Coordination chemistry of organotin (IV) complexes with ono-donor ligands

Three organotin(IV) complexes of salicylaldehyde furoic acid hydrazone ligand (1) with RnSnCl4-n (n = 2, 3) have been synthesized in the presence of base in absolute methanol in 1:2:1 mole ratio (metal:base:ligand). Two organotin(IV) complexes of ligand (1) have also been synthesized in the presenc...

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Main Author: Mayuran, Perumal
Format: Final Year Project Report / IMRAD
Language:English
Published: Universiti Malaysia Sarawak, UNIMAS 2009
Subjects:
Online Access:http://ir.unimas.my/id/eprint/7707/
http://ir.unimas.my/id/eprint/7707/3/Coordination%20Chemistry%20of%20Organotin%20%28IV%29%20Complexes%20with%20ONO-Donor%20Ligands.pdf
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author Mayuran, Perumal
author_facet Mayuran, Perumal
author_sort Mayuran, Perumal
building UNIMAS Institutional Repository
collection Online Access
description Three organotin(IV) complexes of salicylaldehyde furoic acid hydrazone ligand (1) with RnSnCl4-n (n = 2, 3) have been synthesized in the presence of base in absolute methanol in 1:2:1 mole ratio (metal:base:ligand). Two organotin(IV) complexes of ligand (1) have also been synthesized in the presence of base in absolute methanol in 1:1:1 mole ratio (metal:base:ligand). Another three organotin(IV) complexes of 2-hydroxyacetophenone furoic acid hydrazone ligand (2) in 1:2:1 mole ratio (metal:base:ligand) have been synthesized using the same method. All organotin(IV) complexes (3-10) have been characterized by CHN analyses, UV-Visible and FTIR spectral analyses. Among them, ligand (2) and its organotin(IV) complex have also been studied by 1H NMR spectra. Spectral studies suggested that both the ligands (1-2) act as dinegative tridentate chelating agents in all the organotin(IV) complexes (3-10). Organotin(IV) complexes (3-5, 8-10) are non electrolytic in nature and are proposed to have five coordinated molecular geometry around the central tin(IV) atom whereas for the organotin(IV) complexes (6-7), they are electrolytic in nature and are proposed to have six coordinated molecular geometry around the central tin(IV) atom, respectively.
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institution Universiti Malaysia Sarawak
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language English
last_indexed 2025-11-15T06:19:55Z
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spelling unimas-77072023-09-11T03:38:58Z http://ir.unimas.my/id/eprint/7707/ Coordination chemistry of organotin (IV) complexes with ono-donor ligands Mayuran, Perumal QD Chemistry Three organotin(IV) complexes of salicylaldehyde furoic acid hydrazone ligand (1) with RnSnCl4-n (n = 2, 3) have been synthesized in the presence of base in absolute methanol in 1:2:1 mole ratio (metal:base:ligand). Two organotin(IV) complexes of ligand (1) have also been synthesized in the presence of base in absolute methanol in 1:1:1 mole ratio (metal:base:ligand). Another three organotin(IV) complexes of 2-hydroxyacetophenone furoic acid hydrazone ligand (2) in 1:2:1 mole ratio (metal:base:ligand) have been synthesized using the same method. All organotin(IV) complexes (3-10) have been characterized by CHN analyses, UV-Visible and FTIR spectral analyses. Among them, ligand (2) and its organotin(IV) complex have also been studied by 1H NMR spectra. Spectral studies suggested that both the ligands (1-2) act as dinegative tridentate chelating agents in all the organotin(IV) complexes (3-10). Organotin(IV) complexes (3-5, 8-10) are non electrolytic in nature and are proposed to have five coordinated molecular geometry around the central tin(IV) atom whereas for the organotin(IV) complexes (6-7), they are electrolytic in nature and are proposed to have six coordinated molecular geometry around the central tin(IV) atom, respectively. Universiti Malaysia Sarawak, UNIMAS 2009 Final Year Project Report / IMRAD NonPeerReviewed text en http://ir.unimas.my/id/eprint/7707/3/Coordination%20Chemistry%20of%20Organotin%20%28IV%29%20Complexes%20with%20ONO-Donor%20Ligands.pdf Mayuran, Perumal (2009) Coordination chemistry of organotin (IV) complexes with ono-donor ligands. [Final Year Project Report / IMRAD] (Unpublished)
spellingShingle QD Chemistry
Mayuran, Perumal
Coordination chemistry of organotin (IV) complexes with ono-donor ligands
title Coordination chemistry of organotin (IV) complexes with ono-donor ligands
title_full Coordination chemistry of organotin (IV) complexes with ono-donor ligands
title_fullStr Coordination chemistry of organotin (IV) complexes with ono-donor ligands
title_full_unstemmed Coordination chemistry of organotin (IV) complexes with ono-donor ligands
title_short Coordination chemistry of organotin (IV) complexes with ono-donor ligands
title_sort coordination chemistry of organotin (iv) complexes with ono-donor ligands
topic QD Chemistry
url http://ir.unimas.my/id/eprint/7707/
http://ir.unimas.my/id/eprint/7707/3/Coordination%20Chemistry%20of%20Organotin%20%28IV%29%20Complexes%20with%20ONO-Donor%20Ligands.pdf