Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide
The crystal and molecular structure of (RS)-N-Tert-butyl-2-anilino-3,3-dirnethylbutanamide, a derivative of an amino acid that was obtained by highly selective cleavage of 1,3-di-tert-butylaziridinone by aniline, is described. The racemic mixture of the amide crystallizes in the space grot)p P 2in w...
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| Format: | Article |
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Springer
1997
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| Online Access: | http://umpir.ump.edu.my/id/eprint/4772/ |
| _version_ | 1848817464198037504 |
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| author | M. M., Yusoff Reibenspies, Joseph H. Talaty, Erach R. |
| author_facet | M. M., Yusoff Reibenspies, Joseph H. Talaty, Erach R. |
| author_sort | M. M., Yusoff |
| building | UMP Institutional Repository |
| collection | Online Access |
| description | The crystal and molecular structure of (RS)-N-Tert-butyl-2-anilino-3,3-dirnethylbutanamide, a derivative of an amino acid that was obtained by highly selective cleavage of 1,3-di-tert-butylaziridinone by aniline, is described. The racemic mixture of the amide crystallizes in the space grot)p P 2in with four molecules per unit cell. Crystal Data: a - 10.483(2) A, h - 6.206(I) A, c = 24.767(5) A, [3 - 90.39(3), V = 1611.5(6) A ~, R(F)[I > 2r = 0.0679, wR(F 2) [1 > 2or(l)] = 0. 1148.
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| first_indexed | 2025-11-15T01:22:11Z |
| format | Article |
| id | ump-4772 |
| institution | Universiti Malaysia Pahang |
| institution_category | Local University |
| last_indexed | 2025-11-15T01:22:11Z |
| publishDate | 1997 |
| publisher | Springer |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | ump-47722018-01-22T01:39:25Z http://umpir.ump.edu.my/id/eprint/4772/ Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide M. M., Yusoff Reibenspies, Joseph H. Talaty, Erach R. Q Science (General) QD Chemistry The crystal and molecular structure of (RS)-N-Tert-butyl-2-anilino-3,3-dirnethylbutanamide, a derivative of an amino acid that was obtained by highly selective cleavage of 1,3-di-tert-butylaziridinone by aniline, is described. The racemic mixture of the amide crystallizes in the space grot)p P 2in with four molecules per unit cell. Crystal Data: a - 10.483(2) A, h - 6.206(I) A, c = 24.767(5) A, [3 - 90.39(3), V = 1611.5(6) A ~, R(F)[I > 2r = 0.0679, wR(F 2) [1 > 2or(l)] = 0. 1148. Springer 1997-12 Article PeerReviewed M. M., Yusoff and Reibenspies, Joseph H. and Talaty, Erach R. (1997) Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide. Journal of Chemical Crystallography, 27 (12). pp. 727-730. ISSN 1074-1542 (print), 1572-8854 (online). (Published) http://dx.doi.org/10.1007/BF02576552 DOI: 10.1007/BF02576552 |
| spellingShingle | Q Science (General) QD Chemistry M. M., Yusoff Reibenspies, Joseph H. Talaty, Erach R. Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide |
| title | Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide |
| title_full | Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide |
| title_fullStr | Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide |
| title_full_unstemmed | Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide |
| title_short | Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide |
| title_sort | synthesis and x-ray analysis of (rs)-n-tert-butyl-2-anilino- 3,3-dimethylbutanamide |
| topic | Q Science (General) QD Chemistry |
| url | http://umpir.ump.edu.my/id/eprint/4772/ http://umpir.ump.edu.my/id/eprint/4772/ http://umpir.ump.edu.my/id/eprint/4772/ |