended to 2-D (tracking size and shape), and the data fitted by a combination of optimization approaches. The effect of pellet length on the likelihood of breakage over rounding, and the influence of plate rotation speed and initial number of extrudates, is reported.
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institution Universiti Putra Malaysia
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spelling upm-1060932024-10-03T04:49:59Z http://psasir.upm.edu.my/id/eprint/106093/ Modelling pellet size and shape evolution during the breakage stage in spheronisation Whelan-Smith, J. How, M. S. Rough, S. L. Wang, L. Wilson, D. I. In the breakage stage of extrusion-spheronisation, initially cylindrical extrudates undergo simultaneous breakage and rounding on a rotating friction plate. This sets the starting conditions (number of pellets, size and shape distributions) for the subsequent, lengthy, rounding stage. The simultaneous evolution of pellet size and shape during the initial stages of spheronisation has not been considered in depth. Wang et al. (2021) AIChEJ, 67(6), e17247 investigated the breakage of 2 mm diameter microcrystalline cellulose/water extrudates and modelled the evolution of length using a 1-D population balance model. Here the data (over 17,000 images) were reanalysed and classified by both length and shape (8 shape classes). Their model was extended to 2-D (tracking size and shape), and the data fitted by a combination of optimization approaches. The effect of pellet length on the likelihood of breakage over rounding, and the influence of plate rotation speed and initial number of extrudates, is reported. Elsevier BV 2024 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/106093/1/1-s2.0-S0032591024001074-main.pdf Whelan-Smith, J. and How, M. S. and Rough, S. L. and Wang, L. and Wilson, D. I. (2024) Modelling pellet size and shape evolution during the breakage stage in spheronisation. Powder Technology, 436. art. no. 119465. pp. 1-17. ISSN 0032-5910; ESSN: 1873-328X https://www.sciencedirect.com/science/article/pii/S0032591024001074 10.1016/j.powtec.2024.119465
spellingShingle Whelan-Smith, J.
How, M. S.
Rough, S. L.
Wang, L.
Wilson, D. I.
Modelling pellet size and shape evolution during the breakage stage in spheronisation
title Modelling pellet size and shape evolution during the breakage stage in spheronisation
title_full Modelling pellet size and shape evolution during the breakage stage in spheronisation
title_fullStr Modelling pellet size and shape evolution during the breakage stage in spheronisation
title_full_unstemmed Modelling pellet size and shape evolution during the breakage stage in spheronisation
title_short Modelling pellet size and shape evolution during the breakage stage in spheronisation
title_sort modelling pellet size and shape evolution during the breakage stage in spheronisation
url http://psasir.upm.edu.my/id/eprint/106093/
http://psasir.upm.edu.my/id/eprint/106093/
http://psasir.upm.edu.my/id/eprint/106093/
http://psasir.upm.edu.my/id/eprint/106093/1/1-s2.0-S0032591024001074-main.pdf