Enhanced critical current density of ex situ MgB2 via control of Mg assisted sintering

In this work, ex situ MgB2 was mixed with 0.5 mol of Mg and sintered. The sintering conditions were varied over a temperature range of 600–1000 °C for 1, 3, and 7 h, respectively. The addition of Mg during the sintering increased the partial pressure of Mg and thus suppressed the decomposition of Mg...

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Main Authors: Mohd Hapipi, Nurhidayah, Chen, Soo Kien, Shaari, Abdul Halim, Awang Kechik, Mohd Mustafa, Lim, Kean Pah, Tan, Kar Ban, Lee, Oon Jew, Arvapalli, Sai Srikanth, Miryala, Muralidhar
Format: Article
Published: Springer 2022
Online Access:http://psasir.upm.edu.my/id/eprint/101260/
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author Mohd Hapipi, Nurhidayah
Chen, Soo Kien
Shaari, Abdul Halim
Awang Kechik, Mohd Mustafa
Lim, Kean Pah
Tan, Kar Ban
Lee, Oon Jew
Arvapalli, Sai Srikanth
Miryala, Muralidhar
author_facet Mohd Hapipi, Nurhidayah
Chen, Soo Kien
Shaari, Abdul Halim
Awang Kechik, Mohd Mustafa
Lim, Kean Pah
Tan, Kar Ban
Lee, Oon Jew
Arvapalli, Sai Srikanth
Miryala, Muralidhar
author_sort Mohd Hapipi, Nurhidayah
building UPM Institutional Repository
collection Online Access
description In this work, ex situ MgB2 was mixed with 0.5 mol of Mg and sintered. The sintering conditions were varied over a temperature range of 600–1000 °C for 1, 3, and 7 h, respectively. The addition of Mg during the sintering increased the partial pressure of Mg and thus suppressed the decomposition of MgB2. Onset of critical temperature, Tc, was retained at ∼ 38 K even after the addition of Mg. By increasing the sintering temperature, magnetic critical current density, Jc at self-field, and 20 K of the ex situ samples increased consistently. With the addition of Mg for 1 h sintering, self-field Jc (20 K) was enhanced more than 20 times to 104 A cm−2 as the sintering temperature was increased. Such significant enhancement in the Jc is mainly due to the improved grain coupling aided by Mg during the short sintering.
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institution Universiti Putra Malaysia
institution_category Local University
last_indexed 2025-11-15T13:34:17Z
publishDate 2022
publisher Springer
recordtype eprints
repository_type Digital Repository
spelling upm-1012602023-10-19T22:33:55Z http://psasir.upm.edu.my/id/eprint/101260/ Enhanced critical current density of ex situ MgB2 via control of Mg assisted sintering Mohd Hapipi, Nurhidayah Chen, Soo Kien Shaari, Abdul Halim Awang Kechik, Mohd Mustafa Lim, Kean Pah Tan, Kar Ban Lee, Oon Jew Arvapalli, Sai Srikanth Miryala, Muralidhar In this work, ex situ MgB2 was mixed with 0.5 mol of Mg and sintered. The sintering conditions were varied over a temperature range of 600–1000 °C for 1, 3, and 7 h, respectively. The addition of Mg during the sintering increased the partial pressure of Mg and thus suppressed the decomposition of MgB2. Onset of critical temperature, Tc, was retained at ∼ 38 K even after the addition of Mg. By increasing the sintering temperature, magnetic critical current density, Jc at self-field, and 20 K of the ex situ samples increased consistently. With the addition of Mg for 1 h sintering, self-field Jc (20 K) was enhanced more than 20 times to 104 A cm−2 as the sintering temperature was increased. Such significant enhancement in the Jc is mainly due to the improved grain coupling aided by Mg during the short sintering. Springer 2022-03-30 Article PeerReviewed Mohd Hapipi, Nurhidayah and Chen, Soo Kien and Shaari, Abdul Halim and Awang Kechik, Mohd Mustafa and Lim, Kean Pah and Tan, Kar Ban and Lee, Oon Jew and Arvapalli, Sai Srikanth and Miryala, Muralidhar (2022) Enhanced critical current density of ex situ MgB2 via control of Mg assisted sintering. Journal of Materials Science: Materials in Electronics, 33. 11257 - 11268. ISSN 0957-4522; ESSN: 1573-482X https://link.springer.com/article/10.1007/s10854-022-08101-3#:~:text=In%20this%20work%2C%20ex%20situ,the%20decomposition%20of%20MgB2. 10.1007/s10854-022-08101-3
spellingShingle Mohd Hapipi, Nurhidayah
Chen, Soo Kien
Shaari, Abdul Halim
Awang Kechik, Mohd Mustafa
Lim, Kean Pah
Tan, Kar Ban
Lee, Oon Jew
Arvapalli, Sai Srikanth
Miryala, Muralidhar
Enhanced critical current density of ex situ MgB2 via control of Mg assisted sintering
title Enhanced critical current density of ex situ MgB2 via control of Mg assisted sintering
title_full Enhanced critical current density of ex situ MgB2 via control of Mg assisted sintering
title_fullStr Enhanced critical current density of ex situ MgB2 via control of Mg assisted sintering
title_full_unstemmed Enhanced critical current density of ex situ MgB2 via control of Mg assisted sintering
title_short Enhanced critical current density of ex situ MgB2 via control of Mg assisted sintering
title_sort enhanced critical current density of ex situ mgb2 via control of mg assisted sintering
url http://psasir.upm.edu.my/id/eprint/101260/
http://psasir.upm.edu.my/id/eprint/101260/
http://psasir.upm.edu.my/id/eprint/101260/