Conversion of Jatropha curcas Oil to Ester Biolubricant Using Solid Catalyst Derived from Saltwater Clam Shell Waste (SCSW)

The discarded clam shell waste, fossil and edible oil as biolubricant feed stock couse environment issues and food chain dilemma, thus this wok aim to solve this problem by using activated saltwater clam shell waste (SCSW) as solid catalyst for conversion of Jatropha curcas oil as non-edible sources...

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Main Authors: Said, N., Fatimah A., Misebah, R. M., Yunus, Mohd S., Mahmud, Ahmad Z., Sulaiman
Format: Article
Language:English
Published: World Academy of Science, Engineering and Technology 2014
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/7543/
http://umpir.ump.edu.my/id/eprint/7543/1/Conversion-of-Jatropha-curcas-Oil-to-Ester-Biolubricant-Using-Solid-Catalyst-Derived-from-Saltwater-Clam-Shell-Waste-SCSW.pdf
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author Said, N.
Fatimah A., Misebah
R. M., Yunus
Mohd S., Mahmud
Ahmad Z., Sulaiman
author_facet Said, N.
Fatimah A., Misebah
R. M., Yunus
Mohd S., Mahmud
Ahmad Z., Sulaiman
author_sort Said, N.
building UMP Institutional Repository
collection Online Access
description The discarded clam shell waste, fossil and edible oil as biolubricant feed stock couse environment issues and food chain dilemma, thus this wok aim to solve this problem by using activated saltwater clam shell waste (SCSW) as solid catalyst for conversion of Jatropha curcas oil as non-edible sources to ester biolubricant. The characterization of solid catalyst was done by DTA-TGA, XRF, XRD, BET, FESEM and FTIR analysis. The calcined catalyst was used in the transesterification of Jatropha curcas oil to methyl ester as the first step, and the second stage was involved the reaction of Jatropha methyl ester (JME) with trimethylolpropane (TMP) based on the various process parameter. The formated biolubricant was analyzed using the capillary column (DB-5HT) equipped GC. The maximum results of Jatropha oil conversion to ester biolubricant was 96.66% with 72.3% of trimetylolpropane triester (TMPTE) composition.
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spelling ump-75432018-01-15T02:41:50Z http://umpir.ump.edu.my/id/eprint/7543/ Conversion of Jatropha curcas Oil to Ester Biolubricant Using Solid Catalyst Derived from Saltwater Clam Shell Waste (SCSW) Said, N. Fatimah A., Misebah R. M., Yunus Mohd S., Mahmud Ahmad Z., Sulaiman TP Chemical technology The discarded clam shell waste, fossil and edible oil as biolubricant feed stock couse environment issues and food chain dilemma, thus this wok aim to solve this problem by using activated saltwater clam shell waste (SCSW) as solid catalyst for conversion of Jatropha curcas oil as non-edible sources to ester biolubricant. The characterization of solid catalyst was done by DTA-TGA, XRF, XRD, BET, FESEM and FTIR analysis. The calcined catalyst was used in the transesterification of Jatropha curcas oil to methyl ester as the first step, and the second stage was involved the reaction of Jatropha methyl ester (JME) with trimethylolpropane (TMP) based on the various process parameter. The formated biolubricant was analyzed using the capillary column (DB-5HT) equipped GC. The maximum results of Jatropha oil conversion to ester biolubricant was 96.66% with 72.3% of trimetylolpropane triester (TMPTE) composition. World Academy of Science, Engineering and Technology 2014 Article PeerReviewed application/pdf en cc_by http://umpir.ump.edu.my/id/eprint/7543/1/Conversion-of-Jatropha-curcas-Oil-to-Ester-Biolubricant-Using-Solid-Catalyst-Derived-from-Saltwater-Clam-Shell-Waste-SCSW.pdf Said, N. and Fatimah A., Misebah and R. M., Yunus and Mohd S., Mahmud and Ahmad Z., Sulaiman (2014) Conversion of Jatropha curcas Oil to Ester Biolubricant Using Solid Catalyst Derived from Saltwater Clam Shell Waste (SCSW). International Journal of Chemical, Molecular, Nuclear, Materials and Metallurgical Engineering, 8 (9). pp. 1023-1029. ISSN 1307-6892. (Published) http://waset.org/publications/9999674/conversion-of-jatropha-curcas-oil-to-ester-biolubricant-using-solid-catalyst-derived-from-saltwater-clam-shell-waste-scsw-
spellingShingle TP Chemical technology
Said, N.
Fatimah A., Misebah
R. M., Yunus
Mohd S., Mahmud
Ahmad Z., Sulaiman
Conversion of Jatropha curcas Oil to Ester Biolubricant Using Solid Catalyst Derived from Saltwater Clam Shell Waste (SCSW)
title Conversion of Jatropha curcas Oil to Ester Biolubricant Using Solid Catalyst Derived from Saltwater Clam Shell Waste (SCSW)
title_full Conversion of Jatropha curcas Oil to Ester Biolubricant Using Solid Catalyst Derived from Saltwater Clam Shell Waste (SCSW)
title_fullStr Conversion of Jatropha curcas Oil to Ester Biolubricant Using Solid Catalyst Derived from Saltwater Clam Shell Waste (SCSW)
title_full_unstemmed Conversion of Jatropha curcas Oil to Ester Biolubricant Using Solid Catalyst Derived from Saltwater Clam Shell Waste (SCSW)
title_short Conversion of Jatropha curcas Oil to Ester Biolubricant Using Solid Catalyst Derived from Saltwater Clam Shell Waste (SCSW)
title_sort conversion of jatropha curcas oil to ester biolubricant using solid catalyst derived from saltwater clam shell waste (scsw)
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/7543/
http://umpir.ump.edu.my/id/eprint/7543/
http://umpir.ump.edu.my/id/eprint/7543/1/Conversion-of-Jatropha-curcas-Oil-to-Ester-Biolubricant-Using-Solid-Catalyst-Derived-from-Saltwater-Clam-Shell-Waste-SCSW.pdf