Determination of 16 EPA PAHs in food using gas and liquid chromatography

Polycyclic aromatic hydrocarbons (PAHs) in food are discussed in terms of their occurrence, legal limits, sample preparation, identification, and quantification. Recent approaches for optimizing the polycyclic aromatic hydrocarbons (PAHs) extraction from food or food-related products and the subsequ...

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Main Authors: Agus, Baizura Aya Putri, Rajentran, Komati, Selamat, Jinap, Shanti Dwita Lestari, Umar, Nasiru Bilkisu, Hussain, Norhayati
Format: Article
Published: Elsevier 2023
Online Access:http://psasir.upm.edu.my/id/eprint/100933/
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author Agus, Baizura Aya Putri
Rajentran, Komati
Selamat, Jinap
Shanti Dwita Lestari
Umar, Nasiru Bilkisu
Hussain, Norhayati
author_facet Agus, Baizura Aya Putri
Rajentran, Komati
Selamat, Jinap
Shanti Dwita Lestari
Umar, Nasiru Bilkisu
Hussain, Norhayati
author_sort Agus, Baizura Aya Putri
building UPM Institutional Repository
collection Online Access
description Polycyclic aromatic hydrocarbons (PAHs) in food are discussed in terms of their occurrence, legal limits, sample preparation, identification, and quantification. Recent approaches for optimizing the polycyclic aromatic hydrocarbons (PAHs) extraction from food or food-related products and the subsequent clean-up processes during sample preparation are highlighted in relation to the study's specific objectives. Basic information regarding the performances of analytical procedures for PAH quantification is also summarized. Gas chromatography (GC) and high-performance liquid chromatography (HPLC) coupled with mass spectrometry (MS), flame ionization detectors (FID), ultraviolet detectors (UV), and fluorescent detectors (FLD) are among the most widely used techniques for identifying and quantifying PAHs in food. The validation of the method’s performance such as linearity, the limit of detection (LOD), limit of quantification (LOQ), precision (repeatability, intermediate precision, and reproducibility), HORRAT values (Horratr and HorratR), accuracy (recovery) and measurement uncertainty are also briefly discussed.
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institution Universiti Putra Malaysia
institution_category Local University
last_indexed 2025-11-15T13:33:08Z
publishDate 2023
publisher Elsevier
recordtype eprints
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spelling upm-1009332023-07-13T08:39:02Z http://psasir.upm.edu.my/id/eprint/100933/ Determination of 16 EPA PAHs in food using gas and liquid chromatography Agus, Baizura Aya Putri Rajentran, Komati Selamat, Jinap Shanti Dwita Lestari Umar, Nasiru Bilkisu Hussain, Norhayati Polycyclic aromatic hydrocarbons (PAHs) in food are discussed in terms of their occurrence, legal limits, sample preparation, identification, and quantification. Recent approaches for optimizing the polycyclic aromatic hydrocarbons (PAHs) extraction from food or food-related products and the subsequent clean-up processes during sample preparation are highlighted in relation to the study's specific objectives. Basic information regarding the performances of analytical procedures for PAH quantification is also summarized. Gas chromatography (GC) and high-performance liquid chromatography (HPLC) coupled with mass spectrometry (MS), flame ionization detectors (FID), ultraviolet detectors (UV), and fluorescent detectors (FLD) are among the most widely used techniques for identifying and quantifying PAHs in food. The validation of the method’s performance such as linearity, the limit of detection (LOD), limit of quantification (LOQ), precision (repeatability, intermediate precision, and reproducibility), HORRAT values (Horratr and HorratR), accuracy (recovery) and measurement uncertainty are also briefly discussed. Elsevier 2023-03 Article PeerReviewed Agus, Baizura Aya Putri and Rajentran, Komati and Selamat, Jinap and Shanti Dwita Lestari and Umar, Nasiru Bilkisu and Hussain, Norhayati (2023) Determination of 16 EPA PAHs in food using gas and liquid chromatography. Journal of Food Composition and Analysis, 116. art. no. 105038. pp. 1-13. ISSN 0889-1575 https://www.sciencedirect.com/science/article/pii/S0889157522006561 10.1016/j.jfca.2022.105038
spellingShingle Agus, Baizura Aya Putri
Rajentran, Komati
Selamat, Jinap
Shanti Dwita Lestari
Umar, Nasiru Bilkisu
Hussain, Norhayati
Determination of 16 EPA PAHs in food using gas and liquid chromatography
title Determination of 16 EPA PAHs in food using gas and liquid chromatography
title_full Determination of 16 EPA PAHs in food using gas and liquid chromatography
title_fullStr Determination of 16 EPA PAHs in food using gas and liquid chromatography
title_full_unstemmed Determination of 16 EPA PAHs in food using gas and liquid chromatography
title_short Determination of 16 EPA PAHs in food using gas and liquid chromatography
title_sort determination of 16 epa pahs in food using gas and liquid chromatography
url http://psasir.upm.edu.my/id/eprint/100933/
http://psasir.upm.edu.my/id/eprint/100933/
http://psasir.upm.edu.my/id/eprint/100933/