Unveiling the importance of controllable growth of c-axis oriented Sn-doped ZnO nanorod arrays: Towards humidity sensing applications

In this study, tin (Sn)-doped zinc oxide (ZnO) nanorod arrays (SZO) were prepared using a sonication assisted sol gel immersion method, with the growth of the nanorod arrays controlled by varying the immersion time in the precursor material. Morphology images taken using a Field Emission Scanning E...

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Main Authors: Ahmad Syakirin, Ismail @ Rosdi, M. H., Mamat, R., Mohamed, Z., Embong, Kossar, S.
Other Authors: Vincenzini, Pietro
Format: Article
Language:English
Published: Elsevier 2025
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/44176/
http://umpir.ump.edu.my/id/eprint/44176/1/1-s2.0-S0272884224055342-main.pdf
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author Ahmad Syakirin, Ismail @ Rosdi
M. H., Mamat
R., Mohamed
Z., Embong
Kossar, S.
author2 Vincenzini, Pietro
author_facet Vincenzini, Pietro
Ahmad Syakirin, Ismail @ Rosdi
M. H., Mamat
R., Mohamed
Z., Embong
Kossar, S.
author_sort Ahmad Syakirin, Ismail @ Rosdi
building UMP Institutional Repository
collection Online Access
description In this study, tin (Sn)-doped zinc oxide (ZnO) nanorod arrays (SZO) were prepared using a sonication assisted sol gel immersion method, with the growth of the nanorod arrays controlled by varying the immersion time in the precursor material. Morphology images taken using a Field Emission Scanning Electron Microscope (FESEM) demonstrated an enlargement of the average diameter of the nanorod arrays from 55 nm at 5 min immersion to 122 nm at 200 min immersion. The cross-sectional and surface elemental analysis showed that the sample immersed for 60 min has the highest detection of Sn, with a bulk concentration of 1.8 at.% and surface concentration of 1 at.%. Interestingly, we noticed that Sn is not exist on the surface of 200 min immersion, indicating the depletion of the Sn precursor due to the prolongation of the immersion time. From the current voltage (I-V) analysis, 60 min immersion sample generated the lowest thin film resistivity, which engendered the best humidity sensitivity of 4.05. This study demonstrated the significant importance of optimizing the immersion or growth time for doped 1-D nanostructures to obtain the best humidity sensing performance.
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institution Universiti Malaysia Pahang
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language English
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publishDate 2025
publisher Elsevier
recordtype eprints
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spelling ump-441762025-04-07T07:27:59Z http://umpir.ump.edu.my/id/eprint/44176/ Unveiling the importance of controllable growth of c-axis oriented Sn-doped ZnO nanorod arrays: Towards humidity sensing applications Ahmad Syakirin, Ismail @ Rosdi M. H., Mamat R., Mohamed Z., Embong Kossar, S. QC Physics TK Electrical engineering. Electronics Nuclear engineering TS Manufactures In this study, tin (Sn)-doped zinc oxide (ZnO) nanorod arrays (SZO) were prepared using a sonication assisted sol gel immersion method, with the growth of the nanorod arrays controlled by varying the immersion time in the precursor material. Morphology images taken using a Field Emission Scanning Electron Microscope (FESEM) demonstrated an enlargement of the average diameter of the nanorod arrays from 55 nm at 5 min immersion to 122 nm at 200 min immersion. The cross-sectional and surface elemental analysis showed that the sample immersed for 60 min has the highest detection of Sn, with a bulk concentration of 1.8 at.% and surface concentration of 1 at.%. Interestingly, we noticed that Sn is not exist on the surface of 200 min immersion, indicating the depletion of the Sn precursor due to the prolongation of the immersion time. From the current voltage (I-V) analysis, 60 min immersion sample generated the lowest thin film resistivity, which engendered the best humidity sensitivity of 4.05. This study demonstrated the significant importance of optimizing the immersion or growth time for doped 1-D nanostructures to obtain the best humidity sensing performance. Elsevier Vincenzini, Pietro 2025-02 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/44176/1/1-s2.0-S0272884224055342-main.pdf Ahmad Syakirin, Ismail @ Rosdi and M. H., Mamat and R., Mohamed and Z., Embong and Kossar, S. (2025) Unveiling the importance of controllable growth of c-axis oriented Sn-doped ZnO nanorod arrays: Towards humidity sensing applications. Unveiling the importance of controllable growth of c-axis oriented Sn-doped ZnO nanorod arrays: Towards humidity sensing applications, 51 (4). 4487 -4499. ISSN 1873-3956. (Published) https://doi.org/10.1016/j.ceramint.2024.11.424 https://doi.org/10.1016/j.ceramint.2024.11.424
spellingShingle QC Physics
TK Electrical engineering. Electronics Nuclear engineering
TS Manufactures
Ahmad Syakirin, Ismail @ Rosdi
M. H., Mamat
R., Mohamed
Z., Embong
Kossar, S.
Unveiling the importance of controllable growth of c-axis oriented Sn-doped ZnO nanorod arrays: Towards humidity sensing applications
title Unveiling the importance of controllable growth of c-axis oriented Sn-doped ZnO nanorod arrays: Towards humidity sensing applications
title_full Unveiling the importance of controllable growth of c-axis oriented Sn-doped ZnO nanorod arrays: Towards humidity sensing applications
title_fullStr Unveiling the importance of controllable growth of c-axis oriented Sn-doped ZnO nanorod arrays: Towards humidity sensing applications
title_full_unstemmed Unveiling the importance of controllable growth of c-axis oriented Sn-doped ZnO nanorod arrays: Towards humidity sensing applications
title_short Unveiling the importance of controllable growth of c-axis oriented Sn-doped ZnO nanorod arrays: Towards humidity sensing applications
title_sort unveiling the importance of controllable growth of c-axis oriented sn-doped zno nanorod arrays: towards humidity sensing applications
topic QC Physics
TK Electrical engineering. Electronics Nuclear engineering
TS Manufactures
url http://umpir.ump.edu.my/id/eprint/44176/
http://umpir.ump.edu.my/id/eprint/44176/
http://umpir.ump.edu.my/id/eprint/44176/
http://umpir.ump.edu.my/id/eprint/44176/1/1-s2.0-S0272884224055342-main.pdf