Cytotoxic constituent of Melicope latifolia (DC.) T. G. Hartley

An undescribed conjugated sesquiterpene, amelicarin (1), together with nine known compounds (2–10) were isolated for the first time from Melicope latifolia. Their structures were elucidated by extensive NMR spectroscopic and mass spectrometric methods. The conjugated sesquiterpene possesses a unique...

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Main Authors: Lim, Pei Cee, Ali, Zulfiqar, Khan, Ikhlas A., Khan, Shabana I., Kassim, Nur Kartinee, Awang, Khalijah, Shaari, Khozirah, Ismail, Amin
Format: Article
Published: Taylor and Francis 2022
Online Access:http://psasir.upm.edu.my/id/eprint/100866/
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author Lim, Pei Cee
Ali, Zulfiqar
Khan, Ikhlas A.
Khan, Shabana I.
Kassim, Nur Kartinee
Awang, Khalijah
Shaari, Khozirah
Ismail, Amin
author_facet Lim, Pei Cee
Ali, Zulfiqar
Khan, Ikhlas A.
Khan, Shabana I.
Kassim, Nur Kartinee
Awang, Khalijah
Shaari, Khozirah
Ismail, Amin
author_sort Lim, Pei Cee
building UPM Institutional Repository
collection Online Access
description An undescribed conjugated sesquiterpene, amelicarin (1), together with nine known compounds (2–10) were isolated for the first time from Melicope latifolia. Their structures were elucidated by extensive NMR spectroscopic and mass spectrometric methods. The conjugated sesquiterpene possesses a unique 6/6/9/4-ring fused tetracyclic skeleton. The proposed biosynthesis pathway of 1 consist of three reactions steps: (1) polyketide formation, (2) cyclisation and (3) addition to form the conjugated sesquiterpenoid as final metabolite. Out of the ten isolated metabolites, amelicarin (1) showed activity against 4 cancerous cell lines namely SK-MEL skin cancer, KB oral cancer, BT-549 breast cancer, and SK-OV-3 ovarian cancer with IC50 values between 15 and 25 µg/mL.
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institution Universiti Putra Malaysia
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last_indexed 2025-11-15T13:32:51Z
publishDate 2022
publisher Taylor and Francis
recordtype eprints
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spelling upm-1008662023-08-17T04:21:57Z http://psasir.upm.edu.my/id/eprint/100866/ Cytotoxic constituent of Melicope latifolia (DC.) T. G. Hartley Lim, Pei Cee Ali, Zulfiqar Khan, Ikhlas A. Khan, Shabana I. Kassim, Nur Kartinee Awang, Khalijah Shaari, Khozirah Ismail, Amin An undescribed conjugated sesquiterpene, amelicarin (1), together with nine known compounds (2–10) were isolated for the first time from Melicope latifolia. Their structures were elucidated by extensive NMR spectroscopic and mass spectrometric methods. The conjugated sesquiterpene possesses a unique 6/6/9/4-ring fused tetracyclic skeleton. The proposed biosynthesis pathway of 1 consist of three reactions steps: (1) polyketide formation, (2) cyclisation and (3) addition to form the conjugated sesquiterpenoid as final metabolite. Out of the ten isolated metabolites, amelicarin (1) showed activity against 4 cancerous cell lines namely SK-MEL skin cancer, KB oral cancer, BT-549 breast cancer, and SK-OV-3 ovarian cancer with IC50 values between 15 and 25 µg/mL. Taylor and Francis 2022-02-12 Article PeerReviewed Lim, Pei Cee and Ali, Zulfiqar and Khan, Ikhlas A. and Khan, Shabana I. and Kassim, Nur Kartinee and Awang, Khalijah and Shaari, Khozirah and Ismail, Amin (2022) Cytotoxic constituent of Melicope latifolia (DC.) T. G. Hartley. Natural Product Research, 36 (6). 1416 - 1424. ISSN 1478-6419; ESSN: 1478-6427 https://www.tandfonline.com/doi/abs/10.1080/14786419.2021.1885031 10.1080/14786419.2021.1885031
spellingShingle Lim, Pei Cee
Ali, Zulfiqar
Khan, Ikhlas A.
Khan, Shabana I.
Kassim, Nur Kartinee
Awang, Khalijah
Shaari, Khozirah
Ismail, Amin
Cytotoxic constituent of Melicope latifolia (DC.) T. G. Hartley
title Cytotoxic constituent of Melicope latifolia (DC.) T. G. Hartley
title_full Cytotoxic constituent of Melicope latifolia (DC.) T. G. Hartley
title_fullStr Cytotoxic constituent of Melicope latifolia (DC.) T. G. Hartley
title_full_unstemmed Cytotoxic constituent of Melicope latifolia (DC.) T. G. Hartley
title_short Cytotoxic constituent of Melicope latifolia (DC.) T. G. Hartley
title_sort cytotoxic constituent of melicope latifolia (dc.) t. g. hartley
url http://psasir.upm.edu.my/id/eprint/100866/
http://psasir.upm.edu.my/id/eprint/100866/
http://psasir.upm.edu.my/id/eprint/100866/