Physical, Mechanical, and Thermal Analysis of Polylactic Acid/Fumed Silica/Clay (1.28E) Nanocomposites

Polylactic acid/fumed silica/clay (PLA/FS/clay) (1.28E) nanocomposites have been successfully prepared by solution-intercalation film-casting technique. The resultant nanocomposites were characterized by Fourier Transform Infrared Spectroscopy (FT-IR), Scanning Electron Microscopy (SEM), tensile tes...

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Bibliographic Details
Main Authors: Lai, Josephine Chang Hui, Md. Rezaur, Rahman, Sinin, Hamdan
Format: Article
Language:English
Published: Hindawi Publishing Corporation 2015
Subjects:
Online Access:http://ir.unimas.my/id/eprint/12089/
http://ir.unimas.my/id/eprint/12089/1/No%2029%20%28abstrak%29.pdf
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Summary:Polylactic acid/fumed silica/clay (PLA/FS/clay) (1.28E) nanocomposites have been successfully prepared by solution-intercalation film-casting technique. The resultant nanocomposites were characterized by Fourier Transform Infrared Spectroscopy (FT-IR), Scanning Electron Microscopy (SEM), tensile test, thermogravimetric analysis (TGA), and moisture absorption test. The FT-IR spectrum indicated that PLA/FS/clay with 2 wt% hadmuch broader peak compared to 5 wt%, 10 wt%, and 15wt% nanocomposites. Incorporation of clay (1.28E) with 2wt% showed the best compatibility with PLA/FS matrix. PLA/FS/clay (1.28E) nanocomposite with 2wt% of clay loading had higher tensile strength and modulus compared to other nanocomposites. The thermal stability and activation energy of 2wt% of PLA/FS/clay (1.28E) nanocomposite are the highest among all the nanocomposites. The moisture absorbed into PLA/FS/clay (1.28E) nanocomposite was significantly reduced with clay loading of 2 wt%.