Synthesis and characterizations of magnetic nanoparticles

Magnetic nanoparticles can be applied in various applications such as drug targeting and delivery, magnetic resonance imaging, electrochemical cells, capacitors and etc. However, these applications require narrow size distribution and uniform shape magnetic nanoparticles and the synthesis of these...

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Main Author: Tan, Ching Hong
Format: Final Year Project Report / IMRAD
Language:English
English
Published: Universiti Malaysia Sarawak, (UNIMAS) 2011
Subjects:
Online Access:http://ir.unimas.my/id/eprint/6440/
http://ir.unimas.my/id/eprint/6440/1/Ching%2824%20pgs%29.pdf
http://ir.unimas.my/id/eprint/6440/4/TAN%20CHING%20HONG.pdf
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author Tan, Ching Hong
author_facet Tan, Ching Hong
author_sort Tan, Ching Hong
building UNIMAS Institutional Repository
collection Online Access
description Magnetic nanoparticles can be applied in various applications such as drug targeting and delivery, magnetic resonance imaging, electrochemical cells, capacitors and etc. However, these applications require narrow size distribution and uniform shape magnetic nanoparticles and the synthesis of these magnetic nanoparticles often result in a broad size distribution. In present study, thermal decomposition method was adapted to obtain a monodispersed size and uniform shape of Fe3O4 nanoparticles while coprecipitation method was adapted to synthesize MnFe2O4 nanoparticles and the cyclic voltammetry was applied to examine the electrochemical properties of MnFe2O4. The morphology, chemical composition and electrochemical properties of synthesized magnetic nanoparticles were characterized using SEM, TEM, AAS and CV respectively. It was found that by increasing concentration of Fe(acac)3, the Fe3O4 nanoparticles size increases, the addition of oleic acid created a more uniform nanoparticles and longer time duration of thermal decomposition had increased the size of Fe3O4 nanoparticles. MnFe2O4 nanoparticles size was affected by the heating temperature, the presence of surfactant PVP and the metal salt concentration with hydroxide ions. The highest specific capacitance of MnFe2O4 nanoparticles was found to be at 500 ˚C and the higher the mass of the MnFe2O4 nanoparticles, the higher the charge capacity.
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format Final Year Project Report / IMRAD
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institution Universiti Malaysia Sarawak
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language English
English
last_indexed 2025-11-15T06:15:30Z
publishDate 2011
publisher Universiti Malaysia Sarawak, (UNIMAS)
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spelling unimas-64402024-05-03T07:44:16Z http://ir.unimas.my/id/eprint/6440/ Synthesis and characterizations of magnetic nanoparticles Tan, Ching Hong Q Science (General) QD Chemistry T Technology (General) Magnetic nanoparticles can be applied in various applications such as drug targeting and delivery, magnetic resonance imaging, electrochemical cells, capacitors and etc. However, these applications require narrow size distribution and uniform shape magnetic nanoparticles and the synthesis of these magnetic nanoparticles often result in a broad size distribution. In present study, thermal decomposition method was adapted to obtain a monodispersed size and uniform shape of Fe3O4 nanoparticles while coprecipitation method was adapted to synthesize MnFe2O4 nanoparticles and the cyclic voltammetry was applied to examine the electrochemical properties of MnFe2O4. The morphology, chemical composition and electrochemical properties of synthesized magnetic nanoparticles were characterized using SEM, TEM, AAS and CV respectively. It was found that by increasing concentration of Fe(acac)3, the Fe3O4 nanoparticles size increases, the addition of oleic acid created a more uniform nanoparticles and longer time duration of thermal decomposition had increased the size of Fe3O4 nanoparticles. MnFe2O4 nanoparticles size was affected by the heating temperature, the presence of surfactant PVP and the metal salt concentration with hydroxide ions. The highest specific capacitance of MnFe2O4 nanoparticles was found to be at 500 ˚C and the higher the mass of the MnFe2O4 nanoparticles, the higher the charge capacity. Universiti Malaysia Sarawak, (UNIMAS) 2011 Final Year Project Report / IMRAD NonPeerReviewed text en http://ir.unimas.my/id/eprint/6440/1/Ching%2824%20pgs%29.pdf text en http://ir.unimas.my/id/eprint/6440/4/TAN%20CHING%20HONG.pdf Tan, Ching Hong (2011) Synthesis and characterizations of magnetic nanoparticles. [Final Year Project Report / IMRAD] (Unpublished)
spellingShingle Q Science (General)
QD Chemistry
T Technology (General)
Tan, Ching Hong
Synthesis and characterizations of magnetic nanoparticles
title Synthesis and characterizations of magnetic nanoparticles
title_full Synthesis and characterizations of magnetic nanoparticles
title_fullStr Synthesis and characterizations of magnetic nanoparticles
title_full_unstemmed Synthesis and characterizations of magnetic nanoparticles
title_short Synthesis and characterizations of magnetic nanoparticles
title_sort synthesis and characterizations of magnetic nanoparticles
topic Q Science (General)
QD Chemistry
T Technology (General)
url http://ir.unimas.my/id/eprint/6440/
http://ir.unimas.my/id/eprint/6440/1/Ching%2824%20pgs%29.pdf
http://ir.unimas.my/id/eprint/6440/4/TAN%20CHING%20HONG.pdf