Effect of V-type crystallinity and starch particle structure on the oil loading capacity and anti-oxidation

Starch-based carriers have a great potential in functional oil encapsulation because of their mild preparation conditions, but the oil loading capacity and underlying anti-oxidation mechanism remain unclear. Here V-type starches were applied to fabricate flaxseed oil powder. Particle size analysis a...

Full description

Bibliographic Details
Main Authors: Wu, Chenbei, Junejo, Shahid Ahmed, Zhang, Bin, Fu, Xiong, Tan, Chin Ping, Huang, Qiang
Format: Article
Published: Elsevier 2022
Online Access:http://psasir.upm.edu.my/id/eprint/101153/
_version_ 1848863505765105664
author Wu, Chenbei
Junejo, Shahid Ahmed
Zhang, Bin
Fu, Xiong
Tan, Chin Ping
Huang, Qiang
author_facet Wu, Chenbei
Junejo, Shahid Ahmed
Zhang, Bin
Fu, Xiong
Tan, Chin Ping
Huang, Qiang
author_sort Wu, Chenbei
building UPM Institutional Repository
collection Online Access
description Starch-based carriers have a great potential in functional oil encapsulation because of their mild preparation conditions, but the oil loading capacity and underlying anti-oxidation mechanism remain unclear. Here V-type starches were applied to fabricate flaxseed oil powder. Particle size analysis and scanning electron microscopy showed a loose aggregation microstructure of normal maize starch (NMS) prepared using the anti-solvent (AS) precipitation method, with an average size of 24.9 μm. Differential scanning calorimetry displayed a good thermo-oxidation resistance of NMS-derived V-type starch prepared via AS precipitation. Principal component analysis revealed that the oil loading capacity, related closely to V-type crystallinity and D50, has a significant positive correlation with the onset oxidation temperature and a negative correlation with the peroxide, thiobarbituric acid, and ρ-anisidine values. Our original study reveals the effects of V-type crystallinity and aggregation microstructure on the oil loading capacity and anti-oxidation, providing theoretical guidance for developing novel, starch-based carriers.
first_indexed 2025-11-15T13:33:59Z
format Article
id upm-101153
institution Universiti Putra Malaysia
institution_category Local University
last_indexed 2025-11-15T13:33:59Z
publishDate 2022
publisher Elsevier
recordtype eprints
repository_type Digital Repository
spelling upm-1011532024-04-22T03:02:09Z http://psasir.upm.edu.my/id/eprint/101153/ Effect of V-type crystallinity and starch particle structure on the oil loading capacity and anti-oxidation Wu, Chenbei Junejo, Shahid Ahmed Zhang, Bin Fu, Xiong Tan, Chin Ping Huang, Qiang Starch-based carriers have a great potential in functional oil encapsulation because of their mild preparation conditions, but the oil loading capacity and underlying anti-oxidation mechanism remain unclear. Here V-type starches were applied to fabricate flaxseed oil powder. Particle size analysis and scanning electron microscopy showed a loose aggregation microstructure of normal maize starch (NMS) prepared using the anti-solvent (AS) precipitation method, with an average size of 24.9 μm. Differential scanning calorimetry displayed a good thermo-oxidation resistance of NMS-derived V-type starch prepared via AS precipitation. Principal component analysis revealed that the oil loading capacity, related closely to V-type crystallinity and D50, has a significant positive correlation with the onset oxidation temperature and a negative correlation with the peroxide, thiobarbituric acid, and ρ-anisidine values. Our original study reveals the effects of V-type crystallinity and aggregation microstructure on the oil loading capacity and anti-oxidation, providing theoretical guidance for developing novel, starch-based carriers. Elsevier 2022 Article PeerReviewed Wu, Chenbei and Junejo, Shahid Ahmed and Zhang, Bin and Fu, Xiong and Tan, Chin Ping and Huang, Qiang (2022) Effect of V-type crystallinity and starch particle structure on the oil loading capacity and anti-oxidation. Carbohydrate Polymers, 297. art. no. 120015. pp. 1-11. ISSN 0144-8617 https://www.sciencedirect.com/science/article/pii/S0144861722009201 10.1016/j.carbpol.2022.120015
spellingShingle Wu, Chenbei
Junejo, Shahid Ahmed
Zhang, Bin
Fu, Xiong
Tan, Chin Ping
Huang, Qiang
Effect of V-type crystallinity and starch particle structure on the oil loading capacity and anti-oxidation
title Effect of V-type crystallinity and starch particle structure on the oil loading capacity and anti-oxidation
title_full Effect of V-type crystallinity and starch particle structure on the oil loading capacity and anti-oxidation
title_fullStr Effect of V-type crystallinity and starch particle structure on the oil loading capacity and anti-oxidation
title_full_unstemmed Effect of V-type crystallinity and starch particle structure on the oil loading capacity and anti-oxidation
title_short Effect of V-type crystallinity and starch particle structure on the oil loading capacity and anti-oxidation
title_sort effect of v-type crystallinity and starch particle structure on the oil loading capacity and anti-oxidation
url http://psasir.upm.edu.my/id/eprint/101153/
http://psasir.upm.edu.my/id/eprint/101153/
http://psasir.upm.edu.my/id/eprint/101153/