Testing the applicability of the k(o)-NAA method at the MINT's TRIGA MARK II reactor

The Analytical Chemistry Laboratory at MINT is using the NAA technique since 1980s and is the only laboratory in Malaysia equipped with a research reactor, namely the TRIGA MARK II. Throughout the years the development of NAA technique has been very encouraging and was made applicable to a wide ra...

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Main Authors: Wee, Boon Siong, Ho, Manh Dung, Ab. Khalik, Wood, Nazaratul Ashifa, Abdullah Salim, Md. Suhaimi, Elias
Format: Article
Language:English
Published: North-Holland 2006
Subjects:
Online Access:http://ir.unimas.my/id/eprint/10271/
http://ir.unimas.my/id/eprint/10271/1/Testing%20the%20applicability%20of%20the%20k%28o%29-NAA%20method%20at%20the%20MINT%27s%20TRIGA%20MARK%20II%20reactor%20%28abstract%29.pdf
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author Wee, Boon Siong
Ho, Manh Dung
Ab. Khalik, Wood
Nazaratul Ashifa, Abdullah Salim
Md. Suhaimi, Elias
author_facet Wee, Boon Siong
Ho, Manh Dung
Ab. Khalik, Wood
Nazaratul Ashifa, Abdullah Salim
Md. Suhaimi, Elias
author_sort Wee, Boon Siong
building UNIMAS Institutional Repository
collection Online Access
description The Analytical Chemistry Laboratory at MINT is using the NAA technique since 1980s and is the only laboratory in Malaysia equipped with a research reactor, namely the TRIGA MARK II. Throughout the years the development of NAA technique has been very encouraging and was made applicable to a wide range of samples. At present, the k0 method has become the preferred standardization method of NAA (k0-NAA) due to its multi-elemental analysis capability without using standards. Additionally, the k0 method describes NAA in physically and mathematically understandable definitions and is very suitable for computer evaluation. Eventually, the k0-NAA method has been adopted by MINT in 2003, in collaboration with the Nuclear Research Institute (NRI), Vietnam. The reactor neutron parameters (a and f) for the pneumatic transfer system and for the rotary rack at various locations, as well as the detector efficiencies were determined. After calibration of the reactor and the detectors, the implemented k0 method was validated by analyzing some certified reference materials (including IAEA Soil 7, NIST 1633a, NIST 1632c, NIST 1646a and IAEA 140/TM). The analysis results of the CRMs showed an average u score well below the threshold value of 2 with a precision of better than 710% for most of the elemental concentrations obtained, validating herewith the introduction of the k0-NAA method at the MINT.
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publisher North-Holland
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spelling unimas-102712016-01-19T07:45:42Z http://ir.unimas.my/id/eprint/10271/ Testing the applicability of the k(o)-NAA method at the MINT's TRIGA MARK II reactor Wee, Boon Siong Ho, Manh Dung Ab. Khalik, Wood Nazaratul Ashifa, Abdullah Salim Md. Suhaimi, Elias QD Chemistry The Analytical Chemistry Laboratory at MINT is using the NAA technique since 1980s and is the only laboratory in Malaysia equipped with a research reactor, namely the TRIGA MARK II. Throughout the years the development of NAA technique has been very encouraging and was made applicable to a wide range of samples. At present, the k0 method has become the preferred standardization method of NAA (k0-NAA) due to its multi-elemental analysis capability without using standards. Additionally, the k0 method describes NAA in physically and mathematically understandable definitions and is very suitable for computer evaluation. Eventually, the k0-NAA method has been adopted by MINT in 2003, in collaboration with the Nuclear Research Institute (NRI), Vietnam. The reactor neutron parameters (a and f) for the pneumatic transfer system and for the rotary rack at various locations, as well as the detector efficiencies were determined. After calibration of the reactor and the detectors, the implemented k0 method was validated by analyzing some certified reference materials (including IAEA Soil 7, NIST 1633a, NIST 1632c, NIST 1646a and IAEA 140/TM). The analysis results of the CRMs showed an average u score well below the threshold value of 2 with a precision of better than 710% for most of the elemental concentrations obtained, validating herewith the introduction of the k0-NAA method at the MINT. North-Holland 2006 Article NonPeerReviewed text en http://ir.unimas.my/id/eprint/10271/1/Testing%20the%20applicability%20of%20the%20k%28o%29-NAA%20method%20at%20the%20MINT%27s%20TRIGA%20MARK%20II%20reactor%20%28abstract%29.pdf Wee, Boon Siong and Ho, Manh Dung and Ab. Khalik, Wood and Nazaratul Ashifa, Abdullah Salim and Md. Suhaimi, Elias (2006) Testing the applicability of the k(o)-NAA method at the MINT's TRIGA MARK II reactor. Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, 564 (2). pp. 716-720. ISSN 0168-9002 https://scholar.google.com.my/citations?view_op=view_citation&hl=en&user=KmdSVJMAAAAJ&citation_for_view=KmdSVJMAAAAJ:YsMSGLbcyi4C doi:10.1016/j.nima.2006.04.012
spellingShingle QD Chemistry
Wee, Boon Siong
Ho, Manh Dung
Ab. Khalik, Wood
Nazaratul Ashifa, Abdullah Salim
Md. Suhaimi, Elias
Testing the applicability of the k(o)-NAA method at the MINT's TRIGA MARK II reactor
title Testing the applicability of the k(o)-NAA method at the MINT's TRIGA MARK II reactor
title_full Testing the applicability of the k(o)-NAA method at the MINT's TRIGA MARK II reactor
title_fullStr Testing the applicability of the k(o)-NAA method at the MINT's TRIGA MARK II reactor
title_full_unstemmed Testing the applicability of the k(o)-NAA method at the MINT's TRIGA MARK II reactor
title_short Testing the applicability of the k(o)-NAA method at the MINT's TRIGA MARK II reactor
title_sort testing the applicability of the k(o)-naa method at the mint's triga mark ii reactor
topic QD Chemistry
url http://ir.unimas.my/id/eprint/10271/
http://ir.unimas.my/id/eprint/10271/
http://ir.unimas.my/id/eprint/10271/
http://ir.unimas.my/id/eprint/10271/1/Testing%20the%20applicability%20of%20the%20k%28o%29-NAA%20method%20at%20the%20MINT%27s%20TRIGA%20MARK%20II%20reactor%20%28abstract%29.pdf