Characterization of Bisphenol a MIP (BPA-MIP) Synthesizing

Molecular Imprinted Polymer (MIP) has caught the attention of many researches in recent years as a great tool for molecule recognition and other applications. But the main issue in the synthesis of MIP nanoparticles is the identification and optimization of the main factors affecting the material st...

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Main Authors: Shahaidah , Shariff, C. K. M., Faizal, Shareena, Mohd Sharif
Format: Article
Language:English
Published: Asian Network for Scientific Information 2014
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/5863/
http://umpir.ump.edu.my/id/eprint/5863/1/fkksa-2014-cheku-Characterization_of_Bisphenol_abs_only.pdf
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author Shahaidah , Shariff
C. K. M., Faizal
Shareena, Mohd Sharif
author_facet Shahaidah , Shariff
C. K. M., Faizal
Shareena, Mohd Sharif
author_sort Shahaidah , Shariff
building UMP Institutional Repository
collection Online Access
description Molecular Imprinted Polymer (MIP) has caught the attention of many researches in recent years as a great tool for molecule recognition and other applications. But the main issue in the synthesis of MIP nanoparticles is the identification and optimization of the main factors affecting the material structure and size. This study describe an experimental design approach to synthesis bisphenol A molecular imprinted polymer nanoparticles (BPA-MIP NPs) aimed at analysis of the relationship of four selected parameters: the polymerisation temperature, agitation rate, cross-linker to solvent ratio and percentage of initiator. The results presented demonstrate the importance of keeping the right balance between these various parameters of polymerisation conditions. Generally, it can be concluded that MIPs should be synthesized using enough heating, adequate agitation, low concentration of initiator and with a considerably higher amount of solvent. Such procedure is proven as time and cost effective and also can be used as a general tool in the preparation of MIPs for many different target molecules.
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spelling ump-58632018-01-15T01:07:09Z http://umpir.ump.edu.my/id/eprint/5863/ Characterization of Bisphenol a MIP (BPA-MIP) Synthesizing Shahaidah , Shariff C. K. M., Faizal Shareena, Mohd Sharif TP Chemical technology Molecular Imprinted Polymer (MIP) has caught the attention of many researches in recent years as a great tool for molecule recognition and other applications. But the main issue in the synthesis of MIP nanoparticles is the identification and optimization of the main factors affecting the material structure and size. This study describe an experimental design approach to synthesis bisphenol A molecular imprinted polymer nanoparticles (BPA-MIP NPs) aimed at analysis of the relationship of four selected parameters: the polymerisation temperature, agitation rate, cross-linker to solvent ratio and percentage of initiator. The results presented demonstrate the importance of keeping the right balance between these various parameters of polymerisation conditions. Generally, it can be concluded that MIPs should be synthesized using enough heating, adequate agitation, low concentration of initiator and with a considerably higher amount of solvent. Such procedure is proven as time and cost effective and also can be used as a general tool in the preparation of MIPs for many different target molecules. Asian Network for Scientific Information 2014 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/5863/1/fkksa-2014-cheku-Characterization_of_Bisphenol_abs_only.pdf Shahaidah , Shariff and C. K. M., Faizal and Shareena, Mohd Sharif (2014) Characterization of Bisphenol a MIP (BPA-MIP) Synthesizing. Journal of Applied Sciences, 14 (13). pp. 1455-1459. ISSN 1812-5654 (print); 1812-5662 (online). (Published) http://scialert.net/abstract/?doi=jas.2014.1455.1459 DOI: 10.3923/jas.2014.1455.1459
spellingShingle TP Chemical technology
Shahaidah , Shariff
C. K. M., Faizal
Shareena, Mohd Sharif
Characterization of Bisphenol a MIP (BPA-MIP) Synthesizing
title Characterization of Bisphenol a MIP (BPA-MIP) Synthesizing
title_full Characterization of Bisphenol a MIP (BPA-MIP) Synthesizing
title_fullStr Characterization of Bisphenol a MIP (BPA-MIP) Synthesizing
title_full_unstemmed Characterization of Bisphenol a MIP (BPA-MIP) Synthesizing
title_short Characterization of Bisphenol a MIP (BPA-MIP) Synthesizing
title_sort characterization of bisphenol a mip (bpa-mip) synthesizing
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/5863/
http://umpir.ump.edu.my/id/eprint/5863/
http://umpir.ump.edu.my/id/eprint/5863/
http://umpir.ump.edu.my/id/eprint/5863/1/fkksa-2014-cheku-Characterization_of_Bisphenol_abs_only.pdf