N-Doped rGO-sike carbon prepared from coconut shell: structure and specific capacitance

An rGO−like carbon compound has been synthesized from biomass, i.e., old coconut shell, by a carbonization process followed by heating at 400°C for 5 h. The nitrogen doping was achieved by adding the urea (CH4N2O) and stirring at 70°C for 14 h. The morphology and structure of the rGO-like carbon wer...

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Main Authors: Khambali, Imam, Priyanto, Budhi, Asih, Retno, Baqiya, Malik Anjelh, Ramli, Muhammad Mahyiddin, Osman, Nurul Huda, Tunmee, Sarayut, Nakajima, Hideki, Triwikantoro, Zainuri, Mochamad, Darminto
Format: Article
Published: Tech Science Press 2022
Online Access:http://psasir.upm.edu.my/id/eprint/102294/
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author Khambali, Imam
Priyanto, Budhi
Asih, Retno
Baqiya, Malik Anjelh
Ramli, Muhammad Mahyiddin
Osman, Nurul Huda
Tunmee, Sarayut
Nakajima, Hideki
Triwikantoro
Zainuri, Mochamad
Darminto
author_facet Khambali, Imam
Priyanto, Budhi
Asih, Retno
Baqiya, Malik Anjelh
Ramli, Muhammad Mahyiddin
Osman, Nurul Huda
Tunmee, Sarayut
Nakajima, Hideki
Triwikantoro
Zainuri, Mochamad
Darminto
author_sort Khambali, Imam
building UPM Institutional Repository
collection Online Access
description An rGO−like carbon compound has been synthesized from biomass, i.e., old coconut shell, by a carbonization process followed by heating at 400°C for 5 h. The nitrogen doping was achieved by adding the urea (CH4N2O) and stirring at 70°C for 14 h. The morphology and structure of the rGO-like carbon were investigated by electron microscopies and Raman spectroscopy. The presence of C-N functional groups was analyzed by Fourier transform infrared and synchrotron X-ray photoemission spectroscopy, while the particle and the specific capacitance were measured by particle sizer and cyclic voltammetry. The highest specific capacitance of 72.78 F/g is achieved by the sample with 20% urea, having the smallest particles size and the largest surface area. The corresponding sample has shown to be constituted by the appropriate amount of C–N pyrrolic and pyridinic defects.
first_indexed 2025-11-15T13:38:08Z
format Article
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institution Universiti Putra Malaysia
institution_category Local University
last_indexed 2025-11-15T13:38:08Z
publishDate 2022
publisher Tech Science Press
recordtype eprints
repository_type Digital Repository
spelling upm-1022942023-07-10T00:35:57Z http://psasir.upm.edu.my/id/eprint/102294/ N-Doped rGO-sike carbon prepared from coconut shell: structure and specific capacitance Khambali, Imam Priyanto, Budhi Asih, Retno Baqiya, Malik Anjelh Ramli, Muhammad Mahyiddin Osman, Nurul Huda Tunmee, Sarayut Nakajima, Hideki Triwikantoro Zainuri, Mochamad Darminto An rGO−like carbon compound has been synthesized from biomass, i.e., old coconut shell, by a carbonization process followed by heating at 400°C for 5 h. The nitrogen doping was achieved by adding the urea (CH4N2O) and stirring at 70°C for 14 h. The morphology and structure of the rGO-like carbon were investigated by electron microscopies and Raman spectroscopy. The presence of C-N functional groups was analyzed by Fourier transform infrared and synchrotron X-ray photoemission spectroscopy, while the particle and the specific capacitance were measured by particle sizer and cyclic voltammetry. The highest specific capacitance of 72.78 F/g is achieved by the sample with 20% urea, having the smallest particles size and the largest surface area. The corresponding sample has shown to be constituted by the appropriate amount of C–N pyrrolic and pyridinic defects. Tech Science Press 2022-12-01 Article PeerReviewed Khambali, Imam and Priyanto, Budhi and Asih, Retno and Baqiya, Malik Anjelh and Ramli, Muhammad Mahyiddin and Osman, Nurul Huda and Tunmee, Sarayut and Nakajima, Hideki and Triwikantoro and Zainuri, Mochamad and Darminto (2022) N-Doped rGO-sike carbon prepared from coconut shell: structure and specific capacitance. Journal of Renewable Materials, 11 (4). pp. 1-11. ISSN 2164-6325; ESSN: 2164-6341 https://www.techscience.com/jrm/v11n4/50690 10.32604/jrm.2023.025026
spellingShingle Khambali, Imam
Priyanto, Budhi
Asih, Retno
Baqiya, Malik Anjelh
Ramli, Muhammad Mahyiddin
Osman, Nurul Huda
Tunmee, Sarayut
Nakajima, Hideki
Triwikantoro
Zainuri, Mochamad
Darminto
N-Doped rGO-sike carbon prepared from coconut shell: structure and specific capacitance
title N-Doped rGO-sike carbon prepared from coconut shell: structure and specific capacitance
title_full N-Doped rGO-sike carbon prepared from coconut shell: structure and specific capacitance
title_fullStr N-Doped rGO-sike carbon prepared from coconut shell: structure and specific capacitance
title_full_unstemmed N-Doped rGO-sike carbon prepared from coconut shell: structure and specific capacitance
title_short N-Doped rGO-sike carbon prepared from coconut shell: structure and specific capacitance
title_sort n-doped rgo-sike carbon prepared from coconut shell: structure and specific capacitance
url http://psasir.upm.edu.my/id/eprint/102294/
http://psasir.upm.edu.my/id/eprint/102294/
http://psasir.upm.edu.my/id/eprint/102294/