Extensive stability assessment of TiO2/polyvinyl ether nanolubricant with physical homogenization

Proper preparation and stability evaluation of the nanolubricant shall be established when applying the nanoparticle dispersion technique in a two-phase system. The stability of the nanolubricant ensures the maximum benefit gained from the dispersion of nanoparticles in specified Polyvinyl ether (PV...

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Main Authors: Mohd Farid, Ismail, Wan Hamzah, Azmi, Rizalman, Mamat, Sharma, Korada Viswanatha, Hafiz, Muhammad Ali
Format: Article
Language:English
Published: MDPI 2023
Subjects:
Online Access:https://umpir.ump.edu.my/id/eprint/44762/
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author Mohd Farid, Ismail
Wan Hamzah, Azmi
Rizalman, Mamat
Sharma, Korada Viswanatha
Hafiz, Muhammad Ali
author_facet Mohd Farid, Ismail
Wan Hamzah, Azmi
Rizalman, Mamat
Sharma, Korada Viswanatha
Hafiz, Muhammad Ali
author_sort Mohd Farid, Ismail
building UMP Institutional Repository
collection Online Access
description Proper preparation and stability evaluation of the nanolubricant shall be established when applying the nanoparticle dispersion technique in a two-phase system. The stability of the nanolubricant ensures the maximum benefit gained from the dispersion of nanoparticles in specified Polyvinyl ether (PVE). In this study, TiO2/PVE nanolubricant was prepared using two methods of physical homogenization: high-speed homogenizer (HSH) and ultrasonication bath. The HSH used a preparation time of up to 300 s in the stability assessment. Meanwhile, the ultrasonication bath had a preparation time of 1, 3, 5, and 7 h. The stability condition of the nanolubricant was evaluated using photo capturing, ultraviolet-visible (UV-Vis) spectrophotometer, zeta potential, and zeta sizer. A sample with 180 s of preparation time shows the best stability condition from HSH. The nanolubricant with ultrasonication offers excellent stability at 5 h of homogenizing time with a concentration ratio of more than 90% for up to 30 days of observation. In conclusion, ultrasonication homogenizing methods show better results than HSH with a zeta potential of more than 60 mV. In addition, HSH can be recommended as an optional method to produce nanolubricant with a low preparation time for immediate use.
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spelling ump-447622025-08-27T07:06:01Z https://umpir.ump.edu.my/id/eprint/44762/ Extensive stability assessment of TiO2/polyvinyl ether nanolubricant with physical homogenization Mohd Farid, Ismail Wan Hamzah, Azmi Rizalman, Mamat Sharma, Korada Viswanatha Hafiz, Muhammad Ali TJ Mechanical engineering and machinery TP Chemical technology Proper preparation and stability evaluation of the nanolubricant shall be established when applying the nanoparticle dispersion technique in a two-phase system. The stability of the nanolubricant ensures the maximum benefit gained from the dispersion of nanoparticles in specified Polyvinyl ether (PVE). In this study, TiO2/PVE nanolubricant was prepared using two methods of physical homogenization: high-speed homogenizer (HSH) and ultrasonication bath. The HSH used a preparation time of up to 300 s in the stability assessment. Meanwhile, the ultrasonication bath had a preparation time of 1, 3, 5, and 7 h. The stability condition of the nanolubricant was evaluated using photo capturing, ultraviolet-visible (UV-Vis) spectrophotometer, zeta potential, and zeta sizer. A sample with 180 s of preparation time shows the best stability condition from HSH. The nanolubricant with ultrasonication offers excellent stability at 5 h of homogenizing time with a concentration ratio of more than 90% for up to 30 days of observation. In conclusion, ultrasonication homogenizing methods show better results than HSH with a zeta potential of more than 60 mV. In addition, HSH can be recommended as an optional method to produce nanolubricant with a low preparation time for immediate use. MDPI 2023 Article PeerReviewed pdf en cc_by_4 https://umpir.ump.edu.my/id/eprint/44762/1/Extensive%20stability%20assessment%20of%20TiO2polyvinyl%20ether%20nanolubricant.pdf Mohd Farid, Ismail and Wan Hamzah, Azmi and Rizalman, Mamat and Sharma, Korada Viswanatha and Hafiz, Muhammad Ali (2023) Extensive stability assessment of TiO2/polyvinyl ether nanolubricant with physical homogenization. Lubricants, 11 (2). pp. 1-18. ISSN 2075-4442. (Published) https://doi.org/10.3390/lubricants11020067 https://doi.org/10.3390/lubricants11020067 https://doi.org/10.3390/lubricants11020067
spellingShingle TJ Mechanical engineering and machinery
TP Chemical technology
Mohd Farid, Ismail
Wan Hamzah, Azmi
Rizalman, Mamat
Sharma, Korada Viswanatha
Hafiz, Muhammad Ali
Extensive stability assessment of TiO2/polyvinyl ether nanolubricant with physical homogenization
title Extensive stability assessment of TiO2/polyvinyl ether nanolubricant with physical homogenization
title_full Extensive stability assessment of TiO2/polyvinyl ether nanolubricant with physical homogenization
title_fullStr Extensive stability assessment of TiO2/polyvinyl ether nanolubricant with physical homogenization
title_full_unstemmed Extensive stability assessment of TiO2/polyvinyl ether nanolubricant with physical homogenization
title_short Extensive stability assessment of TiO2/polyvinyl ether nanolubricant with physical homogenization
title_sort extensive stability assessment of tio2/polyvinyl ether nanolubricant with physical homogenization
topic TJ Mechanical engineering and machinery
TP Chemical technology
url https://umpir.ump.edu.my/id/eprint/44762/
https://umpir.ump.edu.my/id/eprint/44762/
https://umpir.ump.edu.my/id/eprint/44762/