Effects of pH on Grain Size and Structure of ZnO Nanoparticle Synthesized via Sol–Gel Method for Enhanced Thermoelectric Materials

This chapter delves into the critical role of pH in the synthesis of ZnO nanoparticles using the sol–gel method, focusing on how varying pH levels influence grain size, structure, and thermoelectric performance. The study highlights the importance of nanostructuring and doping techniques to enhance...

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Main Authors: Suraya, Sulaiman, Tuan Muhammad, Tuan Zahrin, Nadhrah, Md Yatim, Mohd Faizul, Mohd Sabri, Mohamad Farid, Mohamad Sharif
Format: Book Chapter
Language:English
Published: Springer Nature Singapore 2024
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/44816/
http://umpir.ump.edu.my/id/eprint/44816/1/Effects%20of%20pH%20on%20Grain%20Size%20and%20Structure%20of%20ZnO%20Nanoparticle%20Synthesized.pdf
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author Suraya, Sulaiman
Tuan Muhammad, Tuan Zahrin
Nadhrah, Md Yatim
Mohd Faizul, Mohd Sabri
Mohamad Farid, Mohamad Sharif
author_facet Suraya, Sulaiman
Tuan Muhammad, Tuan Zahrin
Nadhrah, Md Yatim
Mohd Faizul, Mohd Sabri
Mohamad Farid, Mohamad Sharif
author_sort Suraya, Sulaiman
building UMP Institutional Repository
collection Online Access
description This chapter delves into the critical role of pH in the synthesis of ZnO nanoparticles using the sol–gel method, focusing on how varying pH levels influence grain size, structure, and thermoelectric performance. The study highlights the importance of nanostructuring and doping techniques to enhance the figure of merit (ZT) of ZnO-based thermoelectric materials. Through XRD analysis, the authors confirm the successful synthesis of highly crystalline ZnO nanoparticles with a hexagonal wurtzite structure. FESEM images reveal the impact of pH on the morphology of ZnO nanoparticles, with optimal conditions identified for achieving desirable crystalline structures and morphologies. EDX analysis validates the high purity and stoichiometric composition of the synthesized ZnO nanoparticles. The findings contribute to the development of more efficient thermoelectric materials for waste heat recovery, paving the way for sustainable energy solutions.
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format Book Chapter
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institution Universiti Malaysia Pahang
institution_category Local University
language English
last_indexed 2025-11-15T03:56:46Z
publishDate 2024
publisher Springer Nature Singapore
recordtype eprints
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spelling ump-448162025-06-16T03:33:59Z http://umpir.ump.edu.my/id/eprint/44816/ Effects of pH on Grain Size and Structure of ZnO Nanoparticle Synthesized via Sol–Gel Method for Enhanced Thermoelectric Materials Suraya, Sulaiman Tuan Muhammad, Tuan Zahrin Nadhrah, Md Yatim Mohd Faizul, Mohd Sabri Mohamad Farid, Mohamad Sharif TJ Mechanical engineering and machinery TS Manufactures This chapter delves into the critical role of pH in the synthesis of ZnO nanoparticles using the sol–gel method, focusing on how varying pH levels influence grain size, structure, and thermoelectric performance. The study highlights the importance of nanostructuring and doping techniques to enhance the figure of merit (ZT) of ZnO-based thermoelectric materials. Through XRD analysis, the authors confirm the successful synthesis of highly crystalline ZnO nanoparticles with a hexagonal wurtzite structure. FESEM images reveal the impact of pH on the morphology of ZnO nanoparticles, with optimal conditions identified for achieving desirable crystalline structures and morphologies. EDX analysis validates the high purity and stoichiometric composition of the synthesized ZnO nanoparticles. The findings contribute to the development of more efficient thermoelectric materials for waste heat recovery, paving the way for sustainable energy solutions. Springer Nature Singapore 2024 Book Chapter PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/44816/1/Effects%20of%20pH%20on%20Grain%20Size%20and%20Structure%20of%20ZnO%20Nanoparticle%20Synthesized.pdf Suraya, Sulaiman and Tuan Muhammad, Tuan Zahrin and Nadhrah, Md Yatim and Mohd Faizul, Mohd Sabri and Mohamad Farid, Mohamad Sharif (2024) Effects of pH on Grain Size and Structure of ZnO Nanoparticle Synthesized via Sol–Gel Method for Enhanced Thermoelectric Materials. In: Intelligent Manufacturing and Mechatronics. Springer Proceedings in Materials, 40 . Springer Nature Singapore, Singapore, 233 -242. ISBN 978-981-99-9847-0 https://doi.org/10.1007/978-981-99-9848-7_21 https://doi.org/10.1007/978-981-99-9848-7_21
spellingShingle TJ Mechanical engineering and machinery
TS Manufactures
Suraya, Sulaiman
Tuan Muhammad, Tuan Zahrin
Nadhrah, Md Yatim
Mohd Faizul, Mohd Sabri
Mohamad Farid, Mohamad Sharif
Effects of pH on Grain Size and Structure of ZnO Nanoparticle Synthesized via Sol–Gel Method for Enhanced Thermoelectric Materials
title Effects of pH on Grain Size and Structure of ZnO Nanoparticle Synthesized via Sol–Gel Method for Enhanced Thermoelectric Materials
title_full Effects of pH on Grain Size and Structure of ZnO Nanoparticle Synthesized via Sol–Gel Method for Enhanced Thermoelectric Materials
title_fullStr Effects of pH on Grain Size and Structure of ZnO Nanoparticle Synthesized via Sol–Gel Method for Enhanced Thermoelectric Materials
title_full_unstemmed Effects of pH on Grain Size and Structure of ZnO Nanoparticle Synthesized via Sol–Gel Method for Enhanced Thermoelectric Materials
title_short Effects of pH on Grain Size and Structure of ZnO Nanoparticle Synthesized via Sol–Gel Method for Enhanced Thermoelectric Materials
title_sort effects of ph on grain size and structure of zno nanoparticle synthesized via sol–gel method for enhanced thermoelectric materials
topic TJ Mechanical engineering and machinery
TS Manufactures
url http://umpir.ump.edu.my/id/eprint/44816/
http://umpir.ump.edu.my/id/eprint/44816/
http://umpir.ump.edu.my/id/eprint/44816/
http://umpir.ump.edu.my/id/eprint/44816/1/Effects%20of%20pH%20on%20Grain%20Size%20and%20Structure%20of%20ZnO%20Nanoparticle%20Synthesized.pdf