Size Selective Synthesis of Superparamagnetic Nanoparticles in Thin Fluids under Continuous Flow Conditions

Continuous flow spinning disc processing (SDP), which has extremely rapid mixing under plug flow conditions, effective heat and mass transfer, allowing high throughput with low wastage solvent efficiency, is effective in gaining access to superparamagnetic Fe3O4 nanoparticles at room temperature. Th...

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Main Authors: Chin, Suk Fun, K., Swaminathan Iyer, Raston, Colin L., Saunders, Martin
Format: Article
Language:English
Published: WILEY-VCH Verlag GmbH & Co. 2008
Subjects:
Online Access:http://ir.unimas.my/id/eprint/9899/
http://ir.unimas.my/id/eprint/9899/1/Size%20Selective%20Synthesis%20of%20Superparamagnetic%20Nanoparticles%20in%20Thin%20Fluids%20under%20Continuous%20Flow%20Conditions%20%28abstract%29.pdf
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author Chin, Suk Fun
K., Swaminathan Iyer
Raston, Colin L.
Saunders, Martin
author_facet Chin, Suk Fun
K., Swaminathan Iyer
Raston, Colin L.
Saunders, Martin
author_sort Chin, Suk Fun
building UNIMAS Institutional Repository
collection Online Access
description Continuous flow spinning disc processing (SDP), which has extremely rapid mixing under plug flow conditions, effective heat and mass transfer, allowing high throughput with low wastage solvent efficiency, is effective in gaining access to superparamagnetic Fe3O4 nanoparticles at room temperature. These are formed by passing ammonia gas over a thin aqueous film of Fe2þ/3þ which is introduced through a jet feed close to the centre of a rapidly rotating disc (500 to 2500 rpm), the particle size being controlled with a narrow size distribution over the range 5 nm to 10 nm, and the material having very high saturation magnetizations, in the range 68–78 emu g-�1.
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publishDate 2008
publisher WILEY-VCH Verlag GmbH & Co.
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spelling unimas-98992016-04-14T01:24:56Z http://ir.unimas.my/id/eprint/9899/ Size Selective Synthesis of Superparamagnetic Nanoparticles in Thin Fluids under Continuous Flow Conditions Chin, Suk Fun K., Swaminathan Iyer Raston, Colin L. Saunders, Martin GE Environmental Sciences QD Chemistry Continuous flow spinning disc processing (SDP), which has extremely rapid mixing under plug flow conditions, effective heat and mass transfer, allowing high throughput with low wastage solvent efficiency, is effective in gaining access to superparamagnetic Fe3O4 nanoparticles at room temperature. These are formed by passing ammonia gas over a thin aqueous film of Fe2þ/3þ which is introduced through a jet feed close to the centre of a rapidly rotating disc (500 to 2500 rpm), the particle size being controlled with a narrow size distribution over the range 5 nm to 10 nm, and the material having very high saturation magnetizations, in the range 68–78 emu g-�1. WILEY-VCH Verlag GmbH & Co. 2008 Article NonPeerReviewed text en http://ir.unimas.my/id/eprint/9899/1/Size%20Selective%20Synthesis%20of%20Superparamagnetic%20Nanoparticles%20in%20Thin%20Fluids%20under%20Continuous%20Flow%20Conditions%20%28abstract%29.pdf Chin, Suk Fun and K., Swaminathan Iyer and Raston, Colin L. and Saunders, Martin (2008) Size Selective Synthesis of Superparamagnetic Nanoparticles in Thin Fluids under Continuous Flow Conditions. Advanced Functional Materials, 18 (6). pp. 922-927. ISSN 1616-3028 http://www.researchgate.net/publication/229862109_Size_Selective_Synthesis_of_Superparamagnetic_Nanoparticles_in_Thin_Fluids_under_Continuous_Flow_Conditions DOI: 10.1002/adfm.200701101
spellingShingle GE Environmental Sciences
QD Chemistry
Chin, Suk Fun
K., Swaminathan Iyer
Raston, Colin L.
Saunders, Martin
Size Selective Synthesis of Superparamagnetic Nanoparticles in Thin Fluids under Continuous Flow Conditions
title Size Selective Synthesis of Superparamagnetic Nanoparticles in Thin Fluids under Continuous Flow Conditions
title_full Size Selective Synthesis of Superparamagnetic Nanoparticles in Thin Fluids under Continuous Flow Conditions
title_fullStr Size Selective Synthesis of Superparamagnetic Nanoparticles in Thin Fluids under Continuous Flow Conditions
title_full_unstemmed Size Selective Synthesis of Superparamagnetic Nanoparticles in Thin Fluids under Continuous Flow Conditions
title_short Size Selective Synthesis of Superparamagnetic Nanoparticles in Thin Fluids under Continuous Flow Conditions
title_sort size selective synthesis of superparamagnetic nanoparticles in thin fluids under continuous flow conditions
topic GE Environmental Sciences
QD Chemistry
url http://ir.unimas.my/id/eprint/9899/
http://ir.unimas.my/id/eprint/9899/
http://ir.unimas.my/id/eprint/9899/
http://ir.unimas.my/id/eprint/9899/1/Size%20Selective%20Synthesis%20of%20Superparamagnetic%20Nanoparticles%20in%20Thin%20Fluids%20under%20Continuous%20Flow%20Conditions%20%28abstract%29.pdf